Prediction of Tensile Shear Fracture Load of Friction Stir Spot-Welded AA2024-T3/HCS Dissimilar Joints

provided the original work is properly cited. Lightweight materials play a vital role in many industries because of their weight reduction, corrosion resistance, and formability. On the other hand, joining this alloy is a very tedious process for everyone in industries due to incompatibility in metallurgical properties. The thick intermetallic formation, porosity, and segregation of alloys in the weld are the possible causes during welding of dissimilar materials by the fusion welding process. Nowadays, these materials have been joined by solid-state welding friction stir welding. AA2024 and high carbon steel (HCS) were used for friction stir spot welding in this investigation. Tool rotational speed, plunge rate, plunge depth, and dwell time were the major in ﬂ uencing process parameters. Design of experiments and response surface methodology were used to optimize the process parameters to attain maximum lap shear strength of AA2024/HCS.


Introduction
AA2024 and high carbon steel (HCS) are the most prevalent materials in heavy structural fabrication industries because of their availability, formability, machinability, etc. [1]; these two alloys are high-strength materials that possess unique properties like corrosion resistance, strength, and light-weight material [2]. The only problem with these materials is that joining materials is very difficult in the fusion welding process due to metallurgical incompatibility [3]. Hence, it is a significant challenge for welding and manufacturing engineers. Nowadays, these two alloys are welded using a solidstate welding process, friction stir welding (FSW). In some of the areas like fabrication, aircraft structure uses riveted joints [4]. By the use of rivets, the payload of the aircraft increases; also, corrosion takes place between two dissimilar materials (galvanic coupling) [5]. Friction stir spot welding is a modified version of the FSW process. This is the most familiar process for replacing riveted joints in all structural fabrication. Bozkurt and Bilici [6] used Taguchi to find optimal FSSW process parameters on AA2024-AA5754 dissimilar alloy. L9 orthogonal array was used to optimize the parameters, and the position of the palate was the primary influencing parameter, among others. Ahmed et al. [7] carried out FSW of AA2024-AISI1018 different alloy. A continuous layer of intermetallic was formed at high temperatures. This layer was found to be the most predominant location for fracture. Moreover, the fracture mode was found to be mixed mode. Yang et al. [8] reviewed the mechanical and metallurgical properties of FSSW joints. The review concluded that the FSSW is the potential process to join dissimilar materials. Lyu et al. [9] investigated the effect of double-sided FSSW on the shear fracture load of aluminum alloy and steel sheet. The shear force of the FSSW joints increased with increasing plunge force. Ojo et al. [10] reviewed the latest trend in FSSW on similar and dissimilar materials. The investigation studied the material flow in the nugget zone and shoulder diameter effect on weld nugget formation. Siddharth and Senthilkumar [11] optimized FSSW parameters of AA2024-C 1100 dissimilar materials using response surface methodology (RSM). Analysis of variance (ANOVA) was used to identify the individual parameter effect on shear fracture load. The maximum shear fracture load was obtained using RSM. Colmenero et al. [12] used the vibration signal's energy to optimize FSSW parameters of Al-Cu dissimilar joints. Two significant parameters, such as rotational speed and dwell time, were used, and RSM predicted     [14] investigated the optimum shear strength of friction stir spot welding parameters of AA1050/C10100. The primary and interaction of FSSW parameters were obtained by analysis of variance. Zhang et al. [1] investigated the multiobjective optimization of friction stir spot-welded parameters on aluminum alloy sheets. NSGA-II method was selected to determine the Pareto front and subsequently choose the best possible solutions. Many researchers throughout the globe have used DOE to improve FSSW parameters in both similar and dissimilar alloys, different Al alloys [14], and aluminum-steel [15]. However, no attempt has yet been made to construct empirical correlations to forecast the ability of aluminum and car-bon steel joints to bear tensile shear fracture load-carrying capacities. This study is aimed at building a mathematical relationship to forecast shear fracture load of FSSW dissimilar joints.

Experimental Work
In this investigation, 2 mm thick AA2024 and 2 mm thick high carbon steel were chosen as the base materials, whose chemical and mechanical properties are presented in Tables 1 and 2, respectively. Samples were cut into the required size (25 mm width and 75 mm length) using a doall machine followed by cleaning burrs and removed by the buffing wheel. The samples were washed with acetone to remove the scale and rust formation on the piece. Table 3 presents the feasible range of each process parameter. The impact of primary process parameters on shear fracture load of AA2024/HCS dissimilar materials was evaluated. In this work, the following process parameters such as diameter ratio (shoulder to pin diameter) (D), rotational speed (R), plunge rate (R), and dwell time (T) were identified from the previous work. The feasible range of each process parameter was fixed based on the joint that would get free from visual defects.
The lower limit and upper limit of each process parameter were set as +2 and -2, respectively [16]. The intermediate value of each process parameter was calculated using the below mentioned equation: Table 4 shows the specified process parameters together with their limitations. Table 5 displays the chosen design matrix. The microstructure of base materials is shown in Figures 1(a) and 1(b). Similarly, the photograph of the welding machine is shown in Figure 1(c). Super HSS material was used to make tools with five different shoulder diameters (Figure 1(d)). The diameter and length of the pins were both kept at 5 mm. On the pin, a tapered threaded (left hand) profile was created. With the use of an automatic controlled FSW machine, all of the trials were carried out under the circumstances stipulated by the design matrix. Aluminum test coupon was kept at the bottom, and steel test coupon was placed on the top sheet. The photograph of the fabricated joint before testing and after testing is shown in Figures 1(e) and 1(f), respectively.

Development of Empirical Relationship
TSFL response (Y) of Al/steel FSSW joints (Equation (2)) may be described as a function of N, R, T, and D.
The chosen factor and its influence are presented in the The values of these coefficients were calculated using Design Expert 9.1. The final empirical connection to predict TSFL was built using these coefficients once the coefficients were determined [17], and the generated empirical relationship is shown in the following equation: The appropriateness of the generated empirical  Journal of Nanomaterials relationship was examined using the analysis of variance (ANOVA) approach [18]. The ANOVA findings are shown in Table 6. The model has an F value of 185.56, indicating that it is noteworthy. The F value of a model this big has a 0.01% probability of occurring due to noise. The model terms are important if the "Prob > F" value is less than 0.050. N, R, T, D, TN, TR, DR, DT, R 2 , N 2 , T 2 , and D 2 are important model terms in this situation. The corrected R 2 value of is equally high, at 0.97, indicating the model's high relevance. The corrected R 2 of 0.97 agrees reasonably with the expected R 2 of 0.94, showing that the model may be utilized to forecast the TSFL. The S-N ratio is used to determine adequate accuracy, and a ratio of more than 4 is preferred. Because this model's precession is 34.714. The observed and projected response values are nearly identical, indicating a near-perfect match of the derived empirical connection. Fabricating FSSW joints with three random combinations of parameters in the test range validates the proposed empirical connection; the actual response was determined as the average of three measured results. The validation findings indicated that the empirical connection created is extremely accurate, with a forecast variation of less than 5% (Table 7).

Optimizing FSSW Parameters
The mechanical and metallurgical qualities of the joints are influenced by FSSW process parameters such as N, R, T, and D. In order to achieve exceptional mechanical qualities, the FSSW process parameters must be optimized. RSM is one of the most effective approaches for optimizing the FSSW process parameters. RSM [19] is a set of mathematical and statistical models that may be used to investigate and simulate engineering challenges [20]. To graphically depict the region of best factor settings, a contour map is created.

Journal of Nanomaterials
The contour plots' characteristic circular mound form indicates that the elements are more likely to be interdependent [21]. A plot like this for second-order response surfaces might be more complicated than a simple set of parallel lines for first-order models. It is frequently important to define the response surface in the immediate region of the stationary point after it has been located. Characterization involves deciding if the discovered stationary point is the greatest, lowest, or saddle point. A contour plot is used to discover this. In the examination of the response surface, contour plots are quite useful. The optimum is determined with reasonable precision by defining the form of the surface using contour plots generated with response surface analysis software. If a circular contour patterning occurs, it likely to imply factor independence, but elliptical contours may show factor interactions. The forecasting model' response surfaces were created by taking two middle-level parameters and putting them on the "X"and "Y"-axes, with the response plotted on the "Z"-axis. We can see the ideal response point on the response surfaces. The contour plots and response graphs for the model developed for the FSSW of 2024-T3 with carbon steel alloy are shown in Figures 2 and 3.

Analysis of Contour Plots and Response Surface Plots
The contour plot in Figure 2 clearly shows the beneficial interaction impact of tool rotational speed and plunge rate on tensile shear failure load (a). Changes in the tensile shear failure load are more sensitive to changes in tool rotating speed than  Journal of Nanomaterials to changes in dwell time, as seen in the contour plot in Figure 2(b). Despite the virtually circular shape of Figure 2(c), there is a little interaction between tool rotating speed and tool diameter ratio, and it is believed that dwell time has a bigger impact on TSFL than tool rotational speed. As seen in the contour plot (Figure 2), dwell duration has a stronger impact on TSFL than plunge rate. The interaction effects between the parameters, plunge rate, and tool diameter ratio, on tensile shear failure load are also substantial, as shown in the contour plot Figure 2(e). As demonstrated in Figure 2, changes in dwell time are more sensitive to changes in TSFL than changes in tool diameter ratio. Figure 3 shows the three-dimensional response surface plots for the generated regression model's response (TSFL). The TSFL is shown by the apex of the response surface [22]. The TSFL increases with increasing tool rotational speed, plunge rate, and dwell duration to a certain value and subsequently declines, as shown in Figure 3. It is also noticed that increasing the tool diameter ratio initially raises the TSFL, but future increases have no meaningful influence on the TSFL. The highest attainable TSFL value is discovered to be 9.46 kN after examining the response surfaces and contour plots (Figures 2 and 3). With a tool speed of 999.21 rpm, a plunge rate of 3.91 mm/min, a dwell time of 4.98 seconds, and a tool diameter ratio of 3.01, achievers' optimization approach was validated by fabricating three more joints. Table 7 displays the welding settings as well as the TSFL findings.

Conclusions
The dissimilar materials such as AA2024 and HCS are welded successfully using FSSW. From the experimental investigation, the following conclusions are drawn:  Journal of Nanomaterials (1) The experiments were conducted using the design of experiments; four-factor, five-level central rotatable composite matrix was used (2) The joint welded with rotational tool speed, plunge depth, dwell time, and shoulder diameter to pin diameters was 1000 rpm, 4 mm/min, 5 sec, and 3, respectively (3) The significance of each process parameter was identified using ANOVA; from the analysis, dwell time is the primary influencing parameter, followed by plunge rate, shoulder diameter to pin diameter ratio, and rotational speed (4) The maximum tensile shear fracture load of FSSW dissimilar joints was found to be 9.46 kN (5) The joint yielded a higher TSFL value than other joints, which may be forming an intermetallic compound by optimum heat input

Data Availability
The data used to support the findings of this study are included within the article.