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Specific features of preparation of dense ceramic based on barium zirconate

  • Amorphous, Vitreous, and Organic Semiconductors
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Abstract

In the present work the BaZr0.8Y0.2O3 − δ samples were synthesized by traditional ceramic (solid-state method), citrate-nitrate methods as well as co-precipitation of hydroxides. Among them, the citrate-nitrate combustion method was found to be the optimal one because the obtained powder calcined at 1150°C is single-phase and characterized by high dispersion. It is shown that the transition from solid-state method to wet chemical ones promotes the decrease of the powder particle size from ∼680 nm to 75 nm, respectively. However, at the same time the relative densities of the samples sintered at 1450°C do not exceed the 67%. The dense ceramic (90.2%) was obtained by combination of the citrate-nitrate method and the addition of 1 wt % Co3O4 as a sintering aid to the precursors.

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Authors and Affiliations

  1. Institute of High-Temperature Electrochemistry, Ural Branch, Russian Academy of Sciences, Yekaterinburg, 620990, Russia

    Yu. G. Lyagaeva, D. A. Medvedev, A. K. Demin, T. V. Yaroslavtseva, S. V. Plaksin & N. M. Porotnikova

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  1. Yu. G. Lyagaeva
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  2. D. A. Medvedev
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  3. A. K. Demin
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  4. T. V. Yaroslavtseva
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  5. S. V. Plaksin
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  6. N. M. Porotnikova
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Corresponding author

Correspondence to D. A. Medvedev.

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Original Russian Text © Yu.G. Lyagaeva, D.A. Medvedev, A.K. Demin, T.V. Yaroslavtseva, S.V. Plaksin, N.M. Porotnikova, 2014, published in Fizika i Tekhnika Poluprovodnikov, 2014, Vol. 48, No. 10, pp. 1388–1393.

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Lyagaeva, Y.G., Medvedev, D.A., Demin, A.K. et al. Specific features of preparation of dense ceramic based on barium zirconate. Semiconductors 48, 1353–1358 (2014). https://doi.org/10.1134/S1063782614100182

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  • DOI: https://doi.org/10.1134/S1063782614100182

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