Hydrothermal Synthesis of Silver Sulfide

S. I. Sadovnikov; Садовников С. И.

doi:10.31857/S0044457X22602000

Hydrothermal Synthesis of Silver Sulfide

Authors: Sadovnikov S.I.¹
Affiliations:
1. Institute of Solid-State Chemistry, Ural Branch, Russian Academy of Sciences
Issue: Vol 68, No 5 (2023)
Pages: 589-596
Section: СИНТЕЗ И СВОЙСТВА НЕОРГАНИЧЕСКИХ СОЕДИНЕНИЙ
URL: https://journals.rcsi.science/0044-457X/article/view/136351
DOI: https://doi.org/10.31857/S0044457X22602000
EDN: https://elibrary.ru/SNAAWI
ID: 136351

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Abstract
About the authors
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Abstract

Silver sulfide powders with submicro- and micrometer particle sizes have been synthesized by the hydrothermal method at temperatures from 373 to 453 K in aqueous and alcoholic solutions of silver nitrate, sodium sulfide and citrate, sulfur, and thiocarbamide. The crystal structures of the synthesized powders, morphology, composition, and particle size of silver sulfide have been analyzed by X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray analysis, and gas adsorption. The powder particles have a similar morphology in the form of rectangular parallelepipeds and cubes with smoothed edges; the size of the powder particles depends on the synthesis conditions and ranges from ~500 to 2000 nm.

Keywords

silver sulfide, hydrothermal synthesis, particle size and morphology, EDX analysis

About the authors

S. I. Sadovnikov

Institute of Solid-State Chemistry, Ural Branch, Russian Academy of Sciences

Author for correspondence.
Email: sadovnikov@ihim.uran.ru
620990, Yekaterinburg, Russia

References

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