Abstract
Advanced characterization methods with nanoscale resolution are powerful tools in order to overcome the continuing challenges in the optimization of nitride semiconductor nanostructures for more efficient nanophotonic devices in the UV and green spectral range. This chapter is devoted to the study of optical, electronic, and structural properties of these nitride based nanostructures. In the first part, we discuss several state-of-the-art nanoscale characterization techniques including scanning transmission electron microscopy cathodoluminescence (STEM-CL), tip-enhanced Raman spectroscopy (TERS), micro-photoluminescence (µPL), X-ray diffraction (XRD), and scanning tunneling microscopy and spectroscopy (STM/STS). This selection of complementary microscopic and spectroscopic techniques provides unique insights into a multitude of nanostructure properties such as charge carrier excitation, relaxation, diffusion, and recombination dynamics, vibrational and structural properties including strain, segregation, as well as clustering, and surface and interface morphology. In the second part, we apply and combine these techniques to obtain detailed information on nanoscale properties of nitride based micro-columns, quantum wires, and heterostructures. The study of these nitride nanostructures provides not only insight into device limitations, but also contributes to the fundamental understanding of structural and optical properties of III-nitride nanostructures.
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Notes
- 1.
Until the completion of this publication.
- 2.
The sample was grown at CEA Grenoble at the Institut Nanosciences et Cryogénie in the group of Eva Monroy by Aparna Das.
- 3.
At 80 kV acceleration voltage and acceptance angle of 5 mrad.
- 4.
5000 trajectories were simulated with the Monte-Carlo simulation software CASINO v2.48. An incident electron probe of 0.56 nm in diameter was chosen.
- 5.
The presented HAADF measurements were performed by Florian Krause in the group of Prof. Andreas Rosenauer (University of Bremen).
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Acknowledgements
We gratefully acknowledge the German Research Foundation (DFG) for financial support within the Research Instrumentation Program INST 272/148-1, the Collaborative Research Center SFB 787 “Semiconductor Nanophotonics: Materials, Models, Devices”.
Many thanks to Silke Petzold (University of Magdeburg) for her work regarding the sample preparation.
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Bertram, F. et al. (2020). Optical and Structural Properties of Nitride Based Nanostructures. In: Kneissl, M., Knorr, A., Reitzenstein, S., Hoffmann, A. (eds) Semiconductor Nanophotonics. Springer Series in Solid-State Sciences, vol 194. Springer, Cham. https://doi.org/10.1007/978-3-030-35656-9_5
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