Skip to main content
Log in

Combining Serial Sectioning, EBSD Analysis, and Image-Based Finite Element Modeling

  • Technical Feature
  • Published:
MRS Bulletin Aims and scope Submit manuscript

Abstract

This article first provides a brief review of the status of the subfield of three-dimensional (3D) materials analyses that combine serial sectioning, electron backscatter diffraction (EBSD), and finite element modeling (FEM) of materials microstructures, with emphasis on initial investigations and how they led to the current state of this research area. The discussions focus on studies of the mechanical properties of polycrystalline materials where 3D reconstructions of the microstructure—including crystallographic orientation information—are used as input into image-based 3D FEM simulations. The authors’ recent work on a β-stabilized Ti alloy is utilized for specific examples to illustrate the capabilities of these experimental and modeling techniques, the challenges and the solutions associated with these methods, and the types of results and analyses that can be obtained by the close integration of experiments and simulations.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. M.A. Mangan, G.J. Shiflet, in Solid-Solid Phase Transformations Proceedings, W.C. Johnson, J.M. Howe, D.E. Laughlin, W.A. Soffa, eds. (TMS, Warrendale, PA, 1994), p. 547.

    Google Scholar 

  2. M.A. Mangan, P.D. Lauren, G.J. Shiflet, J. Microsc. 188, 36 (1997).

    Google Scholar 

  3. T.L. Wolfsdorf, W.H. Bender, P.W. Voorhees, Acta Mater. 45, 2279 (1997).

    Google Scholar 

  4. M.V. Kral, G. Spanos, Acta Metall. 47, 711 (1999).

    Google Scholar 

  5. Z. Shan, A.M. Gokhale, Acta Mater. 49, 2001 (2001).

    Google Scholar 

  6. R.E. Hackenberg, D.P. Nordstrom, G.J. Shiflet, Scripta Mater. 47, 357 (2002).

    Google Scholar 

  7. J.E. Spowart, H.M. Mullens, B.T. Puchala, JOM 55, 35 (2003).

    Google Scholar 

  8. T. Yokomizo, M. Enomoto, O. Umezawa, G. Spanos, R.O. Rosenberg, Mater. Sci. Eng. A 344, 261 (2003).

    Google Scholar 

  9. K.M. Wu, Y. Inagawa, M. Enomoto, Mater. Charact. 52, 121 (2004).

    Google Scholar 

  10. J.J.L. Mulders, A.P. Day, Mater. Sci. Forum 495–497, 237 (2005).

    Google Scholar 

  11. J.E. Spowart, Scripta Mater. 55, 5 (2006).

    Google Scholar 

  12. D.J. Rowenhorst, A. Gupta, C.R. Feng, G. Spanos, Scripta Mater. 55, 11 (2006).

    Google Scholar 

  13. M.D. Uchic, M.A. Groeber, D.M. Dimiduk, J.P. Simmonds, Scripta Mater. 55, 23 (2006).

    Google Scholar 

  14. A.J. Schwartz, M. Kumar, B.L. Adams, Electron Backscatter Diffraction in Materials Science (Kluwer Academic, New York, 2000).

    Google Scholar 

  15. D.J. Dingley, J. Microsc. 213, 214 (2004).

    Google Scholar 

  16. R.K. Everett, A.B. Geltmacher, K.E. Simmonds, “3D Image-Based Modeling of Void Interactions in HY100 Steel” in Plasticity, Damage, and Fracture at Macro, Micro, and Nano Scales, A.S. Khan, O. Lopez-Pamies, eds. (NEAT Press, Fulton, MD, 2002), pp. 699–701.

    Google Scholar 

  17. A.C. Lewis, A.B. Geltmacher, Scripta Mater. 55, 81 (2006).

    Google Scholar 

  18. M.A. Mangan, G.J. Shiflet, Scipta Mater. 37, 517 (1997).

    Google Scholar 

  19. A.A. Wahab, M.V. Kral, Mater. Sci. Eng. A 412, 222 (2005).

    Google Scholar 

  20. M.A. Wall, A.J. Schwartz, L. Nguyen, Ultramicroscopy 88, 73 (2001).

    Google Scholar 

  21. H. Jin, P.D. Wu, M.D. Ball, D.J. Lloyd, Mater. Sci. Technol. 21, 419 (2005).

    Google Scholar 

  22. H. Schaeben, M. Apel, T. Frank, M. Iwanowski, S. Zaefferer, Mater. Sci. Forum 495–497, 185 (2005).

    Google Scholar 

  23. M. Groeber, B. Haley, M. Uchic, S. Ghosh, AIP Conference Proceedings—Materials Processing and Design: Modeling, Simulation, and Applications, NUMIFORM (2004), p. 1712.

  24. M.D. Uchic, M. Groeber, R. Wheeler, F. Scheltens, D.M. Dimiduk, Microsc. Microanal. 10, 1136 (2004).

    Google Scholar 

  25. S. Zaefferer, Mater. Sci. Forum 495–497, 3 (2005).

    Google Scholar 

  26. R. Petrov, O.L. Garcìa, J.J.L. Mulders, A.C.C. Reis, J.-H. Bae, L. Kestens, Y. Houbaert, Mater. Sci. Forum 550, 625 (2007).

    Google Scholar 

  27. J. Konrad, S. Zaefferer, D. Raabe, Acta Mater. 54, 1369 (2006).

    Google Scholar 

  28. M. Groeber, B. Haley, M. Uchic, D.M. Dimiduk, S. Ghosh, Mater. Charact. 57, 259 (2006).

    Google Scholar 

  29. J.P. Mathieu, S. Berveiller, K. Inal, O. Diard, Fatigue Fract. Eng. Mater. Struct. 29, 725 (2006).

    Google Scholar 

  30. T.S. Han, P.R. Dawson, Mater. Sci. Eng. A 405, 18 (2005).

    Google Scholar 

  31. P.R. Dawson, D.P. Mika, N.R. Barton, Scripta Mater. 47, 713 (2002).

    Google Scholar 

  32. N. Chawla, V.V. Ganesh, B. Wunsch, Scripta Mater. 51, 161 (2004).

    Google Scholar 

  33. N. Chawla, R.S. Sidhu, J. Mater. Sci.: Mater. Electron. 18, 175 (2007).

    Google Scholar 

  34. N. Zaafarani, D. Raabe, R.N. Singh, F. Roters, S. Zaefferer, Acta Mater. 54, 1863 (2006).

    Google Scholar 

  35. A.C. Lewis, J.F. Bingert, D.J. Rowenhorst, A. Gupta, A.B. Geltmacher, G. Spanos, Mater. Sci. Eng. A 418, 11 (2006).

    Google Scholar 

  36. G. Spanos, A.B. Geltmacher, A.C. Lewis, J.F. Bingert, M. Mehl, D. Papaconstantopoulos, Y. Mishin, A. Gupta, P. Matic, Mater. Sci. Eng. A 452–453, 558 (2007).

    Google Scholar 

  37. E. Nakamachi, N.N. Tam, H. Morimoto, Int. J. Plast. 23, 450 (2007).

    Google Scholar 

  38. M.D. Uchic, L. Holzer, B.J. Inkson, E.L. Principe, P. Munroe, MRS Bull. 32, 408 (2007).

    Google Scholar 

  39. A.B. Geltmacher, A.C. Lewis, D.J. Rowenhorst, M.A. Qidwai, G. Spanos, Proceedings of the 11th World Conference on Titanium: Ti-2007 Science and Technology, Kyoto, Japan, 3 June 2007, pp. 475–478.

  40. M.A. Qidwai, A.B. Geltmacher, A.C. Lewis, D.J. Rowenhorst, G. Spanos, paper IMECE2007-42007 presented at the 2007 ASME International Mechanical Engineering Congress & Exposition (IMECE), Seattle, WA, 11 November 2007.

  41. S.A. Langer, E. Fuller, W.C. Carter, Comput. Sci. Eng. 3, 15 (2001).

    Google Scholar 

  42. A.C. Lewis, K.A. Jordan, A.B. Geltmacher, Metall. Mater. Trans. A 39A, 1109 (2008).

    Google Scholar 

  43. G. Cailletaud, S. Forest, D. Jeulin, F. Feyel, I. Galliet, V. Mounoury, S. Quilici, Comput. Mater. Sci. 27, 351 (2003).

    Google Scholar 

  44. O. Diard, S. Leclereq, G. Rousselier, G. Cailletaud, Int. J. Plast. 21, 691 (2005).

    Google Scholar 

  45. A.C. Lewis, C. Suh, M. Stukowski, A.B. Geltmacher, G. Spanos, K. Rajan, JOM 58, 52 (2006).

    Google Scholar 

  46. H. Ledbetter, H. Ogi, S. Kai, S. Kim, M. Hirao, J. Appl. Phys. 95, 4642 (2004).

    Google Scholar 

Download references

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Spanos, G., Rowenhorst, D.J., Lewis, A.C. et al. Combining Serial Sectioning, EBSD Analysis, and Image-Based Finite Element Modeling. MRS Bulletin 33, 597–602 (2008). https://doi.org/10.1557/mrs2008.124

Download citation

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/mrs2008.124

Navigation