Effects of Calcination Parameters on the Microstructure and Morphology of PZT Nanoparticles Prepared by Modified Sol–Gel Method

Amid Shakeri; Hossein Abdizadeh; Mohammad Reza Golobostanfard

doi:10.4028/www.scientific.net/AMR.576.326

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HomeAdvanced Materials ResearchAdvanced Materials Research Vol. 576Effects of Calcination Parameters on the...

Effects of Calcination Parameters on the Microstructure and Morphology of PZT Nanoparticles Prepared by Modified Sol–Gel Method

Abstract:

Lead zirconate titanate nanopowder Pb(Zr0.53Ti0.47)O3 (PZT) was prepared by modified sol-gel method with 1-propanol as solvent and acetylacetone as stabilizer. The microstructure and particle size measurements at different heat treatment conditions were characterized by field emission scanning electron microscopy and x-ray diffraction analysis. It was found that the PZT nanoparticles calcinated at 600 °C showed mean diameter of 75-125 nm with high crystallinity of perovskite-type structure.

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Periodical:

Advanced Materials Research (Volume 576)

Pages:

326-329

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.576.326

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Online since:

October 2012

Authors:

Amid Shakeri, Hossein Abdizadeh, Mohammad Reza Golobostanfard

Keywords:

Lead Zirconate Titanate (PZT), Nanoparticle, Pyrochlore Phase, Sol-Gel Method

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