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Influence of the degree of deaggregation of YSZ nanopowders in suspension on the process of electrophoretic deposition

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Abstract

Deaggregated nonaqueous suspensions of ZrO2 nanopowders stabilized by Y2O3 (YSZ) with an average diameter of particles of 11 nm obtained by laser evaporation and condensation are studied using dynamic light scattering (DLS). Two types of suspensions with an average size of aggregates of 108 and 66 nm are obtained by ultrasonic machining (USM) and centrifugation. It is shown that the combination of USM and centrifugation allows us to obtain narrow size distributions for the particles in YSZ suspensions. Coatings are obtained using electrophoretic deposition (EPD) from two types of YSZ suspensions with different degrees of deaggregation, and it is shown that no difference in the structure and morphology of suspensions is observed. It is established that, by EPT of the particles, a mechanism of electrochemical coagulation is realized at the electrode from the suspensions with different degrees of deaggregation.

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References

  1. V. V. Osipov, Yu. A. Kotov, M. G. Ivanov, et al., “The way to apply powerful pulse-periodical CO2 laser with high efficiency for producing nanosized powders,” Izv. Akad. Nauk, Ser. Fiz. 63(10), 1968–1971 (1999).

    Google Scholar 

  2. Yu. A. Kotov, V. V. Osipov, M. G. Ivanov, et al., “Properties of oxide nanopowders prepared by target evaporation with a pulse-periodic CO2 laser,” Tech. Phys. 47(11), 1420 (2002).

    Article  Google Scholar 

  3. M. Ivanov, Yu. Kotov, V. Komarov, et al., “The way to synthesize nanopowders by powerful fiber ytterbium laser,” Fotonika, No. 3, 18–20 (2009).

    Google Scholar 

  4. Yu. A. Kotov, O. M. Samatov, M. G. Ivanov, et al., “Production and characteristics of composite nanopowders using a fiber ytterbium laser,” Tech. Phys. 56(5), 652 (2011).

    Article  Google Scholar 

  5. US Patent no. 6,887,361 B1 (2005).

  6. A. P. Safronov, D. V. Leiman, D. N. Blagodetelev, Yu. A. Kotov, A. V. Bagazeev, and A. M. Murzakaev, “Aggregation of air-dry alumina powder nanoparticles redispersed in an aqueous medium,” Nanotech. Russ. 5(11–12), 777 (2010).

    Article  Google Scholar 

  7. A. P. Safronov, E. G. Kalinina, Yu. A. Kotov, et al., “Nanopowders electrophoretic deposition onto porous surface,” Ross. Nanotekhnol. 1(1–2), 162–169 (2006).

    Google Scholar 

  8. E. G. Kalinina, “Physicochemical regulations of electrophoretic deposition for solid thin film ZrO2 electrolyte,” Extended Abstract of Candidate’s Dissertation in Chemical Sciences (Ural Federal Univ., Yekaterinburg, 2010), p. 23.

    Google Scholar 

  9. E. G. Kalinina, N. A. Lyutyagina, A. P. Safronov, and E. S. Buyanova, “Electrophoretic deposition of Y2O3-stabilized ZrO2 nanoparticles on the surface of dense La0.7Sr0.3MnO3 — δ cathodes produced by pyrolysis and solid-state reaction,” Inorg. Mater. 50(2), 184 (2014).

    Article  Google Scholar 

  10. Xu Zhigang, G. Rajaram, J. Sankar, et al., “Electroforetic deposition of YSZ electrolyte coatings for SOFCs,” Fuel Cells Bull., 12–16 (2007).

    Google Scholar 

  11. I. Corni, M. P. Ryan, and A. R. Boccaccini, “Electroforetic deposition: from traditional ceramics to nanotechnology,” J. Europ. Ceram. Soc., No. 28, 1353–1367 (2008).

    Google Scholar 

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Correspondence to E. G. Kalinina.

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Original Russian Text © E.G. Kalinina, N.A. Lyutyagina, D.V. Leiman, A.P. Safronov, 2014, published in Rossiiskie Nanotekhnologii, 2014, Vol. 9, Nos. 5–6.

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Kalinina, E.G., Lyutyagina, N.A., Leiman, D.V. et al. Influence of the degree of deaggregation of YSZ nanopowders in suspension on the process of electrophoretic deposition. Nanotechnol Russia 9, 274–279 (2014). https://doi.org/10.1134/S1995078014030069

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  • DOI: https://doi.org/10.1134/S1995078014030069

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