Abstract
Precipitation hardened stainless steel, like 17-4PH SS, had received significant interest in various industries due to its high strength and corrosion resistance properties. This material may be produced with either traditional or modern manufacturing techniques. However, each carries its benefits and challenges. In this study, 17-4 PH parts produced by laser powder bed fusion (L-PBF) and traditional manufacturing (wrought) techniques are characterized by different method like a tensile test, microhardness, and nanoindentation. The primary aim of this research is to examine the impact of heat treatment on the properties of 17-4PH, comparing specimens manufactured through L-PBF and conventional manufacturing methods. The investigation seeks to determine whether the heat treatment induces similar magnitude changes in both sets of parts, with an emphasis on utilizing a diverse range of characterization techniques for comprehensive analysis. Solution annealing followed by an aging process was employed to investigate post-heat treatment’s impact on the performance of 17–4 PH SS parts in both manufactured parts. Results showed that modulus and hardness of L-PBF additive manufacturing parts were lower than those of conventionally manufactured counterparts. Solution annealing and aging increased these properties significantly in both cases; however, both ductility and ultimate strength of 17-4 PH stainless steel parts produced via the additive manufacturing are still inferior compared to their wrought parts.
Similar content being viewed by others
Data availability
Data supporting the findings of this study are available upon request.
References
Huang Y, Leu MC, Mazumder J, Donmez A (2015) Additive manufacturing: current state, future potential, gaps and needs, and recommendations. J Manuf Sci Eng 137:014001. https://doi.org/10.1115/1.4028725
Wu M-W, Lai P-H, Chen J-K (2016) Anisotropy in the impact toughness of selective laser melted Ti–6Al–4V alloy. Mater Sci Eng A 650:295–299
Frazier WE (2014) Metal additive manufacturing: a review. J Mater Eng Perform 23:1917–1928
Du Plessis A, Yadroitsava I, Yadroitsev I (2020) Effects of defects on mechanical properties in metal additive manufacturing: a review focusing on X-ray tomography insights. Mater Des 187:108385
Sames WJ, List FA, Pannala S, Dehoff RR, Babu SS (2016) The metallurgy and processing science of metal additive manufacturing. Int Mater Rev 61:315–360. https://doi.org/10.1080/09506608.2015.1116649
Yeli G, Auger MA, Wilford K, Smith GDW, Bagot PAJ, Moody MP (2017) Sequential nucleation of phases in a 17-4PH steel: Microstructural characterisation and mechanical properties. Acta Mater 125:38–49. https://doi.org/10.1016/j.actamat.2016.11.052
Munther M, Palma T, Tavangarian F, Beheshti A, Davami K (2020) Nanomechanical properties of additively and traditionally manufactured nickel-chromium-based superalloys through instrumented nanoindentation. Manuf Lett 23:39–43. https://doi.org/10.1016/j.mfglet.2019.09.003
Carter LN, Martin C, Withers PJ, Attallah MM (2014) The influence of the laser scan strategy on grain structure and cracking behaviour in SLM powder-bed fabricated nickel superalloy. J Alloys Compd 615:338–347. https://doi.org/10.1016/j.jallcom.2014.06.172
Parry L, Ashcroft IA, Wildman RD (2016) Understanding the effect of laser scan strategy on residual stress in selective laser melting through thermo-mechanical simulation. Addit Manuf 12:1–15. https://doi.org/10.1016/j.addma.2016.05.014
Yusuf SM, Gao N (2017) Influence of energy density on metallurgy and properties in metal additive manufacturing. Mater Sci Technol 33:1269–1289. https://doi.org/10.1080/02670836.2017.1289444
Cherry JA, Davies HM, Mehmood S, Lavery NP, Brown SGR, Sienz J (2015) Investigation into the effect of process parameters on microstructural and physical properties of 316L stainless steel parts by selective laser melting. Int J Adv Manuf Technol 76:869–879. https://doi.org/10.1007/s00170-014-6297-2
Burkhardt C, Wendler M, Lehnert R, Hauser M, Clausnitzer P, Volkova O, Biermann H, Weidner A (2023) Fine-grained microstructure without texture obtained by electron beam powder bed fusion for AISI 304 L-based stainless steel. Addit Manuf 69:103539. https://doi.org/10.1016/j.addma.2023.103539
Gu D, Shen Y (2009) Balling phenomena in direct laser sintering of stainless steel powder: metallurgical mechanisms and control methods. Mater Des 30:2903–2910. https://doi.org/10.1016/j.matdes.2009.01.013
Thijs L, Sistiaga MLM, Wauthle R, Xie Q, Kruth J-P, Van Humbeeck J (2013) Strong morphological and crystallographic texture and resulting yield strength anisotropy in selective laser melted tantalum. Acta Mater 61(12):4657–4668. https://doi.org/10.1016/j.actamat.2013.04.036
Dadbakhsh S, Vrancken B, Kruth J-P, Luyten J, Van Humbeeck J (2016) Texture and anisotropy in selective laser melting of NiTi alloy. Mater Sci Eng A 650:225–232. https://doi.org/10.1016/j.msea.2015.10.032
Sercombe T, Jones N, Day R, Kop A (2008) Heat treatment of Ti-6Al-7Nb components produced by selective laser melting. Rapid Prototyp J 14:300–304. https://doi.org/10.1108/13552540810907974
Salari S, Rahman MS, Polycarpou AA, Beheshti A (2020) Elevated temperature mechanical properties of Inconel 617 surface oxide using nanoindentation. Mater Sci Eng A 788:139539. https://doi.org/10.1016/j.msea.2020.139539
Jägle EA, Choi P-P, Van Humbeeck J, Raabe D (2014) Precipitation and austenite reversion behavior of a maraging steel produced by selective laser melting. J Mater Res 29:2072–2079. https://doi.org/10.1557/jmr.2014.204
Huber D, Stich P, Fischer A (2022) Heat treatment of 17-4 PH stainless steel produced by binder jet additive manufacturing (BJAM) from N2-atomized powder. Prog Addit Manuf 7:187–199. https://doi.org/10.1007/s40964-021-00224-z
Hamlin RJ, DuPont JN (2017) Microstructural evolution and mechanical properties of simulated heat-affected zones in cast precipitation-hardened stainless steels 17-4 and 13–8+ Mo. Metall Mater Trans A 48:246–264
Rafi HK, Pal D, Patil N, Starr TL, Stucker BE (2014) Microstructure and mechanical behavior of 17-4 precipitation hardenable steel processed by selective laser melting. J Mater Eng Perform 23:4421–4428. https://doi.org/10.1007/s11665-014-1226-y
Casati R, Lemke J, Tuissi A, Vedani M (2016) Aging behaviour and mechanical performance of 18-Ni 300 steel processed by selective laser melting. Metals 6:218. https://doi.org/10.3390/met6090218
Wang X, Chou YK (2015) A method to estimate residual stress in metal parts made by selective laser melting, ASME Int. Mech Eng Congr Expo Proc 2A–2015:1–8. https://doi.org/10.1115/IMECE2015-52386
Abbas TF, Othman FM, Basil Ali H, Effect of infill Parameter on compression property in FDM Process. Int J Eng Res Appl 2017; 7: 16–19. https://doi.org/10.9790/9622-0710021619.
Murr LE, Martinez E, Hernandez J, Collins S, Amato KN, Gaytan SM, Shindo PW (2012) Microstructures and properties of 17-4 PH stainless steel fabricated by selective laser melting. J Mater Res Technol 1:167–177
Mutua J, Nakata S, Onda T, Chen Z-C (2018) Optimization of selective laser melting parameters and influence of post heat treatment on microstructure and mechanical properties of maraging steel. Mater Des 139:486–497. https://doi.org/10.1016/j.matdes.2017.11.042
Yadollahi A, Shamsaei N, Thompson SM, Elwany A, Bian L (2017) Effects of building orientation and heat treatment on fatigue behavior of selective laser melted 17-4 PH stainless steel. Int J Fatigue 94:218–235
Roberts D, Zhang Y, Charit I, Zhang J (2018) A comparative study of microstructure and high-temperature mechanical properties of 15–5 PH stainless steel processed via additive manufacturing and traditional manufacturing. Prog Addit Manuf 3:183–190. https://doi.org/10.1007/s40964-018-0051-5
LeBrun T, Nakamoto T, Horikawa K, Kobayashi H (2015) Effect of retained austenite on subsequent thermal processing and resultant mechanical properties of selective laser melted 17-4 PH stainless steel. Mater Des 81:44–53. https://doi.org/10.1016/j.matdes.2015.05.026
Kudzal A, McWilliams B, Hofmeister C, Kellogg F, Yu J, Taggart-Scarff J, Liang J (2017) Effect of scan pattern on the microstructure and mechanical properties of Powder Bed Fusion additive manufactured 17-4 stainless steel. Mater Des 133:205–215. https://doi.org/10.1016/j.matdes.2017.07.047
Sun Y, Hebert RJ, Aindow M (2018) Effect of heat treatments on microstructural evolution of additively manufactured and wrought 17-4PH stainless steel. Mater Des 156:429–440. https://doi.org/10.1016/j.matdes.2018.07.015
Cheruvathur S, Lass EA, Campbell CE (2016) Additive manufacturing of 17-4 PH stainless steel: post-processing heat treatment to achieve uniform reproducible microstructure. JOM 68:930–942. https://doi.org/10.1007/s11837-015-1754-4
Bai Y, Yang Y, Wang D, Zhang M (2017) Influence mechanism of parameters process and mechanical properties evolution mechanism of maraging steel 300 by selective laser melting. Mater Sci Eng A 703:116–123. https://doi.org/10.1016/j.msea.2017.06.033
Gong X, Lydon J, Cooper K, Chou K. Microstructural analysis and nanoindentation characterization of Ti-6Al-4V parts from electron beam additive manufacturing, in: Vol. 2A Adv. Manuf., American Society of Mechanical Engineers, 2014: pp. 1–8. https://doi.org/10.1115/IMECE2014-36675.
Tillmann W, Dias NFL, Stangier D, Schaak C, Höges S (2022) Heat treatment of binder jet printed 17-4 PH stainless steel for subsequent deposition of tribo-functional diamond-like carbon coatings. Mater Des 213:110304
Sabooni S, Chabok A, Feng SC, Blaauw H, Pijper TC, Yang HJ, Pei YT (2021) Laser powder bed fusion of 17-4 PH stainless steel: a comparative study on the effect of heat treatment on the microstructure evolution and mechanical properties. Addit Manuf 46:102176
Henry TC, Morales MA, Cole DP, Shumeyko CM, Riddick JC (2021) Mechanical behavior of 17-4 PH stainless steel processed by atomic diffusion additive manufacturing. Int J Adv Manuf Technol 114:2103–2114
Khadka S, Bilan HK, Ma T, Yuya PA (2023) Laves phase and equiaxed grains formation in directed energy deposited AlCuFeNiTi high entropy alloy. J Alloys Compd 961:171089. https://doi.org/10.1016/j.jallcom.2023.171089
Guennouni N, Barroux A, Grosjean C, Maisonnette D, Nivet E, Andrieu E, Poquillon D, Laffont L, Blanc C (2021) Comparative study of the microstructure between a laser beam melted 17-4PH stainless steel and its conventional counterpart. Mater Sci Eng A 823:141718
Sanjeev KC, Nezhadfar PD, Phillips C, Kennedy MS, Shamsaei N, Jackson RL (2019) Tribological behavior of 17-4 PH stainless steel fabricated by traditional manufacturing and laser-based additive manufacturing methods. Wear 440:203100
T. Strasser, Comparison of Additively Manufactured and Wrought 17–4 PH Stainless Steels in Ultra Low Cycle Fatigue, University of Arkansas, 2020.
EOS, EOS StainlessSteel 17-4PH, 2017.
Conde FF, Escobar JD, Oliveira JP, Béreš M, Jardini AL, Bose WW, Avila JA (2019) Effect of thermal cycling and aging stages on the microstructure and bending strength of a selective laser melted 300-grade maraging steel. Mater Sci Eng A 758:192–201. https://doi.org/10.1016/j.msea.2019.03.129
Monkova K, Zetkova I, Kučerová L, Zetek M, Monka P, Daňa M (2019) Study of 3D printing direction and effects of heat treatment on mechanical properties of MS1 maraging steel. Arch Appl Mech 89:791–804. https://doi.org/10.1007/s00419-018-1389-3
Lin X, Cao Y, Wu X, Yang H, Chen J, Huang W (2012) Microstructure and mechanical properties of laser forming repaired 17-4PH stainless steel. Mater Sci Eng A 553:80–88
Tan C, Zhou K, Ma W, Zhang P, Liu M, Kuang T (2017) Microstructural evolution, nanoprecipitation behavior and mechanical properties of selective laser melted high-performance grade 300 maraging steel. Mater Des 134:23–34. https://doi.org/10.1016/j.matdes.2017.08.026
Nezhadfar PD, Gradl PR, Shao S, Shamsaei N (2022) Microstructure and deformation behavior of additively manufactured 17-4 stainless steel: laser powder bed fusion vs laser powder directed energy deposition. JOM 74:1136–1148. https://doi.org/10.1007/s11837-021-05032-y
Biswas N, Ding JL, Balla VK, Field DP, Bandyopadhyay A (2012) Deformation and fracture behavior of laser processed dense and porous Ti6Al4V alloy under static and dynamic loading. Mater Sci Eng A 549:213–221. https://doi.org/10.1016/j.msea.2012.04.036
Wei K, Gao M, Wang Z, Zeng X (2014) Effect of energy input on formability, microstructure and mechanical properties of selective laser melted AZ91D magnesium alloy. Mater Sci Eng A 611:212–222. https://doi.org/10.1016/j.msea.2014.05.092
Zai L, Zhang C, Wang Y, Guo W, Wellmann D, Tong X, Tian Y (2020) Laser powder bed fusion of precipitation-hardened martensitic stainless steels: a review. Metals 10(2):255. https://doi.org/10.3390/met10020255
Garcia-Cabezon C, Castro-Sastre MA, Fernandez-Abia AI, Rodriguez-Mendez ML, Martin-Pedrosa F (2022) Microstructure–Hardness–Corrosion performance of 17-4 precipitation hardening stainless steels processed by selective laser melting in comparison with commercial alloy. Met Mater Int 28:2652–2667. https://doi.org/10.1007/s12540-021-01155-8
Garcia-Cabezon C, Hernández CG, Castro-Sastre MA, Fernandez-Abia AI, Rodriguez-Mendez ML, Martin-Pedrosa F (2023) Heat treatments of 17-4 PH SS processed by SLM to improve its strength and biocompatibility in biomedical applications. J Mater Res Technol 26:3524–3543. https://doi.org/10.1016/j.jmrt.2023.08.104
Wu J, Wray PJ, Garcia CI, Hua M, Deardo AJ (2005) Image quality analysis: A new method of characterizing microstructures. ISIJ Int 45:254–262. https://doi.org/10.2355/isijinternational.45.254
Viswanathan UK, Nayar PKK, Krishnan R (1989) Kinetics of precipitation in 17-4 PH stainless steel. Mater Sci Technol 5:346–349. https://doi.org/10.1179/mst.1989.5.4.346
Mirzadeh H, Najafizadeh A (2009) Aging kinetics of 17-4 PH stainless steel. Mater Chem Phys 116:119–124. https://doi.org/10.1016/j.matchemphys.2009.02.049
ASTM International, Standard Test Methods for Density of Compacted or Sintered Powder Metallurgy (PM) Products Using Archimedes’ Principle, Astm B962–13. i (2013) 1–7. https://doi.org/10.1520/B0962-17.2.
Lim YY, Chaudhri MM (2002) The influence of grain size on the indentation hardness of high-purity copper and aluminium. Philos Mag A 82:2071–2080. https://doi.org/10.1080/01418610208235717
Li W, Vittorietti M, Jongbloed G, Sietsma J (2020) The combined influence of grain size distribution and dislocation density on hardness of interstitial free steel. J Mater Sci Technol 45:35–43. https://doi.org/10.1016/j.jmst.2019.11.025
Guo D, Kwok CT, Tam LM, Zhang D, Li X (2020) Hardness, microstructure and texture of friction surfaced 17-4PH precipitation hardening stainless steel coatings with and without subsequent aging. Surf Coatings Technol 402:126302
Akbari Mousavi SAA, Hoseini Hosein Abad SA (2011) Effects of post weld ageing heat treatments on the microstructure of 17-4PH GTA welded joints. Adv Mater Res 264–265:1300–1305. https://doi.org/10.4028/www.scientific.net/AMR.264-265.1300
Triwiyanto A, Hussain P, Ismail MC (2013) Microstructure and nanoindentation characterization of low temperature hybrid treated layer on austenitic stainless steel. IOP Conf Ser Mater Sci Eng 46:012043. https://doi.org/10.1088/1757-899X/46/1/012043
Leyland A, Matthews A (2000) On the significance of the H/E ratio in wear control: a nanocomposite coating approach to optimised tribological behaviour. Wear 246:1–11. https://doi.org/10.1016/S0043-1648(00)00488-9
Long X, Hu B, Feng Y, Chang C, Li M (2019) Correlation of microstructure and constitutive behaviour of sintered silver particles via nanoindentation. Int J Mech Sci 161–162:105020. https://doi.org/10.1016/j.ijmecsci.2019.105020
Tanure L, Bakaeva A, Dubinko A, Terentyev D, Verbeken K (2019) Effect of annealing on microstructure, texture and hardness of ITER-specification tungsten analyzed by EBSD, vickers micro-hardness and nano-indentation techniques. J Nucl Mater 524:191–199. https://doi.org/10.1016/j.jnucmat.2019.07.005
Sutton AP (2020) Stress. In: Sutton AP (ed) Physics of Elasticity and Crystal Defects. Oxford University Press, Oxford, pp 9–28. https://doi.org/10.1093/oso/9780198860785.003.0002
Acknowledgements
This research was supported by the SBI Faculty Summer Research Award at the School of Business and Industry, Jacksonville State University. We are grateful to Dr. Dana Ingalsbe for making the ORLAS Creator machine available to us. We would also like to thank Mrs. Natalia Esparragoza and Mr. Matt Rosser for their help in printing the tensile test specimens. Mr. Hisham Abusalma’s assistance with the tensile testing was invaluable, and we are also grateful to Mr. M. Sepahi for the heat treatment.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of interest
On behalf of all authors, the corresponding author states that there is no conflict of interest.
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.
About this article
Cite this article
Eisazadeh, H., Khadka, S., Wang, X. et al. A comparative study of the mechanical characteristics of additively and conventionally fabricated 17-4 precipitation hardened stainless steel. Prog Addit Manuf (2024). https://doi.org/10.1007/s40964-024-00591-3
Received:
Accepted:
Published:
DOI: https://doi.org/10.1007/s40964-024-00591-3