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Preparation of a Sol–Gel Titania Based Coating for HS-SPME of Aliphatic Alcohols from Non-Alcoholic Beer Samples

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Abstract

A new sol–gel titania based solid phase microextraction fiber for headspace sampling of aliphatic alcohols from non-alcoholic beer samples is introduced. The influences of fiber coating composition and microextraction conditions on the fiber performance were investigated. The proposed fiber is thermally stable up to 250 °C and under optimal conditions demonstrates fast sampling of alcohols with high sensitivity. Finally, aliphatic alcohols content of non-alcoholic beer samples were determined using headspace solid phase microextraction followed by GC-FID.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Science, Urmia University, Urmia, Iran

    Ramin Maleki, Khalil Farhadi & Raheleh Tahmasebi

  2. Research Department of Chromatography, Iranian Academic Center for Education, Culture and Research (ACECR), Urmia Branch, Urmia, Iran

    Ramin Maleki

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  1. Ramin Maleki
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  2. Khalil Farhadi
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  3. Raheleh Tahmasebi
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Correspondence to Ramin Maleki.

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Maleki, R., Farhadi, K. & Tahmasebi, R. Preparation of a Sol–Gel Titania Based Coating for HS-SPME of Aliphatic Alcohols from Non-Alcoholic Beer Samples. Chroma 69, 775–778 (2009). https://doi.org/10.1365/s10337-009-0964-8

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  • DOI: https://doi.org/10.1365/s10337-009-0964-8

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