Abstract
The crystal and molecular structure of 1,1′-dimethyl-isoindigo is studied by single crystal X-ray diffraction analysis. It is shown that the molecules of 1,1′-dimethyl-isoindigo are nonplanar due to the rotation of two oxindole rings relative to the double bond.
Similar content being viewed by others
References
J. Lee, T. Bansal, A. Jayaraman, W. E. Bentley, and T. K. Wood, Appl. Environ. Microbiol., 73, No. 13, 4100–4109 (2007).
M. Sassatelli, F. Bouchikhi, B. Aboab, F. Anizon, D. Fabbro, M. Prudhomme, and P. Moreau, Anticancer Drugs., 18, No. 9, 1069–1074 (2007).
L. Rui, K. F. Reardon, and T. K. Wood, Appl. Microbiol. Biotechnol., 66, No. 4, 422–429 (2005).
M. Sassatelli, E. Saab, F. Anizon, M. Prudhomme, and P. Moreau, Tetrahedron Lett., 45, No. 25, 4827–4830 (2004).
Zh Xiao., Y. Wanga, L. Lu, Z. Li, Zh. Peng, Zh. Han, and Yu. Hao, Leukemia Res., 30, No. 1, 54–59 (2006).
H. von Eller-Pandraud, Acta Crystallogr., 13, 936–938 (1960).
Y. Mao-Sen, F. Qi, J. Lei, and Y. Wen-Tao, Acta Crystallogr., Sect.E: Struct. Rep. Online, 63, o4342 (2007).
G. Miehe, P. Susse, V. Kupcik, E. Egert, M. Nieger, G. Kunz, R. Gerke, B. Knieriem, M. Niemeyer, and W. Luttke, Angew.Chem. Int. Ed., 30, 964–967 (1991).
F. H. Allen, O. Kennard, D. G. Watson, L. Brammer, A. G. Orpen, and R. Taylor, J. Chem. Soc. Perkin Trans. II, s1–s19 (1987).
E. A. Meyer, R. K. Castellano, and F. Diederich, Angew. Chem. Int. Ed. Eng., 42, 1210–1250 (2003).
C. A. Hunter and J. K. M. Sanders, J. Am. Chem. Soc., 112, 5525–5534 (1990).
A. V. Bogdanov, V. F. Mironov, L. I. Musin, and R. Z. Musin, Synthesis, 19, 3268–3270 (2010).
A. Altomare, G. Cascarano, C. Giacovazzo, and D. Viterbo, Acta Crystallogr. Sec. A, 47, 744–748 (1991).
M. Sheldrick, SHELXL-97 Program for Crystal Structure Refinement, Univ. Göttingen, Germany (1997).
L. J. Farrugia, J. Appl. Crystal., 32, 837/838 (1999).
APEX2 (Version 2.1), SAINTPlus, Data Reduction and Correction Program, Version 7.31A, Bruker Advanced X-ray Solutions, BrukerAXS Inc., Madison, Wisconsin, USA (2006).
L. J. Farrugia, J. Appl. Crystallorg., 30, 565/566 (1997).
A. L. Spek, Acta Crystallogr. Sect. A, 46, 34–39 (1990).
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text Copyright © 2012 by Yu. K. Voronina, D. B. Krivolapov, A. V. Bogdanov, V. F. Mironov, I. A. Litvinov
__________
Translated from Zhurnal Strukturnoi Khimii, Vol. 53, No. 2, pp. 408–411, March–April, 2012.
Rights and permissions
About this article
Cite this article
Voronina, Y.K., Krivolapov, D.B., Bogdanov, A.V. et al. An unusual conformation of 1,1′-dimethyl-isoindigo in crystals. J Struct Chem 53, 413–416 (2012). https://doi.org/10.1134/S0022476612020321
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0022476612020321