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Manuscript ID : 686640 Visit : 67 Page: 451 - 456

10.22034/jchr.2021.686640

Article Type: Original Research

Comparative Studies between Conventional Techniques and Green Chemistry to Synthesis of Novel Piperidinium Salts Ionic Liquids (PBSILs)

Subject Areas : Journal of Chemical Health Risks

Shakir M.  Saied 1 (Department of Medical Laboratories Technologies, Al-Noor University College, Barttella, Mosul, Iraq)
Salim J.  Mohammed 2 (Department of Chemistry, College of Science, University of Mosul, Ninevah, Iraq)
Bassam T.  Khaleel 3 (Department of Dentistry, Al-Noor University College, Barttella, Mousl, Iraq)
Mohanad  Saleh 4 (Department of Chemistry, College of Education for pure science, University of Mosul. Ninevah, Iraq)

Received: 2021-08-30 Accepted : 2021-11-27 Published : 2021-12-01

Keywords: Ionic liquids, Synthesis, Alkyl piperidinium salts, Spectroscopic investigation Introduction,

Abstract :

Comparative studies between conventional technique, method (A) and green chemistry (microwave irradiation) , method (B) to synthesis of four novel unsymmetrical alkyl piperidinium salts ionic liquids (PBSILs) by the addition of alkyl halides (methyl or allyl) to piperidine with yields more than (90%) in method (A) and less than (70%) in method (B) respectively with decrease reaction time. Theses novel organic salts are characterized by elemental analysis, 1H NMR, FTIR and mass spectrometry.

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