Abstract
Transmission electron microscopy and electron back-scattered diffraction (EBSD) analysis have been used to study the microstructure of the YBa2Cu3O6.8 compound, which is formed during low-temperature heat treatment in a humid atmosphere and after restoring annealing at T = 930°C. It has been shown that structural defects formed after annealing at 200°C remain after short annealing at 930°C and can serve as pinning centers that favor the improvement of critical characteristics of the material. The restoration of the initial structure is accompanied by the recrystallization of the material.
Similar content being viewed by others
References
J. Kulik, “Defect structures in YBa2Cu3O7 − δ with enhanced pinning at low fields,” J. Appl. Phys. 70, 4398–4408 (1991).
E. D. Specht, A. Goyal, J. Li, P. M. Martin, X. Li, and M. W. Rupich, “Stacking faults in YBa2Cu3O7 − x : Measurement using X-ray diffraction and effects on critical current,” Appl. Phys. Lett. 89, 162510 (2006).
P. X. Zhang, L. Zhou, P. Ji, W. M. Bian, X. Z. Wu, and Z. H. Lai, “The effect of annealing on stacking faults and Jc values of PMP processed YBCO,” Supercond. Sci. Technol. 8, 15–19 (1995).
T. Prikhna, M. Eisterer, H. W. Weber, W. Gawalek, X. Chaud, V. Sokolovsky, V. Moshchil, A. Kozyrev, V. Sverdun, R. Kuznietsov, T. Habisreuther, M. Karpets, V. Kovylaev, J. Noudem, J. Rabier, A. Joulain, W. Goldacker, T. Basyuk, V. Tkach, J. Dellith, C. Schmidt, and A. Shaternik, “Pinning in MgB2- and YBaCuO-based superconductors: Effect of manufacturing pressure and temperature,” IEEE Transact. Appl. Supercond. 23(3), 8001605 (2013).
V. Yu. Monarkha, V. A. Pashchenko, and V. P. Timofeev, Low density flux pinning in YBCO single crystals, ArXiv.org/pdf/1211.5895
M. Murakami, H. Fujimoto, K. Yamaguchi, N. Nakamura, N. Koshizuka, and S. Tanaka, “Flux pinning sites in melt-processed YBaCuO superconductors,” Phase Transition 41, 69–78 (1993).
Yu. I. Kuz’min, “Resistive state of superconducting structures with fractal clusters of a normal phase,” Phys. Solid State 43, 1199–1206 (2001).
S. V. Sudareva, E. I. Kuznetsova, T. P. Krinitsina, I. B. Bobylev, V. N. Morycheva, L. V. Zherdeva, and E. P. Romanov, “Influence of low-temperature annealing on the structure and superconducting properties of YBa2Cu3O7 − δ compound with different oxygen stoichiometries,” Phys. Met. Metallogr. 75, 199–204 (1993).
S. V. Sudareva, E. I. Kuznetsova, T. P. Krinitsina, I. B. Bobylev, E. P. Romanov, “On the nature of tweed contrast in Y-Ba-Cu-O system,” Phys. Met. Metallogr., 77, 513–517 (1994).
E. I. Kuznetsova, T. P. Krinitsina, S. V. Sudareva, I. B. Bobylev, E. P. Romanov, “Effect of oxygen content and low-temperature annealing on the evolution of fine structure of YBa2Cu3O7 − δ compound,” Phys. Met. Metallogr. 81, 429–435 (1996).
I. B. Bobylev, E. G. Gerasimov, and N. A. Zyuzeva, “Effect of low-temperature annealing on the critical parameters of highly textured YBa2Cu3Oy,” Phys. Solid State 54, 1741–1746 (2012).
I. B. Bobylev and N. A. Zyuzeva, “Effect of water vapor and low-temperature decomposition on the structure and electrophysical properties of nonstoichiometric compound YBa2Cu3O7 − δ,” Phys. Met. Metallogr. 112, 127–132 (2011).
I. B. Bobylev, E. I. Kuznetsova, N. A. Zyuzeva, T. P. Krinitsina, S. V. Sudareva, and E. P. Romanov, “Effect of the atmosphere of low-temperature annealing on the structure and electrophysical properties of nonstoichiometric YBa2Cu3O7 − δ ceramics,” Phys. Met. Metallogr. 110, 378–385 (2010).
I. B. Bobylev, N. A. Zyuzeva, and E. P. Romanov, “Electrophysical properties and the structure of the YBa2Cu3Oy compound thermally restored after low-temperature decomposition,” Phys. Solid State 52, 1338–1341 (2010).
I. B. Bobylev, E. G. Gerasimov, and N. A. Zyuzeva, “Effect of double annealing on the critical parameters of highly textured YBa2Cu3O6.9,” J. Exper. Theor. Phys. 115, 474–479 (2012).
I. B. Bobylev and N. A. Zyuzeva, “Effect of low-temperature treatment and subsequent high-temperature annealing on the critical current density of YBa2Cu3Oy,” Phys. Solid State 54, 1332–1335 (2012).
M. Murakami, N. Sakai, T. Higuchi, and S. I. Yooz, “Melt-processed light rare earth element-Ba-Cu-O,” Supercond. Sci. Technol. 9, 1015–1032 (1996).
S. V. Sudareva, E. P. Romanov, T. P. Krinitsina, E. I. Kuznetsova, Yu. V. Blinova, I. B. Bobylev, N. A. Zyuzeva, and A. M. Burkhanov, “Fine structure and the mechanism of the low-temperature decomposition of the nonstoichiometric compounds YBa2Cu3O6.8 and YBa2Cu3O6.8 doped with Ce,” Phys. Metal Metallogr. 106, 364–373 (2008).
Yu. V. Blinova, S. G. Titova, S. V. Sudareva, and E. P. Romanov, “Mechanism of thermal decomposition of the nonstoichiometric compound YBa2Cu3O6.8,” Phys. Solid State 51, 1099–1104 (2009).
S. G. Titova, Yu. V. Blinova, S. V. Sudareva, I. B. Bobylev, and N. A. Zyuzeva, “Thermal stability of nonstoichiometric ceramic YBa2Cu3O6.8 at 200 C in a dried air,” Phys. Solid State 53, 455–457 (2011).
I. B. Bobylev, N. A. Zyuzeva, S. V. Sudareva, and E. P. Romanov, “Effect of the oxygen partial pressure on the kinetics of decomposition of the Ba2YCu3O7 − δ phase at temperatures <400°C,” Phys. Met. Metallogr. 103, 401–406 (2007).
Yu. I. Kuz’min, I. V. Pleshakov, and S. V. Razumov, “The statistical distribution of magnetic critical currents determined by HTSC film morphology,” Phys. Solid State 41, 1594–1597 (1999).
Yu. I. Kuz’min, “Vortex glass state in superconductors with fractal clusters of normal phase,” Tech. Phys. Lett. 36, 400–403 (2010).
R. Zhao, M. J. Goringe, S. Myhra, and P. S. Turner, “Transmission electron microscopy and high-resolution transmission electron microscopy studies of the early stages in the degradation of YBa2Cu3O7 − δ superconductor in water vapor,” Philos. Mag. A 66, 491–506 (1992).
F. Sandiumenge, B. Martinez, and X. Obradors, “Tailoring of microstructure and critical currents in directionally solidified YBa2Cu3O7 − x ,” Supercond. Sci. Technol. A 10, 93–119 (1997).
S. Dziaszyk, E. J. Payton, F. Friedel, V. Marx, and G. Eggeler, “On the characterization of recrystallized fraction using electron backscatter diffraction: A direct comparison to local hardness in an IF steel using nanoindentation,” Mater. Sci. Eng., A 527, 7854–7864 (2010).
D. P. Field, L. T. Bradford, M. M. Nowell, and T. M. Lillo, “The role of annealing twins during recrystallization of Cu,” Acta Mater., 55, 4233–4241 (2007).
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © E.I. Kuznetsova, T.P. Krinitsina, I.B. Bobylev, N.A. Zyuzeva, E.P. Romanov, 2014, published in Fizika Metallov i Metallovedenie, 2014, Vol. 115, No. 8, pp. 846–852.
Rights and permissions
About this article
Cite this article
Kuznetsova, E.I., Krinitsina, T.P., Bobylev, I.B. et al. Microstructure of YBa2Cu3O6.8 after low-temperature annealing and subsequent restoration. Phys. Metals Metallogr. 115, 793–799 (2014). https://doi.org/10.1134/S0031918X14080092
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0031918X14080092