ISIS Neutron and Muon Source Data Journal

This is a page describing data taken during an experiment at the ISIS Neutron and Muon Source. Information about the ISIS Neutron and Muon Source can be found at https://www.isis.stfc.ac.uk.


Structural Analysis of Water Multilayer in Lamellar Mesoporous Materials

Abstract: Although the preparation of lamellar mesoporous materials (LMMs) is very difficult due to collapsion in removing the templating surfactant, we have successfully synthesized a novel functionalized LMM film by supporting the silica layers with pillars. The interlayer distance is adjustable so as to be double of the length of the functional group, which consists of a hydrophilic and hydrophobic part. Thus, the unbound hydrophilic parts are expected to form a monolayer of water at the middle of the two adjacent silica layers in wet atmosphere. However, there are no experimental evidences to support the presence of the water monolayer. We, therefore, wish to propose a neutron reflectivity (NR) experiment for the LMMs with various humidity conditions, because NR is the only technique to provide distribution of the water in the LMM.

Public release date: 06 June 2014

Principal Investigator: Dr Masashi Harada
Experimenter: Dr Jun Sugiyama
Experimenter: Dr Satoru Fujita
Experimenter: Dr Izumi Umegaki

DOI: 10.5286/ISIS.E.24079381

ISIS Experiment Number: RB1010215

Part Number: 1 - INTER

Date of Experiment: 04 June 2011

Publisher: STFC ISIS Neutron and Muon Source

Data format: RAW/Nexus
Select the data format above to find out more about it.

Data Citation

The recommended format for citing this dataset in a research publication is as:
[author], [date], [title], [publisher], [doi]

For Example:
Dr Masashi Harada et al; (2011): Structural Analysis of Water Multilayer in Lamellar Mesoporous Materials, STFC ISIS Neutron and Muon Source, https://doi.org/10.5286/ISIS.E.24079381



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