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Effect of deposition conditions on properties of nanostructured magnesium hydroxide powders

  • Inorganic Synthesis and Industrial Inorganic Chemistry
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Abstract

Change in the dispersity, microstructure, and adsorption properties of mesoporous magnesium hydroxide powders synthesized by the precipitation method from solutions upon introduction of surfactants and under the action of microwave and ultrasonic irradiation was studied. Highly dispersed nanostructured Mg(OH)2 powders were obtained with average sizes of primary and secondary particles of, respectively, 13–27 and 180–383 nm. The specific surface area, pore volume, and average pore diameter of the samples under study varied, depending on the preparation conditions, within the ranges 86–98 m2 g–1, 0.491–0.737 cm3 g–1, and 24–32 nm, respectively. It was shown that highly dispersed mesoporous magnesium hydroxide powders can be directionally synthesized by the precipitation method, which opens up wide opportunities for their application as nanoreactors for synthesis of nanosize isolated particles and development of poly-path catalysts on their basis.

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References

  1. Umar, A. and Hahn, Y.B., Metal Oxide Nanostructures and Their Applications, American Scientific Publishers, USA, 2010.

  2. Jun, Ch., Shuanghong, T., Jiang, L., and Ya, X., Appl. Catal., A, 2015, vol. 506, pp. 118–125.

    Article  Google Scholar 

  3. Selvama, N.C.S., Kumara, R.T., Kennedyb, L.J., and Vijaya, J.J., J. Alloys Compd., 2011, vol. 509, pp. 9809–9815.

    Article  Google Scholar 

  4. Demirci, S., Öztürk, B., Yildirim, S., et al., Mater. Sci. Semi con d. Process., 2015, vol. 34, pp. 154-161.

    Google Scholar 

  5. Yu, J.C., Xu, A., Zhang, L., et al., J. Phys. Chem. B, 2004, vol. 108, pp. 64–70.

    Article  CAS  Google Scholar 

  6. Rizwan, W., Ansari, S.G., Dar, M.A., et al., Mater. Sci. Forum, 2007, vols. 558–559, pp. 983–986.

    Google Scholar 

  7. Zeyneb, C., Sema, E., and Sabriye, Y., Environ. Prog. Sustainable Energy, 2012, vol. 31, no. 4, pp. 536–543.

    Article  Google Scholar 

  8. Sergeev, G.B., Nanokhimiya (Nanochemistry), Moscow Mosk. Gos. Univ., 2003.

    Google Scholar 

  9. Bindhu, M.R., Umadevi, M., Michea, M. Kavin, et al., Mater. Lett., 2016, vol. 166, pp. 19–22.

    Article  CAS  Google Scholar 

  10. Kumari, L., Li, W.Z., Vannoy, Ch.H., et al., Ceram. Int., 2009, vol. 35, pp. 3355–3364.

    Article  CAS  Google Scholar 

  11. Saoud, Kh.M., Saeed, Sh., Al-Soubaihi, R.M., and Bertino, M.F., Am. J. Nanomater., 2014, vol. 2, no. 2, pp. 21–25.

    CAS  Google Scholar 

  12. RF Patent 2 561 379 C2 (publ. 2015).

  13. Matthews, J.S., Just, O., Obi-Johnson, B., and Rees, W.S., Chem. Vap. Deposition, 2000, vol. 6, pp. 129–132.

    Article  CAS  Google Scholar 

  14. Dhaouadi, H., Chaabane, H., and Touati, F., Nano-Micro Lett., 2011, vol. 3 (3), pp. 153–159.

    Article  CAS  Google Scholar 

  15. Ding, Y., Zhang, G., and Wu, H., Chem. Mater., 2001, vol. 13 (2), pp. 435–440.

    Article  CAS  Google Scholar 

  16. Yu, J.C., Xu, A., Zhang, L., et al., J. Phys. Chem. B, 2004, vol. 108, pp. 64–70.

    Article  CAS  Google Scholar 

  17. Almjasheva, O.V., Smirnov, A.V., Fedorov, B.A., et al., Russ. J. Gen. Chem., 2014, vol. 84, no. 5, pp. 804–809.

    Article  CAS  Google Scholar 

  18. Komlev, A.A. and Vilezhaninov, E.F., Russ. J. Appl. Chem., 2013, vol. 86, no. 9, pp. 1344–1351.

    Article  CAS  Google Scholar 

  19. Komlev, A.A. and Gusarov, V.V., Inorg. Mater., 2014, vol. 50, no. 12, pp. 1247–1251.

    Article  CAS  Google Scholar 

  20. Nguyen, A.T., Mittova, I.Ya., Solodukhin, D.O., et al., Russ. J. Inorg. Chem., 2014, vol. 59, no. 2, pp. 40–45.

    Article  CAS  Google Scholar 

  21. Al-Hazmi, F., Umar, Ah., Dar, G.N., et al., J. Alloys Compd., 2012, vol. 519, pp. 4–8.

    Article  CAS  Google Scholar 

  22. Yousefi, M., J. Nanostruct., 2014, vol. 4, pp. 383–388.

    Google Scholar 

  23. Khue, D., Yan, X., and Wang, L., Power Technol., 2009, vol. 191, pp. 98-106.

  24. Frolov, Yu.G. and Grodskii, A.S., Laboratornye raboty i zadachi po kolloidnoi khimii (Laboratory Practicals and Tasks in Colloid Chemistry), Moscow Khimiya, 1986.

    Google Scholar 

  25. Kirillova, S.A., Smirnov, A.V., Fedorov, B.A., et al., Nanosist.: Fiz., Khim., Mat., 2012, vol. 3, no. 4, pp. 101–113.

    Google Scholar 

  26. Powder Diffraction File, Swarthmore: Joint Committee on Powder Diffraction Standard: Card no. 00-007-0239.

  27. Ghanbari, D., Salavati-Niasari, M., and Sabet, M., Composites, Part B, 2013, vol. 45, pp. 550–555.

    Article  CAS  Google Scholar 

  28. Gholamian, F., Salavati-Niasari, M., Ghanbari, D., and Sabet, M., J. Cluster Sci., 2013, vol. 24, pp. 73–84.

    Article  CAS  Google Scholar 

  29. Komarov, V.S., Nauchnye osnovy sinteza adsorbentov (Scientific Foundations of Adsorbent Syntheses), Minsk: Belarus. Navuka, 2013, p. 93.

    Google Scholar 

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Authors and Affiliations

  1. Institute of General and Inorganic Chemistry, National Academy of Sciences of Belarus, ul. Surganova 9, Minsk, 220072, Belarus

    I. V. Matsukevich, A. N. Ruchets, N. P. Krut’ko, V. V. Vashuk & T. F. Kuznetsova

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  1. I. V. Matsukevich
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  2. A. N. Ruchets
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  3. N. P. Krut’ko
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  4. V. V. Vashuk
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  5. T. F. Kuznetsova
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Correspondence to I. V. Matsukevich.

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Original Russian Text © I.V. Matsukevich, A.N. Ruchets, N.P. Krut’ko, V.V. Vashuk, T.F. Kuznetsova, 2017, published in Zhurnal Prikladnoi Khimii, 2017, Vol. 90, No. 1, pp. 3−9.

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Matsukevich, I.V., Ruchets, A.N., Krut’ko, N.P. et al. Effect of deposition conditions on properties of nanostructured magnesium hydroxide powders. Russ J Appl Chem 90, 1–6 (2017). https://doi.org/10.1134/S1070427217010013

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  • DOI: https://doi.org/10.1134/S1070427217010013

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