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Effect of ablation time for loading amounts of magnetic nanoparticles on CNTs for removal of Pb (II) ions from aqueous solution

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Abstract

A straightforward pulsed laser ablation method at room temperature was successful in fabricating Fe3O4/carbon nanotubes (Fe3O4/CNTs). Another thing that was controlled was the laser ablation time when different amounts of magnetic nanoparticles were added to decorate CNTs. The magnetic nanocomposite materials were investigated for their adsorption capacity for lead (Pb2+). The prepared samples were studied via different techniques to show the change in the morphology, structure, magnetic, and adsorption properties in detail, such as FT-IR, XRD, SEM, Raman, TGA, XPS, BET, and VSM. These methods demonstrated that increasing the ablation time could raise the amount of Fe3O4 nanoparticles in the nanocomposites up to a point. After that, the hardness of the tubular structure changed the amount. All of the nanocomposites had good superparamagnetic properties, and the saturation magnetization changed depending on how many Fe3O4 nanoparticles were added. Nanocomposites are very good at adsorbing things and recycling them, which is because they are strongly magnetic and have a lot of Fe3O4/CNTs spread out. A study was done to find the best conditions for adsorption, so that the most Pb2+ ions could be removed. By adjusting various physicochemical variables, such as pH, reaction time, and adsorbent dosage, this was possible. The goal is reached by thoroughly getting rid of as many Pb2+ ions as possible. The pseudo-second-order kinetic model accurately described the adsorption kinetics for getting rid of Pb2+. We can, therefore, conclude that the Fe3O4/CNTs nanocomposites can be used again and again after being destroyed for 30 min. This makes them a cheap way to remove Pb2+ from water-based solutions.

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Acknowledgements

The authors would like to extend their sincere appreciation to Princess Nourah bint Abdulrahman University Researchers Supporting Project number (PNURSP2024R38), Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia. In addition, Wafaa B. Elsharkawy thanks the Scientific Research Deanship (SRD) in the Prince Sattam bin Abdulaziz University, kingdom of Saudi Arabia (KSA).

Funding

This research was funded by the Princess Nourah bint Abdulrahman University Re-searchers Supporting Project number (PNURSP2024R38), Princess Nourah bint Abdulrahman University, Riyadh, Saudi Arabia.

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Authors and Affiliations

  1. Department of Physics, College of Science, Princess Nourah Bint Abdulrahman University, P.O. Box 84428, 11671, Riyadh, Saudi Arabia

    Fatemah H. Alkallas & Amira Ben Gouider Trabelsi

  2. Department of Physics, Faculty of Science, Taibah University, 46423, Yanbu, Saudi Arabia

    Shoug M. Alghamdi, Ohood Albeydani & Emaan Alsubhe

  3. Physical Chemistry Department, National Research Centre, Advanced Materials Technology and Mineral Resources Research Institute, 33 El Bohouth St., Dokki, Giza, 12622, Egypt

    Eman A. Mwafy

  4. Physics Department, College of Science and Humanities, Prince Sattam Bin Abdulaziz University, 11942, Alkharj, Saudi Arabia

    Wafaa B. Elsharkawy

  5. Department of Physics, College of Science, Qassim University, P.O. Box, 6644, 51452, Buraydah Almolaydah, Saudi Arabia

    Ayman M. Mostafa

  6. Physics Research Institute, National Research Centre, 33 El Bohouth St., Dokki, Giza, 12622, Egypt

    Ayman M. Mostafa

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  1. Fatemah H. Alkallas
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All authors contributed to the study conception and design. Material preparation, data collection, and analysis.

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Correspondence to Ayman M. Mostafa.

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Alkallas, F.H., Alghamdi, S.M., Albeydani, O. et al. Effect of ablation time for loading amounts of magnetic nanoparticles on CNTs for removal of Pb (II) ions from aqueous solution. Appl. Phys. A 130, 128 (2024). https://doi.org/10.1007/s00339-024-07274-4

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