Abstract
Nanocrystalline bismuth orthoferrite (BiFeO3) was prepared by soft chemistry. The hydroxide coprecipitation method was shown to influence the formation of nanocrystalline bismuth orthoferrite. Synthetic conditions were determined to prepare nanocrystalline BiFeO3 free of other phases of the Bi2O3–Fe2O3 system with a narrow crystallite-size distribution and the smallest crystallite size of about 6–7 nm.
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ACKNOWLEDGMENTS
X-ray diffraction experiments, scanning electron microscopy, and elemental analysis of the samples were performed on facilities of the Engineering Center of the St. Petersburg State Technological Institute (Technical University).
The transmission electron microscopic studies were carried out using the facilities of the Federal Center for Collective Use “Materials Science and Diagnostics in Advanced Technologies” in the Ioffe Physico-Technical Institute.
Funding
The work was supported by the Russian Scientific Foundation (project no. 16-13-10252).
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Translated by O. Fedorova
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Proskurina, O.V., Sokolova, A.N., Sirotkin, A.A. et al. Role of Hydroxide Precipitation Conditions in the Formation of Nanocrystalline BiFeO3 . Russ. J. Inorg. Chem. 66, 163–169 (2021). https://doi.org/10.1134/S0036023621020157
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DOI: https://doi.org/10.1134/S0036023621020157