• CN:11-2187/TH
  • ISSN:0577-6686

机械工程学报 ›› 2021, Vol. 57 ›› Issue (15): 246-254.doi: 10.3901/JME.2021.15.246

• 制造工艺与装备 • 上一篇    下一篇

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脆性材料在韧性域内的往复纳米划痕深度预测研究

于洲, 余家欣, 袁卫锋, 赖建平, 何洪途   

  1. 西南科技大学制造过程测试技术教育部重点实验室 绵阳 621010
  • 收稿日期:2020-10-26 修回日期:2021-03-09 出版日期:2021-08-05 发布日期:2021-11-03
  • 通讯作者: 余家欣(通信作者),男,1982年出生,博士,教授,博士研究生导师。主要研究方向为摩擦学与超精密加工。E-mail:yujiaxin@swust.edu.cn
  • 作者简介:于洲,男,1996年出生。主要研究方向为纳米摩擦学。E-mail:15281135900@163.com;袁卫锋,男,1970年出生,博士,教授,博士研究生导师。主要研究方向为复合材料力学及计算力学。E-mail:yuanweifeng@swust.edu.cn
  • 基金资助:
    国家自然科学基金面上(51975492,51575462)和四川省教育厅科研重点(18ZA0504)资助项目。

Analytical Prediction of Reciprocating Nanoscratch Depth for Brittle Materials in the Ductile Regime

YU Zhou, YU Jiaxin, YUAN Weifeng, LAI Jianping, HE Hongtu   

  1. Key Laboratory of Testing Technology for Manufacturing Process in Ministry of Education, Southwest University of Science and Technology, Mianyang 621010
  • Received:2020-10-26 Revised:2021-03-09 Online:2021-08-05 Published:2021-11-03

摘要: 提出了一种基于多道次划痕法的划痕深度的预测模型,在此模型中,基本假设为在针尖与材料弹性接触后,在每道次划痕中的划痕深度增量与赫兹接触理论得到的最大剪应力深度成正相关。随后通过建立每道次划痕时针尖与样品接触半径的递推关系,获得每道次划痕深度增量的递推关系,并通过划痕深度增量的总和来建立多次划痕深度的预测模型。考虑到脆性材料在多次划痕过程中会出现力学性能的变化,因此在预测模型中引入了材料弹性模量的修正方程以提高预测模型的精确性。为了验证上述模型的可靠性,本研究在压痕弹性载荷作用下,以磷酸盐激光玻璃为样品,采用球形金刚石针尖进行了多道次往复纳米划痕试验,并实现了对不同次数下的纳米划痕深度的预测。在通过对玻璃样品的弹性模量修正后,发现预测划痕深度和试验深度吻合度高。修正后的弹性模量根据划痕载荷的不同表现为随划痕次数不同的变化趋势,这与玻璃材料在不同载荷下剪切应力诱发的致密化与损伤软化相关。本研究所提出的计算模型理论基础可靠,同时考虑了材料自身力学性能的变化,因此有望推广到其他脆硬材料的纳米划痕变形演变预测中。

关键词: 纳米划痕, 预测模型, 赫兹接触理论, 模量修正, 脆性材料

Abstract: Based on the multi-trace scratch method, a model which predicts the wear depth of the scratch has been proposed in this study. It assumes that the increment of wear depth in each scratch is positively correlated with the maximum shear stress depth obtained by Hertz contact theory due to the elastic contact between the tip and materials. By establishing the recursive relation between the tip and the sample contact radius at each scratch, the recursive relation of each wear depth increment is obtained. The prediction model of multiple wear depth is established through adding the increment of the wear depth. Considering that the change of the mechanical properties of the brittle materials during the wear experiments, the modified equation of elastic modulus is introduced to improve the accuracy of the prediction model. To verify the reliability of the proposed model, various nanoscratches at the optical glass surfaces are achieved by rubbing against a spherical diamond tip under the condition of indentation-elastic-load. The experimental results show that the prediction model provides the better accurate prediction of the wear depth after modifying the elastic modulus of glass materials. The modified elastic modulus varies with the wear cycles based on the different applied load. Further analysis indicates that it is related to the densification and damage softening induced by shear stress. The theoretical basis of the proposed model is reliable which considering the change of the mechanical properties of the material. These results are expected to be extended to the prediction of nanoscratch deformation evolution of other brittle and hard materials.

Key words: nanoscratch, prediction model, Hertz contact theory, modified modulus, brittle materials

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