Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method

@article{ART002836204},
author={ K.W. Goh and Y.H. Wong and R.S.K. Singh and Hari Chandran and S.K. Wong and K.Y. Sara Lee },
title={Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method},
journal={Journal of Ceramic Processing Research},
issn={1229-9162},
year={2022},
volume={23},
number={2},
pages={158-164},
doi={10.36410/jcpr.2022.23.2.158},
url={http://dx.doi.org/10.36410/jcpr.2022.23.2.158}

TY - JOUR
AU - K.W. Goh
AU - Y.H. Wong
AU - R.S.K. Singh
AU - Hari Chandran
AU - S.K. Wong
AU - K.Y. Sara Lee
TI - Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method
T2 - Journal of Ceramic Processing Research
PY - 2022
VL - 23
IS - 2
PB - 한양대학교 청정에너지연구소
SP - 158-164
SN - 1229-9162
AB - The extraction of calcium from natural biowaste material such as chicken eggshells have been shown to be viable to synthesiscalcium phosphate bioceramic. In this work, eggshell-derived hydroxyapatite powder was synthesised by using the wetchemical precipitation technique coupled with microwave irradiation at low power (700 W) at varying exposure time from 5to 30 min. The derived nano-powders were examined to determine the phases present, chemical bonding and microstructuralevolution. It was revealed that the irradiation time has an effect on the degree of crystallinity and both the crystallite andparticle size of the derived powders although the hydroxyapatite phase stability was not disrupted. An exposure time of 15 min. was determined to be sufficient when subjected to low power microwave irradiation to formed a well-defined needle-likehydroxyapatite particles having an average crystallite size of about 22 nm. On the contrary to many literatures, this study hasdemonstrated the viability of synthesizing a useful bioceramic from using biowaste eggshells coupled with microwaveirradiation at low power of 700 W for very short period of time to produce nano-range needle-like hydroxyapatite particlessuitable for biomedical application.
KW - Eggshells, Calcium phosphate, Bioceramic, Microwave-assisted synthesis, Hydroxyapatite
DO - 10.36410/jcpr.2022.23.2.158
UR - http://dx.doi.org/10.36410/jcpr.2022.23.2.158
ER -

K.W. Goh , Y.H. Wong , R.S.K. Singh , Hari Chandran , S.K. Wong and K.Y. Sara Lee (2022). Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method. Journal of Ceramic Processing Research, 23( 2), 158- 164.

K.W. Goh , Y.H. Wong , R.S.K. Singh , Hari Chandran , S.K. Wong and K.Y. Sara Lee . 2022, “Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method”, Journal of Ceramic Processing Research, vol. 23, no. 2, pp. 158-164. Available from: doi:10.36410/jcpr.2022.23.2.158

K.W. Goh Y.H. Wong et al. R.S.K. Singh Hari Chandran S.K. Wong K.Y. Sara Lee “Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method” Journal of Ceramic Processing Research 23.2 pp. 158-164 (2022): 158.

K.W. Goh , Y.H. Wong , R.S.K. Singh , Hari Chandran , S.K. Wong , K.Y. Sara Lee . Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method Journal of Ceramic Processing Research [Internet]. 2022; 23( 2), : 158-164. Available from: doi:10.36410/jcpr.2022.23.2.158

K.W. Goh , Y.H. Wong , R.S.K. Singh , Hari Chandran , S.K. Wong and K.Y. Sara Lee . “Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method” Journal of Ceramic Processing Research 23, no.2 (2022): 158-164. doi: 10.36410/jcpr.2022.23.2.158

홈 권호 목록 논문 목록 논문 상세

Irradiation time-dependent study of eggshell-derived hydroxyapatite powder synthesized by microwave-assisted wet chemical precipitation method

Journal of Ceramic Processing Research

약어 : J. Ceram. Process. Res.

2022, vol.23, no.2, pp.158 - 164

DOI : 10.36410/jcpr.2022.23.2.158

발행기관 : 한양대학교 청정에너지연구소

연구분야 : 재료공학

K.W. Goh¹ , Y.H. Wong² , R.S.K. Singh³ , Hari Chandran⁴ , S.K. Wong⁵ , K.Y. Sara Lee⁶

¹University of Malaya

²University of Malaya

³University of Malaya

⁴University of Malaya

⁵Universiti Kebangsaan Malaysia

⁶Tunku Abdul Rahman University College

인용한 논문 수 : 1 서지 간략 보기

초록

The extraction of calcium from natural biowaste material such as chicken eggshells have been shown to be viable to synthesiscalcium phosphate bioceramic. In this work, eggshell-derived hydroxyapatite powder was synthesised by using the wetchemical precipitation technique coupled with microwave irradiation at low power (700 W) at varying exposure time from 5to 30 min. The derived nano-powders were examined to determine the phases present, chemical bonding and microstructuralevolution. It was revealed that the irradiation time has an effect on the degree of crystallinity and both the crystallite andparticle size of the derived powders although the hydroxyapatite phase stability was not disrupted. An exposure time of 15 min. was determined to be sufficient when subjected to low power microwave irradiation to formed a well-defined needle-likehydroxyapatite particles having an average crystallite size of about 22 nm. On the contrary to many literatures, this study hasdemonstrated the viability of synthesizing a useful bioceramic from using biowaste eggshells coupled with microwaveirradiation at low power of 700 W for very short period of time to produce nano-range needle-like hydroxyapatite particlessuitable for biomedical application.

키워드

Eggshells, Calcium phosphate, Bioceramic, Microwave-assisted synthesis, Hydroxyapatite

참고문헌(25)

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