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Determination of diagnostical markers of urolithiasis by capillary electrophoresis

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Methods of the electrophoretic determination of the main markers of urolithiasis, i.e., inorganic cations, ammonium, potassium, sodium, magnesium, and calcium; inorganic anions, chloride, sulfate, and phosphate; and organic acid anions, urate, citrate and oxalate, and creatinine in 24-hour collection urine with spectrophotometric detection were developed. The detection limits of analytes ranged form 0.25–1.0 μg/mL. The precision and accuracy were 2–5% and 97–101.5%, respectively. In dependence on the analyte. The developed procedures were used in the analysis of 156 urine samples. Normal ranges were preliminarily determined on a group of healthy donors.

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Authors and Affiliations

  1. Core Facility “CSU Analytical Spectrometry” Ltd., ul. Gzhatskaya 27A, post box 27, St. Petersburg, 195220, Russia

    A. A. Sidorova & A. V. Grigoriev

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  1. A. A. Sidorova
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  2. A. V. Grigoriev
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Original Russian Text © A.A. Sidorova, A.V. Grigoriev, 2012, published in Zhurnal Analiticheskoi Khimii, 2012, Vol. 67, No. 5, pp. 535–542.

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Sidorova, A.A., Grigoriev, A.V. Determination of diagnostical markers of urolithiasis by capillary electrophoresis. J Anal Chem 67, 478–485 (2012). https://doi.org/10.1134/S1061934812050115

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  • DOI: https://doi.org/10.1134/S1061934812050115

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