Skip to main content
Log in

A comparative study of the mechanical characteristics of additively and conventionally fabricated 17-4 precipitation hardened stainless steel

  • Full Research Article
  • Published:
Progress in Additive Manufacturing Aims and scope Submit manuscript

Abstract

Precipitation hardened stainless steel, like 17-4PH SS, had received significant interest in various industries due to its high strength and corrosion resistance properties. This material may be produced with either traditional or modern manufacturing techniques. However, each carries its benefits and challenges. In this study, 17-4 PH parts produced by laser powder bed fusion (L-PBF) and traditional manufacturing (wrought) techniques are characterized by different method like a tensile test, microhardness, and nanoindentation. The primary aim of this research is to examine the impact of heat treatment on the properties of 17-4PH, comparing specimens manufactured through L-PBF and conventional manufacturing methods. The investigation seeks to determine whether the heat treatment induces similar magnitude changes in both sets of parts, with an emphasis on utilizing a diverse range of characterization techniques for comprehensive analysis. Solution annealing followed by an aging process was employed to investigate post-heat treatment’s impact on the performance of 17–4 PH SS parts in both manufactured parts. Results showed that modulus and hardness of L-PBF additive manufacturing parts were lower than those of conventionally manufactured counterparts. Solution annealing and aging increased these properties significantly in both cases; however, both ductility and ultimate strength of 17-4 PH stainless steel parts produced via the additive manufacturing are still inferior compared to their wrought parts.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14
Fig. 15
Fig. 16
Fig. 17
Fig. 18

Similar content being viewed by others

Data availability

Data supporting the findings of this study are available upon request.

References

  1. Huang Y, Leu MC, Mazumder J, Donmez A (2015) Additive manufacturing: current state, future potential, gaps and needs, and recommendations. J Manuf Sci Eng 137:014001. https://doi.org/10.1115/1.4028725

    Article  Google Scholar 

  2. Wu M-W, Lai P-H, Chen J-K (2016) Anisotropy in the impact toughness of selective laser melted Ti–6Al–4V alloy. Mater Sci Eng A 650:295–299

    Article  Google Scholar 

  3. Frazier WE (2014) Metal additive manufacturing: a review. J Mater Eng Perform 23:1917–1928

    Article  Google Scholar 

  4. Du Plessis A, Yadroitsava I, Yadroitsev I (2020) Effects of defects on mechanical properties in metal additive manufacturing: a review focusing on X-ray tomography insights. Mater Des 187:108385

    Article  Google Scholar 

  5. Sames WJ, List FA, Pannala S, Dehoff RR, Babu SS (2016) The metallurgy and processing science of metal additive manufacturing. Int Mater Rev 61:315–360. https://doi.org/10.1080/09506608.2015.1116649

    Article  Google Scholar 

  6. Yeli G, Auger MA, Wilford K, Smith GDW, Bagot PAJ, Moody MP (2017) Sequential nucleation of phases in a 17-4PH steel: Microstructural characterisation and mechanical properties. Acta Mater 125:38–49. https://doi.org/10.1016/j.actamat.2016.11.052

    Article  Google Scholar 

  7. Munther M, Palma T, Tavangarian F, Beheshti A, Davami K (2020) Nanomechanical properties of additively and traditionally manufactured nickel-chromium-based superalloys through instrumented nanoindentation. Manuf Lett 23:39–43. https://doi.org/10.1016/j.mfglet.2019.09.003

    Article  Google Scholar 

  8. Carter LN, Martin C, Withers PJ, Attallah MM (2014) The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy. J Alloys Compd 615:338–347. https://doi.org/10.1016/j.jallcom.2014.06.172

    Article  Google Scholar 

  9. Parry L, Ashcroft IA, Wildman RD (2016) Understanding the effect of laser scan strategy on residual stress in selective laser melting through thermo-mechanical simulation. Addit Manuf 12:1–15. https://doi.org/10.1016/j.addma.2016.05.014

    Article  Google Scholar 

  10. Yusuf SM, Gao N (2017) Influence of energy density on metallurgy and properties in metal additive manufacturing. Mater Sci Technol 33:1269–1289. https://doi.org/10.1080/02670836.2017.1289444

    Article  Google Scholar 

  11. Cherry JA, Davies HM, Mehmood S, Lavery NP, Brown SGR, Sienz J (2015) Investigation into the effect of process parameters on microstructural and physical properties of 316L stainless steel parts by selective laser melting. Int J Adv Manuf Technol 76:869–879. https://doi.org/10.1007/s00170-014-6297-2

    Article  Google Scholar 

  12. Burkhardt C, Wendler M, Lehnert R, Hauser M, Clausnitzer P, Volkova O, Biermann H, Weidner A (2023) Fine-grained microstructure without texture obtained by electron beam powder bed fusion for AISI 304 L-based stainless steel. Addit Manuf 69:103539. https://doi.org/10.1016/j.addma.2023.103539

    Article  Google Scholar 

  13. Gu D, Shen Y (2009) Balling phenomena in direct laser sintering of stainless steel powder: metallurgical mechanisms and control methods. Mater Des 30:2903–2910. https://doi.org/10.1016/j.matdes.2009.01.013

    Article  Google Scholar 

  14. Thijs L, Sistiaga MLM, Wauthle R, Xie Q, Kruth J-P, Van Humbeeck J (2013) Strong morphological and crystallographic texture and resulting yield strength anisotropy in selective laser melted tantalum. Acta Mater 61(12):4657–4668. https://doi.org/10.1016/j.actamat.2013.04.036

    Article  Google Scholar 

  15. Dadbakhsh S, Vrancken B, Kruth J-P, Luyten J, Van Humbeeck J (2016) Texture and anisotropy in selective laser melting of NiTi alloy. Mater Sci Eng A 650:225–232. https://doi.org/10.1016/j.msea.2015.10.032

    Article  Google Scholar 

  16. Sercombe T, Jones N, Day R, Kop A (2008) Heat treatment of Ti-6Al-7Nb components produced by selective laser melting. Rapid Prototyp J 14:300–304. https://doi.org/10.1108/13552540810907974

    Article  Google Scholar 

  17. Salari S, Rahman MS, Polycarpou AA, Beheshti A (2020) Elevated temperature mechanical properties of Inconel 617 surface oxide using nanoindentation. Mater Sci Eng A 788:139539. https://doi.org/10.1016/j.msea.2020.139539

    Article  Google Scholar 

  18. Jägle EA, Choi P-P, Van Humbeeck J, Raabe D (2014) Precipitation and austenite reversion behavior of a maraging steel produced by selective laser melting. J Mater Res 29:2072–2079. https://doi.org/10.1557/jmr.2014.204

    Article  Google Scholar 

  19. Huber D, Stich P, Fischer A (2022) Heat treatment of 17-4 PH stainless steel produced by binder jet additive manufacturing (BJAM) from N2-atomized powder. Prog Addit Manuf 7:187–199. https://doi.org/10.1007/s40964-021-00224-z

    Article  Google Scholar 

  20. Hamlin RJ, DuPont JN (2017) Microstructural evolution and mechanical properties of simulated heat-affected zones in cast precipitation-hardened stainless steels 17-4 and 13–8+ Mo. Metall Mater Trans A 48:246–264

    Article  Google Scholar 

  21. Rafi HK, Pal D, Patil N, Starr TL, Stucker BE (2014) Microstructure and mechanical behavior of 17-4 precipitation hardenable steel processed by selective laser melting. J Mater Eng Perform 23:4421–4428. https://doi.org/10.1007/s11665-014-1226-y

    Article  Google Scholar 

  22. Casati R, Lemke J, Tuissi A, Vedani M (2016) Aging behaviour and mechanical performance of 18-Ni 300 steel processed by selective laser melting. Metals 6:218. https://doi.org/10.3390/met6090218

    Article  Google Scholar 

  23. Wang X, Chou YK (2015) A method to estimate residual stress in metal parts made by selective laser melting, ASME Int. Mech Eng Congr Expo Proc 2A–2015:1–8. https://doi.org/10.1115/IMECE2015-52386

    Article  Google Scholar 

  24. Abbas TF, Othman FM, Basil Ali H, Effect of infill Parameter on compression property in FDM Process. Int J Eng Res Appl 2017; 7: 16–19. https://doi.org/10.9790/9622-0710021619.

  25. Murr LE, Martinez E, Hernandez J, Collins S, Amato KN, Gaytan SM, Shindo PW (2012) Microstructures and properties of 17-4 PH stainless steel fabricated by selective laser melting. J Mater Res Technol 1:167–177

    Article  Google Scholar 

  26. Mutua J, Nakata S, Onda T, Chen Z-C (2018) Optimization of selective laser melting parameters and influence of post heat treatment on microstructure and mechanical properties of maraging steel. Mater Des 139:486–497. https://doi.org/10.1016/j.matdes.2017.11.042

    Article  Google Scholar 

  27. Yadollahi A, Shamsaei N, Thompson SM, Elwany A, Bian L (2017) Effects of building orientation and heat treatment on fatigue behavior of selective laser melted 17-4 PH stainless steel. Int J Fatigue 94:218–235

    Article  Google Scholar 

  28. Roberts D, Zhang Y, Charit I, Zhang J (2018) A comparative study of microstructure and high-temperature mechanical properties of 15–5 PH stainless steel processed via additive manufacturing and traditional manufacturing. Prog Addit Manuf 3:183–190. https://doi.org/10.1007/s40964-018-0051-5

    Article  Google Scholar 

  29. LeBrun T, Nakamoto T, Horikawa K, Kobayashi H (2015) Effect of retained austenite on subsequent thermal processing and resultant mechanical properties of selective laser melted 17-4 PH stainless steel. Mater Des 81:44–53. https://doi.org/10.1016/j.matdes.2015.05.026

    Article  Google Scholar 

  30. Kudzal A, McWilliams B, Hofmeister C, Kellogg F, Yu J, Taggart-Scarff J, Liang J (2017) Effect of scan pattern on the microstructure and mechanical properties of Powder Bed Fusion additive manufactured 17-4 stainless steel. Mater Des 133:205–215. https://doi.org/10.1016/j.matdes.2017.07.047

    Article  Google Scholar 

  31. Sun Y, Hebert RJ, Aindow M (2018) Effect of heat treatments on microstructural evolution of additively manufactured and wrought 17-4PH stainless steel. Mater Des 156:429–440. https://doi.org/10.1016/j.matdes.2018.07.015

    Article  Google Scholar 

  32. Cheruvathur S, Lass EA, Campbell CE (2016) Additive manufacturing of 17-4 PH stainless steel: post-processing heat treatment to achieve uniform reproducible microstructure. JOM 68:930–942. https://doi.org/10.1007/s11837-015-1754-4

    Article  Google Scholar 

  33. Bai Y, Yang Y, Wang D, Zhang M (2017) Influence mechanism of parameters process and mechanical properties evolution mechanism of maraging steel 300 by selective laser melting. Mater Sci Eng A 703:116–123. https://doi.org/10.1016/j.msea.2017.06.033

    Article  Google Scholar 

  34. Gong X, Lydon J, Cooper K, Chou K. Microstructural analysis and nanoindentation characterization of Ti-6Al-4V parts from electron beam additive manufacturing, in: Vol. 2A Adv. Manuf., American Society of Mechanical Engineers, 2014: pp. 1–8. https://doi.org/10.1115/IMECE2014-36675.

  35. Tillmann W, Dias NFL, Stangier D, Schaak C, Höges S (2022) Heat treatment of binder jet printed 17-4 PH stainless steel for subsequent deposition of tribo-functional diamond-like carbon coatings. Mater Des 213:110304

    Article  Google Scholar 

  36. Sabooni S, Chabok A, Feng SC, Blaauw H, Pijper TC, Yang HJ, Pei YT (2021) Laser powder bed fusion of 17-4 PH stainless steel: a comparative study on the effect of heat treatment on the microstructure evolution and mechanical properties. Addit Manuf 46:102176

    Google Scholar 

  37. Henry TC, Morales MA, Cole DP, Shumeyko CM, Riddick JC (2021) Mechanical behavior of 17-4 PH stainless steel processed by atomic diffusion additive manufacturing. Int J Adv Manuf Technol 114:2103–2114

    Article  Google Scholar 

  38. Khadka S, Bilan HK, Ma T, Yuya PA (2023) Laves phase and equiaxed grains formation in directed energy deposited AlCuFeNiTi high entropy alloy. J Alloys Compd 961:171089. https://doi.org/10.1016/j.jallcom.2023.171089

    Article  Google Scholar 

  39. Guennouni N, Barroux A, Grosjean C, Maisonnette D, Nivet E, Andrieu E, Poquillon D, Laffont L, Blanc C (2021) Comparative study of the microstructure between a laser beam melted 17-4PH stainless steel and its conventional counterpart. Mater Sci Eng A 823:141718

    Article  Google Scholar 

  40. Sanjeev KC, Nezhadfar PD, Phillips C, Kennedy MS, Shamsaei N, Jackson RL (2019) Tribological behavior of 17-4 PH stainless steel fabricated by traditional manufacturing and laser-based additive manufacturing methods. Wear 440:203100

    Google Scholar 

  41. T. Strasser, Comparison of Additively Manufactured and Wrought 17–4 PH Stainless Steels in Ultra Low Cycle Fatigue, University of Arkansas, 2020.

  42. EOS, EOS StainlessSteel 17-4PH, 2017.

  43. Conde FF, Escobar JD, Oliveira JP, Béreš M, Jardini AL, Bose WW, Avila JA (2019) Effect of thermal cycling and aging stages on the microstructure and bending strength of a selective laser melted 300-grade maraging steel. Mater Sci Eng A 758:192–201. https://doi.org/10.1016/j.msea.2019.03.129

    Article  Google Scholar 

  44. Monkova K, Zetkova I, Kučerová L, Zetek M, Monka P, Daňa M (2019) Study of 3D printing direction and effects of heat treatment on mechanical properties of MS1 maraging steel. Arch Appl Mech 89:791–804. https://doi.org/10.1007/s00419-018-1389-3

    Article  Google Scholar 

  45. Lin X, Cao Y, Wu X, Yang H, Chen J, Huang W (2012) Microstructure and mechanical properties of laser forming repaired 17-4PH stainless steel. Mater Sci Eng A 553:80–88

    Article  Google Scholar 

  46. Tan C, Zhou K, Ma W, Zhang P, Liu M, Kuang T (2017) Microstructural evolution, nanoprecipitation behavior and mechanical properties of selective laser melted high-performance grade 300 maraging steel. Mater Des 134:23–34. https://doi.org/10.1016/j.matdes.2017.08.026

    Article  Google Scholar 

  47. Nezhadfar PD, Gradl PR, Shao S, Shamsaei N (2022) Microstructure and deformation behavior of additively manufactured 17-4 stainless steel: laser powder bed fusion vs laser powder directed energy deposition. JOM 74:1136–1148. https://doi.org/10.1007/s11837-021-05032-y

    Article  Google Scholar 

  48. Biswas N, Ding JL, Balla VK, Field DP, Bandyopadhyay A (2012) Deformation and fracture behavior of laser processed dense and porous Ti6Al4V alloy under static and dynamic loading. Mater Sci Eng A 549:213–221. https://doi.org/10.1016/j.msea.2012.04.036

    Article  Google Scholar 

  49. Wei K, Gao M, Wang Z, Zeng X (2014) Effect of energy input on formability, microstructure and mechanical properties of selective laser melted AZ91D magnesium alloy. Mater Sci Eng A 611:212–222. https://doi.org/10.1016/j.msea.2014.05.092

    Article  Google Scholar 

  50. Zai L, Zhang C, Wang Y, Guo W, Wellmann D, Tong X, Tian Y (2020) Laser powder bed fusion of precipitation-hardened martensitic stainless steels: a review. Metals 10(2):255. https://doi.org/10.3390/met10020255

    Article  Google Scholar 

  51. Garcia-Cabezon C, Castro-Sastre MA, Fernandez-Abia AI, Rodriguez-Mendez ML, Martin-Pedrosa F (2022) Microstructure–Hardness–Corrosion performance of 17-4 precipitation hardening stainless steels processed by selective laser melting in comparison with commercial alloy. Met Mater Int 28:2652–2667. https://doi.org/10.1007/s12540-021-01155-8

    Article  Google Scholar 

  52. Garcia-Cabezon C, Hernández CG, Castro-Sastre MA, Fernandez-Abia AI, Rodriguez-Mendez ML, Martin-Pedrosa F (2023) Heat treatments of 17-4 PH SS processed by SLM to improve its strength and biocompatibility in biomedical applications. J Mater Res Technol 26:3524–3543. https://doi.org/10.1016/j.jmrt.2023.08.104

    Article  Google Scholar 

  53. Wu J, Wray PJ, Garcia CI, Hua M, Deardo AJ (2005) Image quality analysis: A new method of characterizing microstructures. ISIJ Int 45:254–262. https://doi.org/10.2355/isijinternational.45.254

    Article  Google Scholar 

  54. Viswanathan UK, Nayar PKK, Krishnan R (1989) Kinetics of precipitation in 17-4 PH stainless steel. Mater Sci Technol 5:346–349. https://doi.org/10.1179/mst.1989.5.4.346

    Article  Google Scholar 

  55. Mirzadeh H, Najafizadeh A (2009) Aging kinetics of 17-4 PH stainless steel. Mater Chem Phys 116:119–124. https://doi.org/10.1016/j.matchemphys.2009.02.049

    Article  Google Scholar 

  56. ASTM International, Standard Test Methods for Density of Compacted or Sintered Powder Metallurgy (PM) Products Using Archimedes’ Principle, Astm B962–13. i (2013) 1–7. https://doi.org/10.1520/B0962-17.2.

  57. Lim YY, Chaudhri MM (2002) The influence of grain size on the indentation hardness of high-purity copper and aluminium. Philos Mag A 82:2071–2080. https://doi.org/10.1080/01418610208235717

    Article  Google Scholar 

  58. Li W, Vittorietti M, Jongbloed G, Sietsma J (2020) The combined influence of grain size distribution and dislocation density on hardness of interstitial free steel. J Mater Sci Technol 45:35–43. https://doi.org/10.1016/j.jmst.2019.11.025

    Article  Google Scholar 

  59. Guo D, Kwok CT, Tam LM, Zhang D, Li X (2020) Hardness, microstructure and texture of friction surfaced 17-4PH precipitation hardening stainless steel coatings with and without subsequent aging. Surf Coatings Technol 402:126302

    Article  Google Scholar 

  60. Akbari Mousavi SAA, Hoseini Hosein Abad SA (2011) Effects of post weld ageing heat treatments on the microstructure of 17-4PH GTA welded joints. Adv Mater Res 264–265:1300–1305. https://doi.org/10.4028/www.scientific.net/AMR.264-265.1300

    Article  Google Scholar 

  61. Triwiyanto A, Hussain P, Ismail MC (2013) Microstructure and nanoindentation characterization of low temperature hybrid treated layer on austenitic stainless steel. IOP Conf Ser Mater Sci Eng 46:012043. https://doi.org/10.1088/1757-899X/46/1/012043

    Article  Google Scholar 

  62. Leyland A, Matthews A (2000) On the significance of the H/E ratio in wear control: a nanocomposite coating approach to optimised tribological behaviour. Wear 246:1–11. https://doi.org/10.1016/S0043-1648(00)00488-9

    Article  Google Scholar 

  63. Long X, Hu B, Feng Y, Chang C, Li M (2019) Correlation of microstructure and constitutive behaviour of sintered silver particles via nanoindentation. Int J Mech Sci 161–162:105020. https://doi.org/10.1016/j.ijmecsci.2019.105020

    Article  Google Scholar 

  64. Tanure L, Bakaeva A, Dubinko A, Terentyev D, Verbeken K (2019) Effect of annealing on microstructure, texture and hardness of ITER-specification tungsten analyzed by EBSD, vickers micro-hardness and nano-indentation techniques. J Nucl Mater 524:191–199. https://doi.org/10.1016/j.jnucmat.2019.07.005

    Article  Google Scholar 

  65. Sutton AP (2020) Stress. In: Sutton AP (ed) Physics of Elasticity and Crystal Defects. Oxford University Press, Oxford, pp 9–28. https://doi.org/10.1093/oso/9780198860785.003.0002

    Chapter  Google Scholar 

Download references

Acknowledgements

This research was supported by the SBI Faculty Summer Research Award at the School of Business and Industry, Jacksonville State University. We are grateful to Dr. Dana Ingalsbe for making the ORLAS Creator machine available to us. We would also like to thank Mrs. Natalia Esparragoza and Mr. Matt Rosser for their help in printing the tensile test specimens. Mr. Hisham Abusalma’s assistance with the tensile testing was invaluable, and we are also grateful to Mr. M. Sepahi for the heat treatment.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Hamid Eisazadeh.

Ethics declarations

Conflict of interest

On behalf of all authors, the corresponding author states that there is no conflict of interest.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Eisazadeh, H., Khadka, S., Wang, X. et al. A comparative study of the mechanical characteristics of additively and conventionally fabricated 17-4 precipitation hardened stainless steel. Prog Addit Manuf (2024). https://doi.org/10.1007/s40964-024-00591-3

Download citation

  • Received:

  • Accepted:

  • Published:

  • DOI: https://doi.org/10.1007/s40964-024-00591-3

Keywords

Navigation