Published online Apr 30, 2011.
https://doi.org/10.4047/jkap.2011.49.2.161
Influence of porcelain re-firing on the formation of surface bubble and on the change in shade of metal-ceramic crown exposed to artificial saliva
Abstract
Purpose
The purpose of this study was to evaluate the influence of porcelain re-firing on the formation of surface bubble and on the change in shade of metal-ceramic crown exposed to artificial saliva.
Materials and methods
Thirty disk-shaped specimens were made in 10 mm diameter with 0.5 mm metal core thickness and 1 mm ceramic thickness. A spectroradiometer was used to determine the CIE Lab coordinates. The number and size of surface bubble were observed with a stereomicroscope. After the exposure to artificial saliva for 7 days, re-firing was performed at glazing temperature. After re-firing, the CIE Lab were calculated, and the number and size of surface bubble were observed again. The change in shade was expressed with ΔE. Statistical analysis was done with paired t-test for the change in the number of surface bubble and student t-test for the change in the size of surface bubble (α= 0.05).
Results
Shade difference was calculated 2.14 ΔE units. The mean number of surface bubble was 1.33 ± 1.49 before re-firing, 3.27 ± 2.90 after re-firing. After re-firing, the number of surface bubble was significantly increased (P<.05). The mean size of surface bubble was 81.97 ± 32.03 µm before re-firing, 142.94 ± 47.40 µm after re-firing. After re-firing, the size of surface bubble was significantly increased (P<.05).
Conclusion
Shade change after re-firing was perceptible (ΔE < 2.0) and clinically acceptable (ΔE < 3.7). The number and size of surface bubble was significantly increased after re-firing. Further investigation to decrease the surface bubble on the extra oral repair of metal-ceramic crown, will be needed in future study.
Fig. 1
Generated large bubble.
Fig. 2
Effect of immersion in acetone. A: Removal of organic materials, B: Combustion of organic materials.
Fig. 3
Procedure of specimen fabrication. A: Metal coping, B: Mold for porcelain build up, C: fabricated specimens.
Fig. 4
Increase of air bubbles on porcelain surface after re-firing was detected in the stereomicroscope images. (arrows) (Original magnification, ×20). A: Before re-firing, B: After re-firing.
Table 1
Firing procedures
Table 2
Change in shade after re-firing
Table 3
Change in number of air bubbles after re-firing
Table 4
Change in size of air bubbles after re-firing (unit: µm)
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