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Synthesis and Crystal Structure of 5-Bromoisophthalic Acid
Corresponding Author(s) : R. Zhang
Asian Journal of Chemistry,
Vol. 27 No. 8 (2015): Vol 27 Issue 8
Abstract
A new compound viz., 5-bromoisophthalic acid with the molecular formula C8H7BrO5 has been successfully synthesized by the reaction of isophthalic acid and N-bromosuccinimide (NBS). The compound has been characterized by X-ray single-crystal diffraction and shows a one-dimensional framework. The 3D supramolecular structure is formed via hydrogen bonding connection.
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- A. Kleemann and J. Engel, Pharmaceutical Substances, Thieme, New York, edn 4, p. 488 (2001).
- D. Lednicer and L.A. Mitscher, The Organic Chemistry of Drug Synthesis, John Wiley & Sons, New York, Vol. 2, p. 331 (1980).
- (a) A. Kleemann and J. Engel, Pharmaceutical Substances, Thieme, New York, edn 4, p. 269 (2001); (b) D. Lednicer and L.A. Mitscher, The Organic Chemistry of Drug Synthesis, John Wiley & Sons, New York, Vol. 2, p. 210 (1980).
- (a) A. Kleemann and J. Engel, Pharmaceutical Substances, Thieme, New York, edn 2, p. 2085 (2001); (b) D. Lednicer and L.A. Mitscher, The Organic Chemistry of Drug Synthesis, John Wiley & Sons, New York, Vol. 2, p. 17 (1980).
- G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).
References
A. Kleemann and J. Engel, Pharmaceutical Substances, Thieme, New York, edn 4, p. 488 (2001).
D. Lednicer and L.A. Mitscher, The Organic Chemistry of Drug Synthesis, John Wiley & Sons, New York, Vol. 2, p. 331 (1980).
(a) A. Kleemann and J. Engel, Pharmaceutical Substances, Thieme, New York, edn 4, p. 269 (2001); (b) D. Lednicer and L.A. Mitscher, The Organic Chemistry of Drug Synthesis, John Wiley & Sons, New York, Vol. 2, p. 210 (1980).
(a) A. Kleemann and J. Engel, Pharmaceutical Substances, Thieme, New York, edn 2, p. 2085 (2001); (b) D. Lednicer and L.A. Mitscher, The Organic Chemistry of Drug Synthesis, John Wiley & Sons, New York, Vol. 2, p. 17 (1980).
G.M. Sheldrick, SHELXTL97, Program for the Refinement of Crystal Structure, University of Gottingen, Germany (1997).