P07 - Development of a Miniaturized Combined DSC and TGA Sensor

Event
SMSI 2023
2023-05-08 - 2023-05-11
Nürnberg
Band
Poster
Chapter
Poster
Author(s)
J. Distler, J. Kita, R. Moos, R. Werner - University of Bayreuth, Bayreuth (Germany), M. Gerlach, M. Gollner, F. Linseis - Linseis Thermal Analysis, Selb (Germany)
Pages
294 - 295
DOI
10.5162/SMSI2023/P07
ISBN
978-3-9819376-8-8
Price
free

Abstract

A miniaturized sensor with both, differential scanning calorimetry (DSC) and combined thermogravimetric analysis (TGA) functionality is presented. The ceramic sensor with integrated heater features high heating and cooling rates and enables the analysis of aggressive materials. The working principle based on the mass-dependent frequency change of the chip as a vibrating cantilever is described. The analysis of copper sulfate pentahydrate (CuSO4 · 5 H2O, an often-used reference substance) proves that DSC and TGA measurements can be carried out simultaneously under real conditions.

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