Thiele, Karl-Heinz, Scholz, Annett, Scholz, Joachim, Böhme, Uwe, Kempe, Rhett and Sieler, Joachim. "Iminoacetylacetonat-Komplexe der Lanthanoide: Synthese, Eigenschaften und Struktur / Iminoacetylacetonate Complexes of Lanthanides: Synthesis, Properties and Structure"
Zeitschrift für Naturforschung B, vol. 48, no. 12, 1993, pp. 1753-1759.
https://doi.org/10.1515/znb-1993-1210Thiele, K., Scholz, A., Scholz, J., Böhme, U., Kempe, R. & Sieler, J. (1993). Iminoacetylacetonat-Komplexe der Lanthanoide: Synthese, Eigenschaften und Struktur / Iminoacetylacetonate Complexes of Lanthanides: Synthesis, Properties and Structure.
Zeitschrift für Naturforschung B,
48(12), 1753-1759.
https://doi.org/10.1515/znb-1993-1210Thiele, K., Scholz, A., Scholz, J., Böhme, U., Kempe, R. and Sieler, J. (1993) Iminoacetylacetonat-Komplexe der Lanthanoide: Synthese, Eigenschaften und Struktur / Iminoacetylacetonate Complexes of Lanthanides: Synthesis, Properties and Structure. Zeitschrift für Naturforschung B, Vol. 48 (Issue 12), pp. 1753-1759.
https://doi.org/10.1515/znb-1993-1210Thiele, Karl-Heinz, Scholz, Annett, Scholz, Joachim, Böhme, Uwe, Kempe, Rhett and Sieler, Joachim. "Iminoacetylacetonat-Komplexe der Lanthanoide: Synthese, Eigenschaften und Struktur / Iminoacetylacetonate Complexes of Lanthanides: Synthesis, Properties and Structure"
Zeitschrift für Naturforschung B 48, no. 12 (1993): 1753-1759.
https://doi.org/10.1515/znb-1993-1210Thiele K, Scholz A, Scholz J, Böhme U, Kempe R, Sieler J. Iminoacetylacetonat-Komplexe der Lanthanoide: Synthese, Eigenschaften und Struktur / Iminoacetylacetonate Complexes of Lanthanides: Synthesis, Properties and Structure.
Zeitschrift für Naturforschung B. 1993;48(12): 1753-1759.
https://doi.org/10.1515/znb-1993-1210Copied to clipboard
, (Ln = Y, La, Lu; R = C6H5, C6H4-4-Me) 4a-d which have been characterized by IR, NMR and mass spectrometry. In the case of the lanthanum complex 4c, the chelating structure was confirmed by an X-ray structure analysis. 4c crystallizes monoclinically in space group P21/c with a = 10.232(3), b = 10.216(1), c = 29.047(7)Å, α = γ = 90.0°, β = 97.76(3)°, Ζ = 4, and R = Rw = 0.0378 for 4026 observed reflections. The new complexes are sensitive to oxygen and moisture and soluble in all common organic solvents.