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X-Ray Diffraction Study of 8-(Pyridin-2-yl)- and 8-(1,2,4-Triazin-5-yl)-2H-chromen-2-ones

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Abstract

The molecular and crystal structures of 8-(3,6-diphenylpyridin-2-yl)-5,7-dimethoxy-4-phenyl-2H-chromen-2-one, 8-(3,6-diphenylpyridin-2-yl)-5,7-dimethoxy-4-propyl-2H-chromen-2-one, and 8-(3,6-diphenyl-1,2,4-triazin-5-yl)-5,7-dimethoxy-4-methyl-2H-chromen-2-one have been studied by X-ray analysis. Intermolecular interactions in crystal and their effect on the crystal structure have been analyzed.

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Funding

This study was performed under financial support by the Russian Science Foundation (project no. 21-73-00214; synthesis of 4a and 4b) and by the Council for Grants at the President of the Russian Federation (project no. NSh-1223.2022.1.3; synthesis of 4c and X-ray analysis), as well as in the framework of state assignment no. 0398-2019-0005 AAAAA19-119012290117-6 using the equipment of the Spectroscopy and Analysis of Organic Compounds joint center.

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Authors and Affiliations

  1. Postovskii Institute of Organic Synthesis, Ural Branch, Russian Academy of Sciences, 620990, Yekaterinburg, Russia

    P. A. Slepukhin, M. I. Valieva, E. S. Starnovskaya, I. A. Khalymbadzha, D. S. Kopchuk, G. V. Zyryanov & O. N. Chupakhin

  2. Ural Federal University, 620002, Yekaterinburg, Russia

    P. A. Slepukhin, R. F. Fatykhov, A. D. Sharapov, M. I. Valieva, E. S. Starnovskaya, I. A. Khalymbadzha, D. S. Kopchuk, G. V. Zyryanov & O. N. Chupakhin

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  1. P. A. Slepukhin
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  2. R. F. Fatykhov
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  3. A. D. Sharapov
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  4. M. I. Valieva
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  5. E. S. Starnovskaya
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  6. I. A. Khalymbadzha
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  7. D. S. Kopchuk
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  8. G. V. Zyryanov
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  9. O. N. Chupakhin
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Corresponding author

Correspondence to G. V. Zyryanov.

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Slepukhin, P.A., Fatykhov, R.F., Sharapov, A.D. et al. X-Ray Diffraction Study of 8-(Pyridin-2-yl)- and 8-(1,2,4-Triazin-5-yl)-2H-chromen-2-ones. Russ J Gen Chem 92, 1285–1289 (2022). https://doi.org/10.1134/S1070363222070179

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