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Study on synthesis of superparamagnetic spinel cobalt ferrite nanoparticles as layered double hydroxides by co-precipitation method

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Abstract

Cobalt ferrite layered double hydroxide (LDH) nanoparticles with cubic structure were synthesized by the co-precipitation method: addition of NaOH solution to a solution of Co2+ and Fe3+. Formation of nanoparticles was confirmed by XRD, SEM, TEM, PSA, FT-IR, TGA, DSC, and magnetic characteristics were measured using VSM. Crystals produced by calcination at 900°C possessed high coercivity and pronounced physical and chemical stability. Nanoparticles of CoFe2O4 formed outer layers with poor crystallization on the surface of cobalt ferrite nanocrystals.

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Authors and Affiliations

  1. Fabrication Technology Department, Advanced Technology and New Materials Research Institute, City of Scientific Research and Technological Applications (SRTA-City), New Borg El-Arab City, P.O. Box 21934, Alexandria, Egypt

    H. A. Hamad & M. M. Abd El-latif

  2. Electronic Materials Department, Advanced Technology and New Materials Research Institute, City of Scientific Research and Technological Applications (SRTA-City), New Borg El-Arab City, P.O. Box 21934, Alexandria, Egypt

    A. B. Kashyout

  3. Materials Science Department, Institute of Graduate Studies and Research (IGSR), Alexandria University, 163 Horrya Avenue, P.O. Box 832, Shatby, 21526, Alexandria, Egypt

    W. A. Sadik & M. Y. Feteha

Authors
  1. H. A. Hamad
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  2. M. M. Abd El-latif
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  3. A. B. Kashyout
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  4. W. A. Sadik
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  5. M. Y. Feteha
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Correspondence to H. A. Hamad.

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Hamad, H.A., Abd El-latif, M.M., Kashyout, A.B. et al. Study on synthesis of superparamagnetic spinel cobalt ferrite nanoparticles as layered double hydroxides by co-precipitation method. Russ J Gen Chem 84, 2031–2036 (2014). https://doi.org/10.1134/S1070363214100296

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  • DOI: https://doi.org/10.1134/S1070363214100296

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