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Synthesis of 2-substituted 3,4-bis(diethoxyphosphorylmethyl)furans

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Abstract

Bromination of ethyl 4-(diethoxyphosphorylmethyl)-5-methylfuran-2-carboxylate and 4-(diethoxyphosphorylmethyl)-5-methylfuran-2-carbonitrile with N-bromosuccinimide followed by phosphorylation via the Arbuzov reaction have yielded the corresponding 2-substituted 4,5-bis(diethoxyphosphorylmethyl)furans. Synthesis and transformations of bisphosphorylated 2-furoic acid and its derivatives are described.

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Authors and Affiliations

  1. St. Petersburg State Technological Institute (Technical University), Moskovskii pr. 26, St. Petersburg, 190031, Russia

    L. M. Pevzner

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  1. L. M. Pevzner
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Correspondence to L. M. Pevzner.

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Original Russian Text © L.M. Pevzner, 2015, published in Zhurnal Obshchei Khimii, 2015, Vol. 85, No. 2, pp. 255–262.

To the 80th Anniversary of B.I. Ionin

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Pevzner, L.M. Synthesis of 2-substituted 3,4-bis(diethoxyphosphorylmethyl)furans. Russ J Gen Chem 85, 428–435 (2015). https://doi.org/10.1134/S1070363215020139

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  • DOI: https://doi.org/10.1134/S1070363215020139

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