SCHEDULED MAINTENANCE
The reaction of the tert-butyldimethylsilyl protected glucal epoxide 1 with thiophenol under a variety of conditions gives three distinct adducts, including the α-phenylthioglycoside 2a, which exists both in solution and in the solid state in a 1C4 conformation in which the C-2, C-3, C-4 and C-5 substituents are all axial.
C. Walford and S. L. Heath, Chem. Commun., 1997, 1855 DOI: 10.1039/A704534D
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