Fabrication of SnO2/Zn2SnO4/ZnO Nanocables through Thermal Oxidation of Zn and Sn Mixture Powders

Ling Min Yu; Xin Hui Fan; Jing Yi Shui; Lei Cao; Wen Yan

doi:10.4028/www.scientific.net/AMR.532-533.70

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 532-533Fabrication of SnO2/Zn2SnO4/ZnO Nanocables through...

Fabrication of SnO₂/Zn₂SnO₄/ZnO Nanocables through Thermal Oxidation of Zn and Sn Mixture Powders

Abstract:

We demonstrate the synthesis of a three-layer-coaxial SnO₂/ZnSn₂O₄/ZnO core–shell nanocable heterostructures with diameters 80-150 nm via thermal oxidation of Zn and Sn mixture powders. The products are characterized by scanning electron microscopy (SEM), X-ray powder diffraction (XRD) and field emission transmission electron microscopy (TEM). The structural analysis shows the formation of ZnSnO₄ in the interface region between the SnO₂ core and ZnO shell, which is resulted from inter－diffusion of Sn and Zn ions during thermal evaporation. The selected area electron diffraction (SAED) pattern was composed of two series of overlapped polycrystalline rings attributed to SnO₂ and Zn₂SnO₄, one set of hexahedron diffraction spots that can be indexed to the hexagonal ZnO. On the basis of investigation of the microstructures, the possible formation mechanism of Zn₂SnO₄ is discussed.

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Periodical:

Advanced Materials Research (Volumes 532-533)

Pages:

70-73

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.532-533.70

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Online since:

June 2012

Authors:

Ling Min Yu, Xin Hui Fan, Jing Yi Shui, Lei Cao, Wen Yan

Keywords:

Nanocables, SnO₂, Thermal Oxidation, Zinc Oxide (ZnO)

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