Синтез вуглецевих наноструктур при використанні дешевих марок графіту
Анотація
У роботі синтезовані вуглецеві наноструктури (ВНС) на плазмохімічній установці при використанні графітових електродів ЕГСП (Спеціально імпрегновані графітові електроди) та МПГ-7 (Дрібно зернистий щільний графіт) в середовищі гелію. В експериментах встановлено, що графітові електроди марки ЕГСП придатні для синтезу ВНС електродуговим плазмохімічним методом. Крім того, експерименти вказують на те, що графіт марки ЕГСП в електродуговому синтезі в газовому середовищі дозволяє створити сантиметрові композитні стрижні (депозити), де серцевина складається з графенових листів, згорнутих в нанотрубки, які витримують надвисокі температури (>4000 К). Дослідження за допомогою скануючої мікроскопії показали, що синтезований депозит з графіту марки ЕГСП може розділятися на блоки, що важливо для його використання в станціях високого напруження тому, що можна готувати депозити необхідної довжини без механічного впливу і не порушуючи цілісність його конструкції.
Дослідження за допомогою просвітлюванної мікроскопії показали, що в процесі електродугового випаровування електрода марки ЕГСП формуються безкаталітичні вуглецеві нанотрубки). Експерименти підтвердили, що вихід по масі пристінної фуллеренвмісної сажі при випаровуванні графіту марки ЕГСП значно перевищує результати, отримані при випаровуванні графітових електродів марки МПГ-7. Такі результати роблять графіт марки ЕГСП більш продуктивним для синтезу дорогих вуглецевих нанопродуктів (фуллеренів та фуллереноподібних структур) електродуговим методом.
Також зафіксовано, що в процесі синтезу вуглецевих наноструктур формуються одностінні вуглецеві нанотрубки, які мають позитивний заряд і під дією електромагнітного поля осаджуються у вигляді серцевини на поверхні катодного електрода.
Посилання
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