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Low-Voltage Scanning Electron Microscopy and Energy-Dispersive X-Ray Microanalysis of the Interface of Multilayer Polymer Composite

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Abstract

The morphology of the layer of polyelectrolyte complex, which is formed in the composite based on chitosan and sulfoethyl cellulose during the contact of a solution of one of them with a gel film of the other one, has been investigated by the low-voltage (≤3 kV) scanning electron microscopy. A technique for eliminating the effects related to charge accumulation on the dielectric film surface is proposed.

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Reference

  1. J. Goldstein, Scanning Electron Microsc. X-Ray Microanal. 44, 684 (2003).

    Google Scholar 

  2. W. C. Lane, Scanning Electron Microsc. 1970, 297 (1970).

    Google Scholar 

  3. F. Crocolo and C. Riccardi, Microsc. Today 40 (2008).

  4. T. Michael, H. Meng, V. Martin, et al., Key Engin. Mater. 471, 309 (2011).

    Google Scholar 

  5. D. E. Newbury and N. W. M. Ritchie, J. Mater. Sci. 50 (2), 493 (2015).

    Article  ADS  Google Scholar 

  6. A. S. Orekhov, V. V. Klechkovskaya, and S. V. Kononova, Crystallogr. Rep. 62 (5), 710 (2017).

    Article  ADS  Google Scholar 

  7. G. M. Kuzmicheva, A. A. Gainanova, A. S. Orekhov, et al., Crystallogr. Rep. 59 (6), 916 (2014).

    Article  ADS  Google Scholar 

  8. Y. G. Baklagina, S. V. Kononova, V. A. Petrova, et al., Crystallogr. Rep. 58 (2), 287 (2013).

    Article  ADS  Google Scholar 

  9. S. V. Kononova, E. V. Kruchinina, V. A. Petrova, et al., Molecules 22 (12), 2227 (2017).

    Article  Google Scholar 

  10. S. V. Kononova, A. V. Volod’ko, V. A. Petrova, et al., Carbohydr. Polym. 181, 86 (2018).

    Article  Google Scholar 

  11. Casino v.2.42 Simulation. https://doi.org/www.gel.usherbrooke.ca/casino/index.html.

  12. K. I. Dragnevski, A. M. Donald, S. M. Clarke, et al., Colloids Surf. A: Physicochem. Eng. Aspects. 337, 47 (2009).

    Article  Google Scholar 

  13. V. A. Petrova, A. S. Orekhov, D. D. Chernyakov, et al., Crystallogr. Rep. 61 (6), 945 (2016).

    Article  ADS  Google Scholar 

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Authors and Affiliations

  1. Shubnikov Institute of Crystallography, Federal Scientific Research Centre “Crystallography and Photonics,”, Russian Academy of Sciences, Moscow, 119333, Russia

    A. S. Orekhov, N. A. Arkharova & V. V. Klechkovskaya

  2. National Research Centre “Kurchatov Institute”, Moscow, 123182, Russia

    A. S. Orekhov

  3. Institute of Macromolecular Compounds, Russian Academy of Sciences, St. Petersburg, 199004, Russia

    S. V. Kononova

Authors
  1. A. S. Orekhov
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  2. N. A. Arkharova
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  3. S. V. Kononova
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  4. V. V. Klechkovskaya
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Corresponding author

Correspondence to V. V. Klechkovskaya.

Additional information

Original Russian Text © A.S. Orekhov, N.A. Arkharova, S.V. Kononova, V.V. Klechkovskaya, 2018, published in Kristallografiya, 2018, Vol. 63, No. 5, pp. 730–733.

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Orekhov, A.S., Arkharova, N.A., Kononova, S.V. et al. Low-Voltage Scanning Electron Microscopy and Energy-Dispersive X-Ray Microanalysis of the Interface of Multilayer Polymer Composite. Crystallogr. Rep. 63, 745–748 (2018). https://doi.org/10.1134/S1063774518050206

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  • DOI: https://doi.org/10.1134/S1063774518050206

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