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Template-Free Synthesis of Hierarchical Zeolite ZSM-5

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Abstract

The influence of the conditions of template-free, seed-assisted synthesis of hierarchical ZSM-5 zeolite on its crystallinity, particle morphology, and texture has been studied. A method for the synthesis of a hierarchical zeolite, which makes it possible to reduce the template consumption three times, has been proposed.

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REFERENCES

  1. D. P. Serrano and R. van Grieken, J. Mater. Chem. 11, 2391 (2001).

    Article  CAS  Google Scholar 

  2. W. Vermeiren and J. P. Gilson, Top. Catal. 52, 1131 (2009).

    Article  CAS  Google Scholar 

  3. L. Tosheva and V. P. Valtchev, Chem. Mater. 17, 2494 (2005).

    Article  CAS  Google Scholar 

  4. J. Pérez-Ramírez, C. H. Christensen, K. Egeblad, et al., Chem. Soc. Rev. 37, 2530 (2008).

    Article  CAS  PubMed  Google Scholar 

  5. T. O. Drews and M. Tsapatsis, Curr. Opin. Colloid Interface Sci. 10, 233 (2005).

    Article  CAS  Google Scholar 

  6. W. Schwieger, A. G. Machoke, T. Weissenberger, et al., Chem. Soc. Rev. 45, 3353 (2016).

    Article  CAS  PubMed  Google Scholar 

  7. C. Dai, A. Zhang, M. Liu, X. Guo, C. Song, Adv. Funct. Mater. 25, 7479 (2015).

    Article  Google Scholar 

  8. A. H. Janssen, A. J. Koster, and K. P. de Jong, Angew. Chem. Int. Ed. 40, 1102 (2001).

    Article  CAS  Google Scholar 

  9. W. Yu, L. Deng, P. Yuan, et al., Chem. Eng. J. 270, 450 (2015).

    Article  CAS  Google Scholar 

  10. M. Ogura, S.-Y. Shinomiya, J. Tateno, et al., Chem. Lett. 29, 882 (2000).

    Article  Google Scholar 

  11. C. Martinez and A. Corma, Coord. Chem. Rev. 255, 1558 (2011).

    Article  CAS  Google Scholar 

  12. D. P. Serrano and P. Pizarro, Chem. Soc. Rev. 42, 4004 (2013).

    Article  CAS  PubMed  Google Scholar 

  13. H. Zhang, K. Song, L. Wang, et al., ChemCatChem 5, 2874 (2013).

    Article  CAS  Google Scholar 

  14. H. Zhang, Y. Ma, K. Song, et al., J. Catal. 302, 115 (2013).

    Article  CAS  Google Scholar 

  15. K. Itabashi, Y. Kamimura, K. Iyoki, et al., J. Am. Chem. Soc. 134, 11 542 (2012).

    Article  CAS  Google Scholar 

  16. H. Chen, Y. Wang, F. Meng, et al., RSC Adv. 6, 76642 (2016).

    Article  CAS  Google Scholar 

  17. N. Ren, Z. J. Yang, X. C. Lv, et al., Microporous Mesoporous Mater. 131, 103 (2010).

    Article  CAS  Google Scholar 

  18. K. V. Agrawal, B. Topuz, T. C. T. Pham, et al., Adv. Mater. 27, 3243 (2015).

    Article  CAS  PubMed  Google Scholar 

  19. D. Wang, X. Li, Z. Liu, et al., J. Colloid Interface Sci. 350, 290 (2010).

    Article  CAS  PubMed  Google Scholar 

  20. K. J. Chao, T. C. Tasi, and M. S. Chen, J. Chem. Soc., Faraday Trans. 1 77, 547 (1981).

    Article  CAS  Google Scholar 

  21. C. S. Cundy and P. A. Cox, Microporous Mesoporous Mater. 82, 1 (2005).

    Article  CAS  Google Scholar 

  22. G. Majano, A. Darwiche, S. Mintova, and V. Valtchev, Ind. Eng. Chem. Res. 48, 7084.

  23. M. Chareonpanich, T. Namto, P. Kongkachuichay, and J. Limtrakul, Fuel Process. Technol. 85, 1623 (2004).

    Article  CAS  Google Scholar 

  24. A. E. Persson, B. J. Schoeman, J. Sterte, and J. E. Otterstedt, Appl. Spectrosc. 14, 557 (1994).

    CAS  Google Scholar 

  25. H. Van Koningsveld, H. van Bekkum, and J. C. Jansen, Acta Crystallogr. 43, 127 (1987).

    Article  Google Scholar 

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ACKNOWLEDGMENTS

The authors would like to thank N.A. Alekseeva, A.A. Leonova, and N.A. Rudina for assistance in the analysis of samples.

Funding

This work was supported by the Ministry of Science and Higher Education of the Russian Federation, project no. АААА-А17-117041710077-4.

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Authors and Affiliations

  1. Novosibirsk State University, 630090, Novosibirsk, Russia

    D. O. Shestakova, K. A. Sashkina & E. V. Parkhomchuk

  2. Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, 630090, Novosibirsk, Russia

    D. O. Shestakova, K. A. Sashkina & E. V. Parkhomchuk

Authors
  1. D. O. Shestakova
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  2. K. A. Sashkina
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  3. E. V. Parkhomchuk
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Corresponding author

Correspondence to D. O. Shestakova.

Additional information

Translated by E. Boltukhina

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Shestakova, D.O., Sashkina, K.A. & Parkhomchuk, E.V. Template-Free Synthesis of Hierarchical Zeolite ZSM-5. Pet. Chem. 59, 838–844 (2019). https://doi.org/10.1134/S0965544119080188

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  • DOI: https://doi.org/10.1134/S0965544119080188

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