Green Synthesis of Spinel Magnetite Iron Oxide Nanoparticles

Article Preview

Abstract:

Spinel magnetite Fe3O4 nanoparticles were synthesized using rambutan peel waste extract as a green ligation and chelating agent. The green synthesized nanoparticles were characterized employing X-ray diffraction (XRD), Raman spectroscopy, FTIR spectroscopy and transmission electron microscopy (TEM) studies. The XRD study revealed spinel phase hda a magnetite structure. The formation of iron oxide nanoparticles using rambutan extract was confirmed employing IR studies. XRD, FTIR and Raman spectrum analyses all supports the synthesis of Fe3O4 nanoparticles. The TEM revealed the spinel morphology of the biosynthesized nanoparticles with 200 nm.

You might also be interested in these eBooks

Info:

Periodical:

Pages:

39-42

Citation:

Online since:

October 2014

Export:

Price:

* - Corresponding Author

[1] M.E. Sadat, R. Patel, J. Sookoor, S.L. Bud'ko, R.C. Ewing, J. Zhang, H. Xu, Y. Wang, G.M. Pauletti, D.B. Mast, D. Shi, Effect of spatial confinement on magnetic hyperthermia via dipolar interactions in Fe3O4 nanoparticles for biomedical applications, Mater. Sci. Eng. C 42 (2014).

DOI: 10.1016/j.msec.2014.04.064

Google Scholar

[2] A. Nemati, S. Shadpour, H. Khalafbeygi, M. Barkhi, Hydrothermal synthesis and size control of Fe3O4 nanoparticles in the Presence of 2, 2', 2', 2', - (ethane-1, 2-diylbis(azanetriyl) tetraaceto hydrazide, Synth. React. Inorg. Met. -Org. Chem. 44 (2014).

DOI: 10.1080/15533174.2013.797443

Google Scholar

[3] F. Chen, R. Liu, S. Xiao, M. Lin, One-step solvothermal synthesis of epichlorohydrin-modified magnetic Fe3O4 microspheres in ethylene glycol, Mater. Lett. 130 (2014) 101-103.

DOI: 10.1016/j.matlet.2014.05.022

Google Scholar

[4] X. Huang, C. Yi, Y. Fan, Y. Zhang, L. Zhao, Z. Liang, J. Pan, Magnetic Fe3O4 nanoparticles grafted with single-chain antibody (scFv) and docetaxel loaded β-cyclodextrin potential for ovarian cancer dual-targeting therapy, Mater. Sci. Eng. C 42 (2014).

DOI: 10.1016/j.msec.2014.05.041

Google Scholar

[5] P. Liu, Y. Huang, X. Zhang, Synthesis and excellent microwave absorption properties of graphene/polypyrrolecomposites with Fe3O4 particles prepared via a co-precipitation method, Mater. Lett. 129 (2014) 35–38.

DOI: 10.1016/j.matlet.2014.04.194

Google Scholar

[6] M.E. Sadat, R. Patel, S.L. Budko, R.C. Ewing, J. Zhang, H. Xu, D.B. Mast, D. Shi, Dipole-interaction mediated hyperthermia heating mechanism of nanostructured Fe3O4 composites, Mater. Lett. 129 (2014) 57–60.

DOI: 10.1016/j.matlet.2014.05.001

Google Scholar

[7] S. Venkateswarlu, B. Natesh Kumar, C.H. Prasad, P. Venkateswarlu, N.V.V. Jyothi, Bio-inspired green synthesis of Fe3O4 spherical magnetic nanoparticles using Syzygium cumini seed extract, Physica B 449 (2014) 67–71.

DOI: 10.1016/j.physb.2014.04.031

Google Scholar

[8] R. Yuvakkumar, J. Suresh, S.I. Hong, Green synthesis of zinc oxide nanoparticles, Adv. Mater. Res. 952 (2014) 137-140.

DOI: 10.4028/www.scientific.net/amr.952.137

Google Scholar

[9] J. Suresh, R. Yuvakkumar, M. Sundrarajan, S.I. Hong, Green synthesis of magnesium oxide nanoparticles, Adv. Mater. Res. 952 (2014) 141-144.

DOI: 10.4028/www.scientific.net/amr.952.141

Google Scholar

[10] R. Yuvakkumar, V. Elango, V. Rajendran, N. Kannan, P. Prabu, Influence of nanosilica powder on the growth of maize crop (Zea Mays L. ), Int. J. Green Nanotechnol. Phys. Chem. 3 (2011) 180-190.

DOI: 10.1080/19430892.2011.628581

Google Scholar

[11] R. Yuvakkumar, V. Elango, V. Rajendran, N. Kannan, P. Prabu, Influence of nano nutrients on heterocyst forming cyanobacterium Anabaena ambigua Rao, Synth. React. Inorg. Met. -Org. Chem. 41 (2011) 1234-1239.

DOI: 10.1080/15533174.2011.591875

Google Scholar

[12] O. Pascu, S. Marre, C. Aymonier, A. Roig, Ultrafast and continuous synthesis of crystalline ferrite nanoparticles in supercritical ethanol, RSC Nanoscale 5 (2013) 2126-2132.

DOI: 10.1039/c3nr33501a

Google Scholar

[13] R. Yuvakkumar, J. Suresh, A. Joseph Nathanael, M. Sundrarajan, S.I. Hong, Novel green synthetic strategy to prepare ZnO nanocrystals using rambutan (Nephelium lappaceum L. ) peel extract and its antibacterial applications, Mater. Sci. Eng., C 41 (2014).

DOI: 10.1016/j.msec.2014.04.025

Google Scholar

[14] R. Yuvakkumar, J. Suresh, A. Joseph Nathanael, M. Sundrarajan, S.I. Hong, Rambutan (Nephelium lappaceum L. ) peel extract assisted biomimetic synthesis of nickel oxide nanocrystals, Mat. Lett. 128 (2014) 170-174.

DOI: 10.1016/j.matlet.2014.04.112

Google Scholar

[15] R. Yuvakkumar, V. Elango, V. Rajendran, N. Kannan, A new approach to preparing crystalline nano molybdenum particles, Synth. React. Inorg. Met. -Org. Chem. 41 (2011) 309-314.

DOI: 10.1080/15533174.2011.555864

Google Scholar

[16] R. Yuvakkumar, V. Elango, V. Rajendran, N. Kannan, High-purity nano silica powder from rice husk using a simple chemical method, J. Exp. Nanosci. 9 (2014) 272-281.

DOI: 10.1080/17458080.2012.656709

Google Scholar

[17] R. Yuvakkumar, V. Elango, V. Rajendran, N. Kannan, Preparation and characterization of zero-valent iron nanoparticles, Digest J. Nanomaterials and Biostructures 6 (2011) 1771-1776.

Google Scholar