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Hydrothermal Synthesis of Hierarchical CoMoO4 Nanostructures

  • SYNTHESIS AND PROPERTIES OF INORGANIC COMPOUNDS
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Abstract

The formation of CoMoO4 anisotropic nanostructures has been studied with a combination of programmed co-precipitation of metal hydroxides and the hydrothermal method. The thermal behavior, phase composition, and microstructure features of the obtained nanopowder have been investigated. Using a set of physicochemical methods of analysis, it has been shown that the proposed synthesis conditions make it possible to form a single-phase nanodispersed (average CSR size of about 30 ± 3 nm) oxide with a monoclinic spinel-type structure (space group C2/m) that does not contain impurity inclusions.

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ACKNOWLEDGMENTS

X-ray powder diffraction studies and SEM studies were carried out using the equipment of the Center for Collective Use of the Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences.

Funding

This work was partially supported by a Scholarship of the President of the Russian Federation for young scientists and graduate students (project SP-2407.2019.1, synthesis of nanostructures of the CoMoO4 composition) and the Ministry of Science and Higher Education of the Russian Federation within the framework of the State Assignment of the Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences (study of the microstructural characteristics of the obtained nanopowder).

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia

    T. L. Simonenko, V. A. Bocharova, N. P. Simonenko, E. P. Simonenko, V. G. Sevastyanov & N. T. Kuznetsov

  2. Mendeleev University of Chemical Technology of Russia, 125047, Moscow, Russia

    V. A. Bocharova

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  1. T. L. Simonenko
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  2. V. A. Bocharova
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  3. N. P. Simonenko
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  4. E. P. Simonenko
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  5. V. G. Sevastyanov
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  6. N. T. Kuznetsov
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Correspondence to T. L. Simonenko.

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Translated by V. Avdeeva

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Simonenko, T.L., Bocharova, V.A., Simonenko, N.P. et al. Hydrothermal Synthesis of Hierarchical CoMoO4 Nanostructures. Russ. J. Inorg. Chem. 66, 1633–1638 (2021). https://doi.org/10.1134/S0036023621110176

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