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Synthesis and crystal structure of nickel(II) complex based on 2-trifluoroacetylcycloalkanone benzoylhydrazones

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Abstract

The reaction of ethanol solutions of benzoylhydrazones of 2-trifluoroacetylcycloalkanones (H2L) with a solution of nickel(II) acetate in aqueous ammonia in 1 : 1 ratio gave complexes NiL · NH3 with square structure. The composition and structure of the complexes were determined by elemental analysis, IR and 1H NMR spectroscopy, and X-ray diffraction analysis.

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References

  1. Filyakova, V.I., Doctoral (Chem) Dissertation, Yekaterinburg: Inst. Organ. Synth., Ural Branch of the RAS, 1999.

  2. Nikonov, M.V., Chizhov, D.L., Ratner, V.G., and Pashkevich, K.I., J. Fluorine Chem., 2000, vol. 106, p. 115.

    Article  CAS  Google Scholar 

  3. Chekhlov, A.N. and Tkachev, V.V., Russ. J. Inorg. Chem., 2003, vol. 48, no. 7, p. 1031.

    Google Scholar 

  4. Umarov, B.B. Kuchkarova, R.R., et al., V Respubl. konf. molodykh khimikov “Problemy bioorganicheskoi khimii” (V Republ. Conf. of Young Scientists “Problems of Bioorganic Chemistry”), Namangan: NamGU, 2006, p. 7.

    Google Scholar 

  5. Perevalov, S.G., Cand. Sci. (Chem) Dissertation, Yekaterinburg: Ural State Technical University, 2000.

  6. Toshev, M.T., Yusupov, V.G., Dustov, Kh.B., and Parpiev, N.A., Kristallokhimiya kompleksov metallov s gidrazidami i gidrazonami (Crystal Chemistry of Metal Complexes with Hydrazides and Hydrazones), Tashkent: Fan, 1994.

    Google Scholar 

  7. Umarov, B.B., Doctoral (Chem) Dissertation, Tashkent: Uzbekistan Acad. Sci, 1996.

    Google Scholar 

  8. Gaibullaev, Kh.S., Pumpor, K.B., Yakimovich, S.I., et al., Abstracts of Papers, III Nats. konf. po primeneniyu rentgenovskogo, sinkhotronnogo izluchenii neitronov i elektronov “RSNE-2001” (III National Conf. on the Use of X-ray and Syncrotron Radiation of Neutrons and Electrons “RSNE-2001”), Moscow: IK RAN, 2001, p. 58.

    Google Scholar 

  9. Sheldrick, G.M., SHELXL-86. Program for the Solution of Crystal Structures, Göttingen (Germany): Univ. of Göttingen, 1986.

    Google Scholar 

  10. Sheldrick, G.M., SHELXL-93. Program for the Refinement of Crystal Structures, Göttingen (Germany): Univ. of Göttingen, 1997.

    Google Scholar 

  11. Toshev, M.T., Dustov, Kh.B., Saidov, S.O., et al., Koord. Khim., 1992, vol. 18, no. 12, p. 1184.

    CAS  Google Scholar 

  12. Umarov, B.B., Yakimovich, S.I., Zerova, I.V., et al., Abstracts of Papers, III Nats. konf. po primeneniyu rentgenovskogo, sinkhotronnogo izluchenii neitronov i elektronov “RSNE-2001” (III National Conf. on the Use of X-Ray and Syncrotron Radiation of Neutrons and Electrons “RSNE-2001”), Moscow: IK RAN, 2001, p. 162.

    Google Scholar 

  13. Umarov, B.B., Tursunov, M.A., Mardonov, U.M., et al., Abstracts of Papers, IV Nats. konf. po primeneniyu rentgenovskogo, sinkhotronnogo izluchenii neitronov i elektronov dlya issledovaniya materialov “RSNE-2003” (IV National Conf. on the Use of X-Ray and Syncrotron Radiation of Neutrons and Electrons for Material Research “RSNE-2003”), Moscow: IK RAN, 2003, p. 171.

    Google Scholar 

  14. Pakal’nis, V.V., Zerova, I.V., and Yakimovich, S.I., Russ. J. Gen. Chem., 2007, vol. 77, no. 10, p. 1732.

    Article  Google Scholar 

  15. Pakal’nis, V.V., Cand. Sci. (Chem) Dissertation, St. Petersburg: St. Petersburg State Univ., 2009.

  16. Toshev, M.T. and Umarov, B.B., Yusupov VG., et al., Koord. Khim., 1990, vol. 16, no. 3, p. 403.

    CAS  Google Scholar 

  17. Umarov, B.B., Toshev, M.T., Saidov, S.O., et al., Koord. Khim., 1992, vol. 18, no. 9, p. 980.

    CAS  Google Scholar 

  18. Khudoerov, A.B., Sharipov, Kh.T., and Yusupov, V.G., Koord. Khim., 1984, vol. 10, no. 3, p. 419.

    Google Scholar 

  19. Karimov, M.M., Cand. Sci. (Chem) Dissertation, Tashkent: Institute of Chemistry, Uzbekistan Acad. Sci., 1990.

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Authors and Affiliations

  1. Bukhara State University, Bukhara, 705018, Uzbekistan

    B. B. Umarov, K. G. Avezov, M. A. Tursunov, N. G. Sevinchov & N. A. Parpiev

  2. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 31, Moscow, 117907, Russia

    G. G. Aleksandrov

Authors
  1. B. B. Umarov
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  2. K. G. Avezov
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  3. M. A. Tursunov
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  4. N. G. Sevinchov
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  5. N. A. Parpiev
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  6. G. G. Aleksandrov
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Corresponding author

Correspondence to K. G. Avezov.

Additional information

Dedicated to the 80th Anniversary of the Kurnakov Institute of General and Inorganic Chemistry

Original Russian Text © B.B. Umarov, K.G. Avezov, M.A. Tursunov, N.G. Sevinchov, N.A. Parpiev, G.G. Aleksandrov, 2014, published in Koordinatsionnaya Khimiya, 2014, Vol. 40, No. 7, pp. 415–418.

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Umarov, B.B., Avezov, K.G., Tursunov, M.A. et al. Synthesis and crystal structure of nickel(II) complex based on 2-trifluoroacetylcycloalkanone benzoylhydrazones. Russ J Coord Chem 40, 473–476 (2014). https://doi.org/10.1134/S1070328414070094

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  • DOI: https://doi.org/10.1134/S1070328414070094

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