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Effect of synthesis parameters on characteristics of expanded graphite

  • Inorganic Synthesis and Industrial Inorganic Chemistry
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Abstract

Effect of synthesis parameters on the characteristics of expanded graphite were studied. The starting sample, intercalated graphite, was treated by several methods: thermal shock (400, 1000°C) and programmed heating (400–700°C). The samples were examined by scanning electron microscopy, energy-dispersive spectroscopy, X-ray diffraction analysis, and low-temperature nitrogen adsorption. The programmed-heating method yields better texture characteristics as compared with the thermal shock. The programmed-heating method was used to obtain high-quality expanded graphite with high specific surface area (299 m2 g–1) at a comparatively moderate temperature of 400°C.

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Authors and Affiliations

  1. Novosibirsk State Technical University, pr. Karla Marksa 20, Novosibirsk, 630073, Russia

    Yu. P. Steksova, I. S. Berdyugina, A. A. Shibaev, M. V. Popov & A. G. Bannov

  2. Institute of Solid-State Chemistry and Mechanochemistry, Siberian Branch, Russian Academy of Sciences, ul. Kutateladze 18, Novosibirsk, 630128, Russia

    A. V. Ukhina

  3. Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, ul. Akademika Lavrent’eva 3, Novosibirsk, 630090, Russia

    E. A. Maksimovskii

  4. Novosibirsk State University, Novosibirsk, Russia

    E. A. Maksimovskii

Authors
  1. Yu. P. Steksova
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  2. I. S. Berdyugina
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  3. A. A. Shibaev
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  4. A. V. Ukhina
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  5. E. A. Maksimovskii
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  6. M. V. Popov
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  7. A. G. Bannov
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Corresponding author

Correspondence to A. G. Bannov.

Additional information

Original Russian Text © Yu.P. Steksova, I.S. Berdyugina, A.A. Shibaev, A.V. Ukhina, E.A. Maksimovskii, M.V. Popov, A.G. Bannov, 2016, published in Zhurnal Prikladnoi Khimii, 2016, Vol. 89, No. 10, pp. 1265−1273.

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Steksova, Y.P., Berdyugina, I.S., Shibaev, A.A. et al. Effect of synthesis parameters on characteristics of expanded graphite. Russ J Appl Chem 89, 1588–1595 (2016). https://doi.org/10.1134/S1070427216100049

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  • DOI: https://doi.org/10.1134/S1070427216100049

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