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Crystal structure analysis of 4-phenylquinolin-2-(1H)-one

  • Structures of Organic Compounds
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Abstract

The crystal structure of 4-phenylquinolin-2-(1H)-one (C15H11NO) is determined by X-ray diffraction. The compound crystallizes in the orthorhombic crystal system (space group Pbca) with the unit cell parameters a = 7.382(2) Å, b = 21.795(3) Å, c = 14.066(5) Å, and Z = 8. The structure is solved by direct methods and refined to an R-value of 0.0398 for 1360 observed reflections [F 0 > 4σ (F 0)]. The quinoline moiety and the substituted phenyl ring are nearly planar. The dihedral angle between these two moieties is 64.65(6)°. The crystal structure is stabilized by two intermolecular N-H⋯O and C-H⋯O interactions.

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Authors and Affiliations

  1. X-ray Crystallography Laboratory, Post-Graduate Department of Physics, University of Jammu, Jammu Tawi, 180006, India

    Rajnikant, V. K. Gupta &  Dinesh

  2. Department of Chemistry, Shivaji University, 416004, Kolhapur, Maharashtra, India

    M. B. Deshmukh

  3. Regional Sophisticated Instrumentation Center, Indian Institute of Technology, Chennai, 600036, India

    B. Varghese

Authors
  1. Rajnikant
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  2. V. K. Gupta
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  3. M. B. Deshmukh
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  4. B. Varghese
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  5. Dinesh
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Correspondence to Rajnikant.

Additional information

From Kristallografiya, Vol. 47, No. 3, 2002, pp. 494–496.

Original English Text Copyright © 2002 by Rajnikant, Gupta, Deshmukh, Varghese, Dinesh.

This article was submitted by the authors in English.

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Rajnikant, Gupta, V.K., Deshmukh, M.B. et al. Crystal structure analysis of 4-phenylquinolin-2-(1H)-one. Crystallogr. Rep. 47, 449–451 (2002). https://doi.org/10.1134/1.1481933

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  • DOI: https://doi.org/10.1134/1.1481933

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