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Title: The design of an automated electrolytic enrichment apparatus for tritium

Technical Report ·
DOI:https://doi.org/10.2172/96644· OSTI ID:96644

The Radiation Analytical Sciences Section at Laboratory at Lawrence Livermore National Laboratory performs analysis of low-level tritium concentrations in various natural water samples from the Tri-Valley Area, DOE Nevada Test Site, Site 300 in Tracy, CA, and other various places around the world. Low levels of tritium, a radioactive isotope of hydrogen, which is pre-concentrated in the RAS laboratory using an electrolytic enrichment apparatus. Later these enriched waters are analyzed by liquid scintillation counting to determine the activity of tritium. The enrichment procedure and the subsequent purification process by vacuum distillation are currently undertaken manually, hence being highly labor-intensive. The whole process typically takes about 2 to 3 weeks to complete a batch of 30 samples, with a dedicated personnel operating the process. The goal is to automate the entire process, specifically having the operation PC-LabVIEW{trademark} controlled with real-time monitoring capability. My involvement was in the design and fabrication of a prototypical automated electrolytic enrichment cell. Work will be done on optimizing the electrolytic process by assessing the different parameters of the enrichment procedure. Hardware and software development have also been an integral component of this project.

Research Organization:
Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)
OSTI ID:
96644
Report Number(s):
UCRL-ID-114972-3; ON: DE95009444; TRN: 95:004626-0014
Resource Relation:
Other Information: PBD: Dec 1994; Related Information: Is Part Of SERS internship: Fall 1994 abstracts and research papers; Goldman, B.; PB: 352 p.
Country of Publication:
United States
Language:
English