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Formation of a Corrugated Surface on a Carbon Fiber under High-Fluence Irradiation with Nitrogen Ions

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Abstract

The behavior of the surface of carbon fibers based on polyacrylonitrile, which reinforce the KUP-VM composite, upon corrugation under high-fluence irradiation with \({\text{N}}_{2}^{ + }\) ions with an energy of 15 and 30 keV and a temperature of the irradiated composite in the range from 100°C to 600°C is described and discussed. In contrast to irradiation with ions of noble gases, it is found that the main parameters of the corrugated structure, such as the tilt angles of corrugations and their fractions on the surface of a fiber, are practically independent of the composite temperature. The corrugation periodicity is hundreds of nanometers, as in the case of irradiation with neon and argon ions. In the case of using ion energies of 15 and 30 keV, the tilt angles are 30° and 40°, respectively. The difference between the temperature dependences of the tilt angle of the corrugations and their fraction on the fiber surface and similar dependences in the case of irradiation with noble gas ions is determined by the peculiarities of the dynamic annealing of radiation-induced damage in the fiber shell due to the chemical activity of nitrogen associated with the creation of C–N bonds and a larger proportion of the amorphous component.

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Funding

This study was supported by the Ministry of Education and Science of the Russian Federation under an agreement with the unique identification code RFMEFI57717X0275.

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Authors and Affiliations

  1. Moscow Aviation Institute (National Research University), 125993, Moscow, Russia

    N. N. Andrianova, A. M. Borisov & M. A. Ovchinnikov

  2. Keldysh Research Center, 125438, Moscow, Russia

    V. A. Kazakov

  3. Moscow State University, Skobeltsyn Institute of Nuclear Physics, 119991, Moscow, Russia

    A. V. Makunin, E. S. Mashkova & M. A. Ovchinnikov

Authors
  1. N. N. Andrianova
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  2. A. M. Borisov
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  3. V. A. Kazakov
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  4. A. V. Makunin
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  5. E. S. Mashkova
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  6. M. A. Ovchinnikov
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Corresponding author

Correspondence to E. S. Mashkova.

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Translated by O. Kadkin

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Andrianova, N.N., Borisov, A.M., Kazakov, V.A. et al. Formation of a Corrugated Surface on a Carbon Fiber under High-Fluence Irradiation with Nitrogen Ions. J. Surf. Investig. 14, 231–236 (2020). https://doi.org/10.1134/S1027451020020202

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  • DOI: https://doi.org/10.1134/S1027451020020202

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