Crystal Structure of <font size=-1>D</font>-(+)-Camphoric Imide

Wei HUANG; Huifen QIAN; Yizhi LI; Zhaolian CHU; Shaohua GOU

doi:10.2116/analscix.20.x75

April - June

Crystal Structure of D-(+)-Camphoric Imide

Wei HUANG, Huifen QIAN, Yizhi LI, Zhaolian CHU, Shaohua GOU

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JOURNAL FREE ACCESS

2004 Volume 20 Pages x75-x76

DOI https://doi.org/10.2116/analscix.20.x75

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Abstract

(1R,5S)-1,8,8-Trimethyl-3-azabicylo[3.2.1]octane-2,4-dione [D-(+)-camphoric imide] has been synthesized and characterized by IR, EA, ES-MS, ¹H NMR, ¹³C NMR and X-ray diffraction techniques. The four independent molecules form a two-dimensional network by means of eight-membered N-H…O (C₂O₂N₂H₂) hydrogen-bond rings between their imide groups, and weak C-H…O hydrogen bonding interactions involving the imide oxygen atoms.

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