Abstract
We investigated through X- ray diffraction and transmission electron microscopy the crystal refinement of the intermetallic compound AIRu by high- energy ball milling. The deformation process causes a decrease of crystal size to 5–7 rum and an increase of atomic level strain. This deformation is localized in shear bands with a thickness of 0.5 to 1 micron. Within these bands the crystal lattice breaks into small grains with a typical size of 8–14 rum. Further deformation leads to a final nanocrystalline structure with randomly oriented crystallite grains separated by high- angle grain boundaries.
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Hellstern, E., Fecht, H.J., Garland, C. et al. Mechanism of Achieving Nanocrystalline AIRu By Ball Milling. MRS Online Proceedings Library 132, 137–142 (1988). https://doi.org/10.1557/PROC-132-137
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DOI: https://doi.org/10.1557/PROC-132-137