Skip to main content
Log in

High Jc YBa2Cu3O7-δ films via rapid, low pO2 pyrolysis

  • Articles
  • Published:
Journal of Materials Research Aims and scope Submit manuscript

Abstract

In this investigation YBa2Cu3O7-δ (YBCO) films were fabricated via a metal acetate, trifluoroacetic acid based sol-gel route and spin-coat deposited on (100) LaAlO3 with a focus on maximizing Jc, while minimizing processing time. We demonstrate that the use of a low-pO2 atmosphere during the pyrolysis stage can lead to at least a tenfold reduction in pyrolysis time, compared to a 1 atm O2 ambient. High-quality YBCO films on LaAlO3, with Jc values up to 3 MA/cm2 at 77 K, can be routinely crystallized from these rapidly pyrolyzed films.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. P.M. Mankiewich, J.H. Scofield, W.J. Skocpol, R.E. Howard, A.H. Dayem, and E. Good, Appl. Phys. Lett. 51, 1753 (1987).

    Article  CAS  Google Scholar 

  2. M.P. Siegal, J.M. Phillips, R.B. van Dover, T.H. Tiefel, and J.H. Marshall, J. Appl. Phys. 68, 6353 (1990).

    Article  CAS  Google Scholar 

  3. M.P. Siegal, S.Y. Hou, J.M. Phillips, T.H. Tiefel, and J.H. Marshall, J. Mater. Res. 7, 2658 (1992).

    Article  CAS  Google Scholar 

  4. F.H. Garzon, J.G. Beery, D.R. Brown, R.J. Sherman, and I.D. Raistrick, Appl. Phys. Lett. 54, 1365 (1989).

    Article  CAS  Google Scholar 

  5. S-W. Chan, B.G. Bagley, L.H. Greene, M. Giroud, W.L. Feldmann, K.R. Jenkin II, and B.J. Wilkins, Appl. Phys. Lett. 53, 1443 (1988).

    Article  CAS  Google Scholar 

  6. S.Y. Hou, J.M. Phillips, D.J. Werder, T.H. Tiefel, J.H. Marshall, and M.P. Siegal, J. Mater. Res. 9, 1936 (1994).

    Article  CAS  Google Scholar 

  7. A. Malecki, J. Oblakowski, and S. Labus, Mater. Res. Bull. 30, 731 (1995).

    Article  CAS  Google Scholar 

  8. A. Gupta, R. Jagannathan, E.I. Cooper, E.A. Giess, J.I. Landman, and B.W. Hussey, Appl. Phys. Lett. 52, 2077 (1988).

    Article  CAS  Google Scholar 

  9. P.C. McIntyre, M.J. Cima, J.A. Smith Jr ., R.B. Hallock, M.P. Siegal, and J.M. Phillips, J. Appl. Phys. 71, 1868 (1992).

    Article  CAS  Google Scholar 

  10. P.C. McIntyre and M.J. Cima, J. Mater. Res. 9, 2219 (1994).

    Article  CAS  Google Scholar 

  11. J.A. Smith, M.J. Cima, and N. Sonnenberg, IEEE Trans. Appl. Supercond. 9, 1531 (1999).

    Article  Google Scholar 

  12. P.C. McIntyre, M.J. Cima, and M.F. Ng, J. Appl. Phys. 68, 4183 (1990).

    Article  CAS  Google Scholar 

  13. E.M. Gyorgy, R.B. van Dover, K.A. Jackson, L.F. Schneemeyer, and J.V. Waszczak, Appl. Phys. Lett. 55, 283 (1989).

    Article  CAS  Google Scholar 

  14. S.A. Krupoder, V.S. Danilovich, A.O. Miller, and G.G. Furin, J. Fluorine Chem. 73, 13 (1995).

    Article  CAS  Google Scholar 

  15. D.J. Carlson, M.P. Siegal, J.M. Phillips, T.H. Tiefel, and J.H. Marshall, J. Mater. Res. 5, 2797 (1990).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

About this article

Cite this article

Dawley, J.T., Clem, P.G., Siegal, M.P. et al. High Jc YBa2Cu3O7-δ films via rapid, low pO2 pyrolysis. Journal of Materials Research 16, 13–16 (2001). https://doi.org/10.1557/JMR.2001.0004

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1557/JMR.2001.0004

Navigation