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Comparative Characteristics of Xerogels Based on Zirconium Dioxide Obtained by the Method of Joint Deposition of Hydroxides in a Volume and a Microreactor with Counter Swirled Flows

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Abstract

Methods of coprecipitation of hydroxides in the bulk and in a microreactor with counterswirling flows are used to obtain mesoporous nanodispersed xerogels based on zirconium dioxide. The features of the morphology and state of the surface of the obtained xerogels are studied. It is shown that the investigated method of obtaining nanosized xerogels based on zirconium dioxide in counterswirling flows makes it possible to reduce the degree of particle agglomeration.

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ACKNOWLEDGMENTS

The authors thank A.S. Kovalenko for his help in studying the colloidal properties of materials.

Funding

This study was carried out as part of a state assignment of the Institute of Chemistry of the Russian Academy of Sciences with the support of the Ministry of Education and Science of the Russian Federation (topic no. АААА-А19-119022290091-8).

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Authors and Affiliations

  1. Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences, 199034, St. Petersburg, Russia

    N. Yu. Fedorenko, Yu. S. Kudryashova, O. A. Shilova, M. V. Kalinina, A. V. Zdravkov & R. Sh. Abiev

  2. St. Petersburg State Technological Institute (Technical University), 190013, St. Petersburg, Russia

    S. V. Myakin, O. A. Shilova & R. Sh. Abiev

  3. Institute for Analytical Instrumentation, Russian Academy of Sciences, 198095, St. Petersburg, Russia

    S. V. Myakin

  4. St. Petersburg State Electrotechnical University “LETI,”, 197376, St. Petersburg, Russia

    O. A. Shilova

Authors
  1. N. Yu. Fedorenko
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  2. Yu. S. Kudryashova
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  3. S. V. Myakin
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  4. O. A. Shilova
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  5. M. V. Kalinina
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  6. A. V. Zdravkov
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  7. R. Sh. Abiev
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Correspondence to N. Yu. Fedorenko.

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Fedorenko, N.Y., Kudryashova, Y.S., Myakin, S.V. et al. Comparative Characteristics of Xerogels Based on Zirconium Dioxide Obtained by the Method of Joint Deposition of Hydroxides in a Volume and a Microreactor with Counter Swirled Flows. Glass Phys Chem 47, 653–656 (2021). https://doi.org/10.1134/S1087659621060080

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  • DOI: https://doi.org/10.1134/S1087659621060080

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