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Structure of the Os2S2Br4(4-CNPy)4 complex

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Abstract

The interaction of the quaternary thioselenobromide complex Os2S7Se5Br8 prepared by the reaction of OsO4 with a solution of sulfur in Se2Br2 at 100°C with melted 4-CNPy at 165°C leads to the formation of the Os2S2Br4(4-CNPy)4 complex whose structure is determined by single crystal X-ray diffraction.

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References

  1. Yu. V. Mironov, J. A. Cody, T. A. Albrecht-Schmitt, and J. A. Ibers, J. Am. Chem. Soc., 119, 493 (1997).

    Article  CAS  Google Scholar 

  2. N. G. Naumov, A. V. Virovets, N. V. Podberezskaya, and V. E. Fedorov, J. Struct. Chem., 38, No. 5, 857 (1997).

    Article  CAS  Google Scholar 

  3. Yu. V. Mironov, A. V. Virovets, N. G. Naumov, V. N. Ikorskii, and V. E. Fedorov, Chem. Eur. J., 6, No. 8, 1361 (2000).

    Article  CAS  Google Scholar 

  4. K. A. Brylev, A. V. Virovets, N. G. Naumov, Yu. V. Mironov, D. Fenske, and V. E. Fedorov, Russ. Chem. Bull., No. 7, 1140 (2001).

    Article  Google Scholar 

  5. S. V. Volkov, R. E. Gladyshevskii, Yu. V. Mironov, et al., Russ. J. Coord. Chem., 38, No. 3, 167 (2012).

    Article  CAS  Google Scholar 

  6. APEX2 (version 1.08), SAINT (version 7.03), SADABS (version 2.11), Bruker AXS Inc., Madison WI, USA (2004).

  7. G. M. Sheldrick, Acta Crystallogr. A, 64, 112 (2008).

    Article  CAS  Google Scholar 

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Correspondence to Yu. V. Mironov.

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Original Russian Text © 2015 S. A. Baranets, Yu. V. Mironov, A. I. Smolentsev, S. V. Volkov, L. B. Kharkova, O. G. Yanko.

Translated from Zhurnal Strukturnoi Khimii, Vol. 56, No. 6, pp. 1253–1255, November–December, 2015.

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Baranets, S.A., Mironov, Y.V., Smolentsev, A.I. et al. Structure of the Os2S2Br4(4-CNPy)4 complex. J Struct Chem 56, 1198–1200 (2015). https://doi.org/10.1134/S0022476615060293

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  • DOI: https://doi.org/10.1134/S0022476615060293

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