Published April 2, 2016 | Version 10004502
Journal article Open

Quartz Crystal Microbalance Holder Design for On-Line Sensing in Liquid Applications

Description

In this paper, the design of a QCM sensor for liquid media measurements in vertical position is described. A rugged and low-cost proof holder has been designed, the cost of which is significantly lower than those of traditional commercial holders. The crystal is not replaceable but it can be easily cleaned. Its small volume permits to be used by dipping it in the liquid with the desired location and orientation. The developed design has been experimentally validated by measuring changes in the resonance frequency and resistance of the QCM sensor immersed vertically in different calibrated aqueous glycerol solutions. The obtained results show a great agreement with the Kanazawa theoretical expression. Consequently, the designed QCM sensor would be appropriate for sensing applications in liquids, and might take part of a future on-line multichannel low-cost QCM-based measurement system.

Files

10004502.pdf

Files (321.3 kB)

Name Size Download all
md5:09418b8958b3d02495250492245dc996
321.3 kB Preview Download

Additional details

References

  • rt E. Speight and Matthew A. Cooper, "A Survey of the 2010 Quartz Crystal Microbalance Literature" J. Mol. Recognit. 2012; 25: 451–473, pp. 15–64.
  • Sandeep Kumar Vashist and Priya Vashist, "Recent Advances in Quartz Crystal Microbalance-Based Sensors", Journal of sensors, vol. 2011, Article ID 571405, 13 pages.
  • A. Arnau (Ed.), "Piezoelectric Transducers and Applications", Springer-Verlag, Berlin Heidelberg (2004), pp 73-74.
  • John Henderson, "Electronic Devices. Concepts and Applications", Prentice Hall, NJ, (1991) p. 357.
  • Sauerbrey G 1959 Use of quartz crystal vibrator for weighting thin films on a microbalance Z Phys. 155 206-222.
  • T. Nomura and M. Okuhara, Anal. Chim. Acta 142(1982) 281.
  • A. P. M. Glassford, "Response of a Quartz Crystal Microbalance to a liquid Deposit", J. Vac. Sci. Technol., 15(6) (1978) 1836.
  • K. Keiji Kanazawa and Joseph Gordon II, "Frequency of a Quartz Microbalance in Contact with Liquid", Anal Chem. 57(1985) 1770
  • K. Keiji Kanazawa and Joseph G. Gordon II, Analytica Chimica Acta, 175(1985) 99-105. [10] Stephen Martin, Victoria Edwards Granstaff and Gregory C. Frye, "Characterization of a Quartz Crystal Microbalance with Simultaneous Mass and Liquid Loading", Anal. Chem. 63 (1991) 2272. [11] Glycerine Producer's Association (New York) Handbook, "Physical Properties of Glicerine and Its Solutions". [12] A. Arnau, "A Review of Interface Electronic Systems for AT-cut Quartz Crystal Microbalance Applications in Liquids", Sensors 2008, 8, 370-411.