Study on Hydrothermal Synthesis of Flower-Sphere MoS2

Jun Zhou; Xin Zhe Lan; Ping Ren; Lei Wu

doi:10.4028/www.scientific.net/AMR.311-313.566

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HomeAdvanced Materials ResearchAdvanced Materials Research Vols. 311-313Study on Hydrothermal Synthesis of Flower-Sphere...

Study on Hydrothermal Synthesis of Flower-Sphere MoS₂

Abstract:

An effective technology of hydrothermal synthesizing flower-sphere MoS₂ by reaction of Na₂MoO₄ and CS(NH₂)₂ with NH₂OH•HCl as reductant was researched. The effect of the molar ratio of Mo to S, reaction temperature, reaction time, aging time on the yield, purity and morphology of the product was explored by means of X-ray diffraction (XRD) and scanning electron microscope (SEM). The results show that the optimal synthesis conditions are as follows: the molar ratio of Mo to S of 1:7, the temperature of 220°C, the reaction time of 24h and the aging time of 16h. Under these conditions, the inerratic and pure flower-sphere MoS₂ was obtained. Its average particle size is about 2μm and the petal is self-assembly growth. The yield of the product can reach 88%.

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Advanced Materials and Processes: ADME 2011

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Periodical:

Advanced Materials Research (Volumes 311-313)

Pages:

566-570

DOI:

https://doi.org/10.4028/www.scientific.net/AMR.311-313.566

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Online since:

August 2011

Authors:

Jun Zhou, Xin Zhe Lan, Ping Ren, Lei Wu

Keywords:

Hydrothermal Synthesis, Liquid Reduction, Molybdenum Disulfide

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References

[1] Alonso G, Berhault G, Aguilar A, et al.: J. of Catal. Vol. 208, No. 2 (2002), p.359

Google Scholar

[2] Iwata Y, Araki Y, Honna K, et al.: Catal. Today Vol. 65, No. 2 (2001), p.355

Google Scholar

[3] Xue Shoufeng, Lan Xinzhe, Zhou Jun, et al.: Ordnance Mater. Sci. and Eng. Vol. 33, No. 3 (2010), p.88

Google Scholar

[4] Wang Quanshan, Lan Xinzhe, Zhou Jun, et al.: Gdchem. Vol. 34, No. 173 (2007), p.32

Google Scholar

[5] Chang L X, Yang H B, Fu W Y, et al.: Mater. Res. Bull. Vol. 43 (2008), p.2427

Google Scholar

[6] Wei Ronghui, Yang Haibin, Du Kai, et al.: Mater. Chem. and Phys. Vol. 108, No. 2-3 (2008), p.188

Google Scholar

[7] Lin Ma, Weixiang Chen, Hui Li, et al.: Mater. Lett. Vol. 62 (2008), p.797

Google Scholar

[8] Shi H Q, Fu X, Zhou X D, et al.: J. of Solid State Chem. Vol. 179 (2006), p.1690

Google Scholar

[9] Sun Yanli: Master's Thesis (Fujian Normal University, 2009).

Google Scholar