Issue 7, 2023

Post-synthesis of Sn-beta zeolite by aerosol method

Abstract

Sn-beta zeolite is a Lewis acid catalyst which can activate the C–O and C[double bond, length as m-dash]O bonds of many organic compounds. In this paper, a simple aerosol method has been firstly applied to the post-synthesis of Sn-beta zeolite. The aqueous solution containing SnCl2 and dealuminated beta zeolite was rapidly dried using an aerosol generator to obtain the Sn-beta zeolites with different Sn contents. The physicochemical properties of the Sn-beta zeolites were further characterized by XRD, nitrogen adsorption–desorption, FT-IR and Py-FT-IR techniques. The catalysts exhibited good catalytic performances in the Baeyer–Villiger oxidation reaction of cyclohexanone.

Graphical abstract: Post-synthesis of Sn-beta zeolite by aerosol method

Supplementary files

Article information

Article type
Paper
Submitted
10 Oct 2022
Accepted
05 Jan 2023
First published
07 Feb 2023
This article is Open Access
Creative Commons BY license

RSC Adv., 2023,13, 4835-4842

Post-synthesis of Sn-beta zeolite by aerosol method

G. Xiong, H. Yang, L. Liu and J. Liu, RSC Adv., 2023, 13, 4835 DOI: 10.1039/D2RA06366B

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