Synthesis and Characterization of Mesoporous Molecular Sieve Al-MCM-41 Using Kaolin as Raw Material

Miao Li; Hong Wang; Xian Qing Li; Jin Rong Liu

doi:10.4028/www.scientific.net/AMR.779-780.201

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 779-780Synthesis and Characterization of Mesoporous...

Synthesis and Characterization of Mesoporous Molecular Sieve Al-MCM-41 Using Kaolin as Raw Material

Abstract:

Ordered hexagonally mesoporous molecular sieve Al-MCM-41 with Si/Al (atom) ratio=9 was prepared by hydrothermal synthesis using raw kaolin. X-ray diffraction (XRD), Nitrogen adsorption desorption, Transmission Electron Microscope (TEM) and Energy Dispersive X-ray Detector (EDX) were employed to characterise raw kaolin, calcined kaolin, as-synthesized and calcined Al-MCM-41. The results indicated that characteristic reflections of raw kaolin disappeared after calcination, both of as-synthesized and calcined Al-MCM-41 exhibited well ordered hexagonally mesoporous molecular sieve structure.

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Periodical:

Advanced Materials Research (Volumes 779-780)

Pages:

201-204

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.779-780.201

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Online since:

September 2013

Authors:

Miao Li, Hong Wang, Xian Qing Li, Jin Rong Liu

Keywords:

Al-MCM-41, Kaolin, Mesoporous Molecular Sieve

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