##############################################################################
#                                                                            #
# This CIF contains the data for a data article accepted for                 #
# publication in IUCrData. It conforms to the requirements of                #
# Notes for Authors for IUCrData, and has been                               #
# peer reviewed under the auspices of IUCrData.                              #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic.                                       #
#                                                                            #
# Software is freely available for graphical display of the structure(s)     #
# in this CIF. For information consult the CIF software page                 #
# http://www.iucr.org/resources/cif/software.                                #
#                                                                            #
# This file may be used for bona fide research purposes within the           #
# scientific community so long as proper attribution is given to the data    # 
# article from which it was obtained.                                        #
#                                                                            #
##############################################################################
data_I
_audit_creation_method     'SHELXL-2018/3'
_chemical_name_systematic
;\
(2,2-Bipyridine-κ²N,N')chlorido\
[η⁶-1-methyl-4-(propan-2-yl)benzene]ruthenium(II) tetraphenylborate
;
_chemical_name_common     ?
_chemical_formula_moiety     'C20 H22 Cl N2 Ru +, C24 H20 B -'
_chemical_formula_sum     'C44 H42 B Cl N2 Ru'
_chemical_formula_iupac     '[Ru Cl (C10 H14) (C10 H8 N2)] (C24 H20 B)'
_chemical_formula_weight     746.12
_chemical_melting_point     ?
_chemical_absolute_configuration     ad
_space_group_crystal_system     monoclinic
_space_group_name_H-M_alt     'P 21'
_space_group_name_Hall     'P 2yb'
loop_
    _space_group_symop_operation_xyz
    'x, y, z'
    '-x, y+1/2, -z'
_cell_length_a     14.1396(15)
_cell_length_b     9.4811(11)
_cell_length_c     14.3009(15)
_cell_angle_alpha     90
_cell_angle_beta     109.013(4)
_cell_angle_gamma     90
_cell_volume     1812.6(3)
_cell_formula_units_Z     2
_cell_measurement_reflns_used     9150
_cell_measurement_theta_min     4.30
_cell_measurement_theta_max     37.09
_cell_measurement_temperature     100(2)
_exptl_crystal_description     block
_exptl_crystal_colour     orange
_exptl_crystal_size_max     0.266
_exptl_crystal_size_mid     0.151
_exptl_crystal_size_min     0.102
_exptl_crystal_density_diffrn     1.367
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     ?
_exptl_crystal_F_000     772
_exptl_absorpt_coefficient_mu     0.540
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al.,  2015)
;
_exptl_absorpt_correction_T_min     0.3908
_exptl_absorpt_correction_T_max     0.4389
_diffrn_ambient_temperature     100(2)
_diffrn_source     ?
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_measurement_device_type     'Bruker Photon II cpad'
_diffrn_measurement_method     'φ and ω scans'
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     57149
_diffrn_reflns_av_R_equivalents     0.0403
_diffrn_reflns_av_unetI/netI     0.0409
_diffrn_reflns_theta_min     2.467
_diffrn_reflns_theta_max     37.089
_diffrn_reflns_theta_full     25.242
_diffrn_measured_fraction_theta_max     0.997
_diffrn_measured_fraction_theta_full     0.998
_diffrn_reflns_limit_h_min     -23
_diffrn_reflns_limit_h_max     23
_diffrn_reflns_limit_k_min     -16
_diffrn_reflns_limit_k_max     16
_diffrn_reflns_limit_l_min     -24
_diffrn_reflns_limit_l_max     24
_refine_special_details
;
Hydrogen atoms were included in calculated positions and treated as
riding on the parent C atom: C---H = 0.95--1.00 Å with Uiso(H) =
1.5Ueq(C-methyl) and 1.2Ueq(C) for other H atoms.
;
_reflns_number_total     18389
_reflns_number_gt     17627
_reflns_threshold_expression     'I > 2σ(I)'
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0273
_refine_ls_R_factor_gt     0.0253
_refine_ls_wR_factor_gt     0.0607
_refine_ls_wR_factor_ref     0.0619
_refine_ls_goodness_of_fit_ref     1.006
_refine_ls_restrained_S_all     1.006
_refine_ls_number_reflns     18389
_refine_ls_number_parameters     446
_refine_ls_number_restraints     1
_refine_ls_hydrogen_treatment     constr
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
              'w=1/[σ²(Fo²)+(0.0280P)²+0.2400P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.000
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.430
_refine_diff_density_min     -0.598
_refine_ls_extinction_method
;
(SHELXL2018; Sheldrick, 2015b)
;
_refine_ls_extinction_coef     0.0054(9)
_refine_ls_extinction_expression
                                  'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
_refine_ls_abs_structure_details
;
Flack x determined using 7947 quotients
[(I⁺)-(I⁻)]/[(I⁺)+(I⁻)]
(Parsons et al.,  2013)
;
_refine_ls_abs_structure_Flack     -0.014(7)
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'B' 'B' 0.0013 0.0007
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Cl' 'Cl' 0.1484 0.1585
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Ru' 'Ru' -1.2594 0.8363
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection
;
APEX3 (Bruker, 2018)
;
_computing_cell_refinement
;
SAINT (Bruker, 2018)
;
_computing_data_reduction
;
SAINT (Bruker, 2018)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_computing_structure_refinement
;
SHELXL2018 (Sheldrick, 2015b)
;
_computing_molecular_graphics
;
Mercury (Macrae et al.,  2008)
;
_computing_publication_material
;
SHELXL2018 (Sheldrick, 2015b), PLATON (Spek, 2009)
and publCIF (Westrip, 2010)
;
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    Ru Ru1 0.18068(2) 0.51286(2) 0.07448(2) 0.01075(3) Uani d 1 . .
    Cl Cl1 0.12759(4) 0.74527(5) 0.01726(4) 0.01957(8) Uani d 1 . .
    N N1 0.09601(10) 0.54459(14) 0.16818(10) 0.0145(2) Uani d 1 . .
    N N2 0.27945(9) 0.61963(14) 0.19404(10) 0.0126(2) Uani d 1 . .
    C C1 0.22538(12) 0.28724(16) 0.09615(11) 0.0146(2) Uani d 1 . .
    C C2 0.12355(14) 0.29922(19) 0.03465(13) 0.0150(3) Uani d 1 . .
    H H2 0.070093 0.263351 0.060173 0.018 Uiso calc 1 . .
    C C3 0.09526(13) 0.38097(18) -0.05258(11) 0.0166(3) Uani d 1 . .
    H H3 0.022771 0.401613 -0.086461 0.020 Uiso calc 1 . .
    C C4 0.16818(13) 0.45675(19) -0.08118(12) 0.0182(3) Uani d 1 . .
    C C5 0.26946(13) 0.45044(19) -0.01971(12) 0.0181(3) Uani d 1 . .
    H H5 0.319034 0.518072 -0.030787 0.022 Uiso calc 1 . .
    C C6 0.29636(12) 0.36769(18) 0.06801(12) 0.0160(3) Uani d 1 . .
    H H6 0.364984 0.379252 0.116869 0.019 Uiso calc 1 . .
    C C7 0.25764(13) 0.19334(18) 0.18562(12) 0.0179(3) Uani d 1 . .
    H H7 0.321125 0.232642 0.232325 0.022 Uiso calc 1 . .
    C C8 0.18197(17) 0.1836(3) 0.24075(17) 0.0333(5) Uani d 1 . .
    H H8A 0.169370 0.278072 0.261917 0.050 Uiso calc 1 . .
    H H8B 0.208624 0.122886 0.298870 0.050 Uiso calc 1 . .
    H H8C 0.119277 0.143665 0.196898 0.050 Uiso calc 1 . .
    C C9 0.2809(2) 0.0474(2) 0.15284(17) 0.0327(5) Uani d 1 . .
    H H9A 0.219180 0.004466 0.109425 0.049 Uiso calc 1 . .
    H H9B 0.309489 -0.012467 0.211108 0.049 Uiso calc 1 . .
    H H9C 0.329040 0.056781 0.117002 0.049 Uiso calc 1 . .
    C C10 0.13714(16) 0.5463(2) -0.17228(13) 0.0259(4) Uani d 1 . .
    H H10A 0.137720 0.489475 -0.229329 0.039 Uiso calc 1 . .
    H H10B 0.183840 0.625332 -0.163962 0.039 Uiso calc 1 . .
    H H10C 0.069533 0.582760 -0.183212 0.039 Uiso calc 1 . .
    C C11 -0.00049(11) 0.5078(3) 0.14594(12) 0.0215(3) Uani d 1 . .
    H H11 -0.032789 0.461693 0.084867 0.026 Uiso calc 1 . .
    C C12 -0.05456(14) 0.5350(2) 0.20943(15) 0.0283(5) Uani d 1 . .
    H H12 -0.122792 0.507808 0.191893 0.034 Uiso calc 1 . .
    C C13 -0.00786(15) 0.6023(3) 0.29879(16) 0.0278(4) Uani d 1 . .
    H H13 -0.043449 0.620928 0.343492 0.033 Uiso calc 1 . .
    C C14 0.09145(13) 0.6420(2) 0.32182(13) 0.0206(3) Uani d 1 . .
    H H14 0.124927 0.688474 0.382439 0.025 Uiso calc 1 . .
    C C15 0.14161(11) 0.61250(17) 0.25445(11) 0.0145(2) Uani d 1 . .
    C C16 0.24499(11) 0.65497(16) 0.26890(11) 0.0128(2) Uani d 1 . .
    C C17 0.30385(12) 0.72922(17) 0.35107(12) 0.0163(3) Uani d 1 . .
    H H17 0.278860 0.751998 0.403353 0.020 Uiso calc 1 . .
    C C18 0.39957(12) 0.76962(17) 0.35571(13) 0.0182(3) Uani d 1 . .
    H H18 0.441031 0.820014 0.411425 0.022 Uiso calc 1 . .
    C C19 0.43407(12) 0.73577(18) 0.27837(13) 0.0186(3) Uani d 1 . .
    H H19 0.499069 0.763543 0.279754 0.022 Uiso calc 1 . .
    C C20 0.37197(11) 0.66058(17) 0.19884(12) 0.0161(3) Uani d 1 . .
    H H20 0.395644 0.637128 0.145788 0.019 Uiso calc 1 . .
    C C1A 0.23530(11) 0.77267(17) 0.60471(11) 0.0132(2) Uani d 1 . .
    C C2A 0.23565(12) 0.88711(16) 0.54243(11) 0.0152(2) Uani d 1 . .
    H H2A 0.298056 0.920629 0.539820 0.018 Uiso calc 1 . .
    C C3A 0.14809(14) 0.95384(18) 0.48412(13) 0.0196(3) Uani d 1 . .
    H H3A 0.152034 1.030055 0.442426 0.023 Uiso calc 1 . .
    C C4A 0.05535(14) 0.9094(2) 0.48677(13) 0.0217(3) Uani d 1 . .
    H H4A -0.004269 0.954885 0.447650 0.026 Uiso calc 1 . .
    C C5A 0.05165(13) 0.7970(2) 0.54779(13) 0.0217(3) Uani d 1 . .
    H H5A -0.010993 0.765367 0.550926 0.026 Uiso calc 1 . .
    C C6A 0.13943(12) 0.73070(19) 0.60434(12) 0.0181(3) Uani d 1 . .
    H H6A 0.134581 0.653307 0.644725 0.022 Uiso calc 1 . .
    C C7A 0.36590(11) 0.75614(16) 0.78984(11) 0.0129(2) Uani d 1 . .
    C C8A 0.30762(13) 0.8527(2) 0.82111(12) 0.0197(3) Uani d 1 . .
    H H8AA 0.247185 0.885698 0.774408 0.024 Uiso calc 1 . .
    C C9A 0.33465(16) 0.9025(2) 0.91823(14) 0.0268(4) Uani d 1 . .
    H H9AA 0.293176 0.968914 0.935999 0.032 Uiso calc 1 . .
    C C10A 0.42176(14) 0.8554(2) 0.98886(13) 0.0228(3) Uani d 1 . .
    H H10D 0.439700 0.887490 1.055300 0.027 Uiso calc 1 . .
    C C11A 0.48227(13) 0.7604(2) 0.96048(12) 0.0202(3) Uani d 1 . .
    H H11A 0.542283 0.727121 1.007701 0.024 Uiso calc 1 . .
    C C12A 0.45494(12) 0.71423(19) 0.86297(12) 0.0173(3) Uani d 1 . .
    H H12A 0.498421 0.651443 0.844919 0.021 Uiso calc 1 . .
    C C13A 0.31168(10) 0.5213(2) 0.67714(9) 0.0126(2) Uani d 1 . .
    C C14A 0.34015(13) 0.43489(17) 0.76138(12) 0.0161(3) Uani d 1 . .
    H H14A 0.376568 0.475869 0.823269 0.019 Uiso calc 1 . .
    C C15A 0.31722(14) 0.29086(19) 0.75824(14) 0.0202(3) Uani d 1 . .
    H H15A 0.337552 0.236845 0.817420 0.024 Uiso calc 1 . .
    C C16A 0.26504(14) 0.22670(18) 0.66926(14) 0.0212(3) Uani d 1 . .
    H H16A 0.249287 0.129060 0.666635 0.025 Uiso calc 1 . .
    C C17A 0.23636(14) 0.3084(2) 0.58416(14) 0.0206(3) Uani d 1 . .
    H H17A 0.200600 0.266322 0.522461 0.025 Uiso calc 1 . .
    C C18A 0.25953(13) 0.45161(18) 0.58838(12) 0.0177(3) Uani d 1 . .
    H H18A 0.239247 0.504547 0.528734 0.021 Uiso calc 1 . .
    C C19A 0.43290(11) 0.71807(15) 0.63904(11) 0.0122(2) Uani d 1 . .
    C C20A 0.47654(11) 0.61317(16) 0.59733(11) 0.0140(2) Uani d 1 . .
    H H20A 0.449422 0.520595 0.590472 0.017 Uiso calc 1 . .
    C C21A 0.55858(12) 0.63956(18) 0.56539(12) 0.0156(2) Uani d 1 . .
    H H21A 0.586610 0.565195 0.538421 0.019 Uiso calc 1 . .
    C C22A 0.59897(12) 0.77414(18) 0.57306(11) 0.0161(3) Uani d 1 . .
    H H22A 0.653725 0.793064 0.550248 0.019 Uiso calc 1 . .
    C C23A 0.55809(12) 0.88118(17) 0.61471(12) 0.0158(3) Uani d 1 . .
    H H23A 0.584916 0.973856 0.620306 0.019 Uiso calc 1 . .
    C C24A 0.47790(12) 0.85237(16) 0.64813(12) 0.0146(2) Uani d 1 . .
    H H24A 0.452554 0.926073 0.678224 0.018 Uiso calc 1 . .
    B B1A 0.33633(12) 0.69173(18) 0.67724(12) 0.0124(2) Uani d 1 . .
loop_
    _atom_site_aniso_label
    _atom_site_aniso_U_11
    _atom_site_aniso_U_22
    _atom_site_aniso_U_33
    _atom_site_aniso_U_12
    _atom_site_aniso_U_13
    _atom_site_aniso_U_23
    Ru1 0.01025(4) 0.01104(4) 0.01128(4) 0.00032(4) 0.00393(3) 0.00047(4)
    Cl1 0.01740(17) 0.01448(16) 0.02383(19) 0.00399(13) 0.00261(14) 0.00439(14)
    N1 0.0140(5) 0.0145(5) 0.0164(5) -0.0034(4) 0.0068(4) -0.0035(4)
    N2 0.0110(5) 0.0118(5) 0.0148(5) 0.0004(4) 0.0038(4) 0.0013(4)
    C1 0.0170(6) 0.0115(5) 0.0142(6) 0.0018(5) 0.0038(5) -0.0009(4)
    C2 0.0173(7) 0.0132(6) 0.0130(6) -0.0003(5) 0.0028(5) -0.0014(5)
    C3 0.0181(6) 0.0178(6) 0.0124(6) 0.0009(5) 0.0030(5) -0.0014(5)
    C4 0.0217(7) 0.0216(7) 0.0125(6) 0.0042(6) 0.0074(5) 0.0011(5)
    C5 0.0191(7) 0.0217(7) 0.0166(6) 0.0028(5) 0.0099(6) 0.0014(5)
    C6 0.0154(6) 0.0169(6) 0.0162(6) 0.0035(5) 0.0057(5) -0.0009(5)
    C7 0.0206(7) 0.0150(6) 0.0147(6) -0.0003(5) 0.0010(5) 0.0018(5)
    C8 0.0301(10) 0.0434(13) 0.0271(9) 0.0023(9) 0.0103(8) 0.0167(9)
    C9 0.0478(13) 0.0140(7) 0.0293(9) 0.0052(7) 0.0030(9) 0.0013(6)
    C10 0.0283(8) 0.0346(10) 0.0167(7) 0.0058(7) 0.0102(6) 0.0087(6)
    C11 0.0166(5) 0.0260(7) 0.0241(6) -0.0095(8) 0.0097(5) -0.0094(9)
    C12 0.0196(7) 0.0391(14) 0.0321(8) -0.0112(7) 0.0167(7) -0.0118(8)
    C13 0.0237(8) 0.0388(11) 0.0277(9) -0.0077(8) 0.0178(7) -0.0091(8)
    C14 0.0210(7) 0.0255(8) 0.0186(7) -0.0030(6) 0.0109(6) -0.0058(6)
    C15 0.0141(6) 0.0152(6) 0.0149(6) -0.0020(5) 0.0058(5) -0.0028(5)
    C16 0.0127(5) 0.0110(5) 0.0140(5) -0.0001(4) 0.0036(5) 0.0000(4)
    C17 0.0174(6) 0.0135(6) 0.0156(6) -0.0001(5) 0.0019(5) -0.0016(5)
    C18 0.0158(6) 0.0135(6) 0.0199(7) -0.0013(5) -0.0015(5) -0.0008(5)
    C19 0.0129(6) 0.0165(6) 0.0233(7) -0.0027(5) 0.0018(5) 0.0024(5)
    C20 0.0115(6) 0.0163(6) 0.0206(7) -0.0011(5) 0.0053(5) 0.0018(5)
    C1A 0.0143(6) 0.0127(6) 0.0125(5) 0.0005(5) 0.0043(5) -0.0012(4)
    C2A 0.0180(6) 0.0122(6) 0.0148(6) -0.0001(5) 0.0047(5) -0.0008(4)
    C3A 0.0240(7) 0.0140(7) 0.0179(7) 0.0032(5) 0.0032(6) 0.0009(5)
    C4A 0.0194(7) 0.0208(7) 0.0208(7) 0.0063(6) 0.0009(6) -0.0001(6)
    C5A 0.0140(6) 0.0276(8) 0.0221(7) 0.0028(6) 0.0040(6) 0.0014(6)
    C6A 0.0139(6) 0.0224(7) 0.0177(6) 0.0010(5) 0.0046(5) 0.0043(5)
    C7A 0.0127(6) 0.0132(6) 0.0133(5) -0.0013(4) 0.0049(5) -0.0014(4)
    C8A 0.0189(7) 0.0225(7) 0.0160(6) 0.0040(6) 0.0034(5) -0.0057(5)
    C9A 0.0266(8) 0.0325(10) 0.0205(8) 0.0056(7) 0.0067(7) -0.0106(7)
    C10A 0.0239(8) 0.0290(9) 0.0146(6) -0.0043(7) 0.0052(6) -0.0060(6)
    C11A 0.0166(6) 0.0271(8) 0.0146(6) -0.0033(6) 0.0021(5) -0.0016(5)
    C12A 0.0139(6) 0.0212(7) 0.0156(6) 0.0003(5) 0.0032(5) -0.0017(5)
    C13A 0.0123(4) 0.0129(5) 0.0139(4) -0.0005(6) 0.0059(4) -0.0006(6)
    C14A 0.0193(6) 0.0147(6) 0.0147(6) 0.0003(5) 0.0064(5) 0.0000(5)
    C15A 0.0251(8) 0.0154(6) 0.0218(7) -0.0001(6) 0.0100(6) 0.0023(5)
    C16A 0.0237(8) 0.0148(6) 0.0285(8) -0.0044(6) 0.0130(7) -0.0023(6)
    C17A 0.0200(7) 0.0184(7) 0.0235(7) -0.0057(6) 0.0071(6) -0.0061(6)
    C18A 0.0186(7) 0.0169(7) 0.0165(6) -0.0038(5) 0.0041(5) -0.0015(5)
    C19A 0.0120(5) 0.0117(5) 0.0125(5) -0.0003(4) 0.0035(4) -0.0004(4)
    C20A 0.0151(6) 0.0117(5) 0.0156(6) -0.0002(4) 0.0056(5) -0.0005(4)
    C21A 0.0144(6) 0.0167(6) 0.0170(6) 0.0003(5) 0.0069(5) -0.0019(5)
    C22A 0.0130(6) 0.0203(7) 0.0156(6) -0.0015(5) 0.0054(5) 0.0016(5)
    C23A 0.0147(6) 0.0143(6) 0.0173(6) -0.0035(5) 0.0035(5) 0.0012(5)
    C24A 0.0142(6) 0.0125(6) 0.0171(6) -0.0012(5) 0.0050(5) -0.0015(5)
    B1A 0.0125(6) 0.0128(6) 0.0116(6) -0.0009(5) 0.0036(5) -0.0010(5)
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Ru1 Cl1 . 2.3851(5) y
    Ru1 N1 . 2.0892(13) y
    Ru1 N2 . 2.0839(13) y
    Ru1 C1 . 2.2234(16) y
    Ru1 C2 . 2.1863(18) y
    Ru1 C3 . 2.2123(16) y
    Ru1 C4 . 2.2391(16) y
    Ru1 C5 . 2.2005(16) y
    Ru1 C6 . 2.1626(16) y
    N1 C11 . 1.3423(19) ?
    N1 C15 . 1.354(2) ?
    N2 C20 . 1.345(2) ?
    N2 C16 . 1.355(2) ?
    C1 C6 . 1.419(2) ?
    C1 C2 . 1.426(3) ?
    C1 C7 . 1.502(2) ?
    C2 C3 . 1.411(2) ?
    C2 H2 . 1.0000 ?
    C3 C4 . 1.422(2) ?
    C3 H3 . 1.0000 ?
    C4 C5 . 1.417(2) ?
    C4 C10 . 1.496(2) ?
    C5 C6 . 1.422(2) ?
    C5 H5 . 1.0000 ?
    C6 H6 . 1.0000 ?
    C7 C8 . 1.525(3) ?
    C7 C9 . 1.531(3) ?
    C7 H7 . 1.0000 ?
    C8 H8A . 0.9800 ?
    C8 H8B . 0.9800 ?
    C8 H8C . 0.9800 ?
    C9 H9A . 0.9800 ?
    C9 H9B . 0.9800 ?
    C9 H9C . 0.9800 ?
    C10 H10A . 0.9800 ?
    C10 H10B . 0.9800 ?
    C10 H10C . 0.9800 ?
    C11 C12 . 1.388(2) ?
    C11 H11 . 0.9500 ?
    C12 C13 . 1.388(3) ?
    C12 H12 . 0.9500 ?
    C13 C14 . 1.386(3) ?
    C13 H13 . 0.9500 ?
    C14 C15 . 1.398(2) ?
    C14 H14 . 0.9500 ?
    C15 C16 . 1.465(2) ?
    C16 C17 . 1.390(2) ?
    C17 C18 . 1.387(2) ?
    C17 H17 . 0.9500 ?
    C18 C19 . 1.384(3) ?
    C18 H18 . 0.9500 ?
    C19 C20 . 1.386(2) ?
    C19 H19 . 0.9500 ?
    C20 H20 . 0.9500 ?
    C1A C2A . 1.405(2) ?
    C1A C6A . 1.411(2) ?
    C1A B1A . 1.655(2) ?
    C2A C3A . 1.399(2) ?
    C2A H2A . 0.9500 ?
    C3A C4A . 1.390(3) ?
    C3A H3A . 0.9500 ?
    C4A C5A . 1.389(3) ?
    C4A H4A . 0.9500 ?
    C5A C6A . 1.391(2) ?
    C5A H5A . 0.9500 ?
    C6A H6A . 0.9500 ?
    C7A C8A . 1.399(2) ?
    C7A C12A . 1.407(2) ?
    C7A B1A . 1.644(2) ?
    C8A C9A . 1.397(2) ?
    C8A H8AA . 0.9500 ?
    C9A C10A . 1.388(3) ?
    C9A H9AA . 0.9500 ?
    C10A C11A . 1.391(3) ?
    C10A H10D . 0.9500 ?
    C11A C12A . 1.391(2) ?
    C11A H11A . 0.9500 ?
    C12A H12A . 0.9500 ?
    C13A C14A . 1.403(2) ?
    C13A C18A . 1.408(2) ?
    C13A B1A . 1.653(3) ?
    C14A C15A . 1.401(2) ?
    C14A H14A . 0.9500 ?
    C15A C16A . 1.386(3) ?
    C15A H15A . 0.9500 ?
    C16A C17A . 1.387(3) ?
    C16A H16A . 0.9500 ?
    C17A C18A . 1.394(3) ?
    C17A H17A . 0.9500 ?
    C18A H18A . 0.9500 ?
    C19A C20A . 1.402(2) ?
    C19A C24A . 1.410(2) ?
    C19A B1A . 1.647(2) ?
    C20A C21A . 1.401(2) ?
    C20A H20A . 0.9500 ?
    C21A C22A . 1.388(2) ?
    C21A H21A . 0.9500 ?
    C22A C23A . 1.394(2) ?
    C22A H22A . 0.9500 ?
    C23A C24A . 1.393(2) ?
    C23A H23A . 0.9500 ?
    C24A H24A . 0.9500 ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    N2 Ru1 N1 . . 76.98(5) y
    N2 Ru1 C6 . . 91.73(6) ?
    N1 Ru1 C6 . . 135.94(6) ?
    N2 Ru1 C2 . . 139.09(6) ?
    N1 Ru1 C2 . . 93.45(6) ?
    C6 Ru1 C2 . . 67.64(7) ?
    N2 Ru1 C5 . . 105.63(6) ?
    N1 Ru1 C5 . . 172.63(6) ?
    C6 Ru1 C5 . . 38.04(6) ?
    C2 Ru1 C5 . . 80.06(7) ?
    N2 Ru1 C3 . . 171.53(6) ?
    N1 Ru1 C3 . . 109.54(6) ?
    C6 Ru1 C3 . . 79.82(6) ?
    C2 Ru1 C3 . . 37.42(6) ?
    C5 Ru1 C3 . . 67.23(7) ?
    N2 Ru1 C1 . . 105.60(5) ?
    N1 Ru1 C1 . . 104.21(6) ?
    C6 Ru1 C1 . . 37.73(6) ?
    C2 Ru1 C1 . . 37.73(7) ?
    C5 Ru1 C1 . . 68.51(6) ?
    C3 Ru1 C1 . . 67.98(6) ?
    N2 Ru1 C4 . . 138.24(6) ?
    N1 Ru1 C4 . . 142.73(6) ?
    C6 Ru1 C4 . . 67.79(6) ?
    C2 Ru1 C4 . . 67.55(7) ?
    C5 Ru1 C4 . . 37.20(6) ?
    C3 Ru1 C4 . . 37.25(6) ?
    C1 Ru1 C4 . . 80.61(6) ?
    N2 Ru1 Cl1 . . 83.37(4) ?
    N1 Ru1 Cl1 . . 84.55(4) ?
    C6 Ru1 Cl1 . . 136.99(5) ?
    C2 Ru1 Cl1 . . 135.91(4) ?
    C5 Ru1 Cl1 . . 102.53(5) ?
    C3 Ru1 Cl1 . . 102.34(5) ?
    C1 Ru1 Cl1 . . 168.54(4) ?
    C4 Ru1 Cl1 . . 87.95(5) y
    C11 N1 C15 . . 119.01(14) ?
    C11 N1 Ru1 . . 124.14(11) ?
    C15 N1 Ru1 . . 116.78(10) ?
    C20 N2 C16 . . 118.85(14) ?
    C20 N2 Ru1 . . 124.25(11) ?
    C16 N2 Ru1 . . 116.82(10) ?
    C6 C1 C2 . . 116.57(14) ?
    C6 C1 C7 . . 120.89(14) ?
    C2 C1 C7 . . 122.53(15) ?
    C6 C1 Ru1 . . 68.81(9) ?
    C2 C1 Ru1 . . 69.72(9) ?
    C7 C1 Ru1 . . 133.03(11) ?
    C3 C2 C1 . . 121.83(17) ?
    C3 C2 Ru1 . . 72.29(10) ?
    C1 C2 Ru1 . . 72.55(9) ?
    C3 C2 H2 . . 118.6 ?
    C1 C2 H2 . . 118.6 ?
    Ru1 C2 H2 . . 118.6 ?
    C2 C3 C4 . . 120.56(15) ?
    C2 C3 Ru1 . . 70.29(9) ?
    C4 C3 Ru1 . . 72.40(9) ?
    C2 C3 H3 . . 119.1 ?
    C4 C3 H3 . . 119.1 ?
    Ru1 C3 H3 . . 119.1 ?
    C5 C4 C3 . . 118.77(15) ?
    C5 C4 C10 . . 120.99(16) ?
    C3 C4 C10 . . 120.19(16) ?
    C5 C4 Ru1 . . 69.92(9) ?
    C3 C4 Ru1 . . 70.35(9) ?
    C10 C4 Ru1 . . 129.54(13) ?
    C4 C5 C6 . . 119.77(15) ?
    C4 C5 Ru1 . . 72.88(9) ?
    C6 C5 Ru1 . . 69.54(9) ?
    C4 C5 H5 . . 119.6 ?
    C6 C5 H5 . . 119.6 ?
    Ru1 C5 H5 . . 119.6 ?
    C1 C6 C5 . . 122.41(15) ?
    C1 C6 Ru1 . . 73.46(9) ?
    C5 C6 Ru1 . . 72.43(9) ?
    C1 C6 H6 . . 118.4 ?
    C5 C6 H6 . . 118.4 ?
    Ru1 C6 H6 . . 118.4 ?
    C1 C7 C8 . . 113.99(15) ?
    C1 C7 C9 . . 108.11(15) ?
    C8 C7 C9 . . 111.16(18) ?
    C1 C7 H7 . . 107.8 ?
    C8 C7 H7 . . 107.8 ?
    C9 C7 H7 . . 107.8 ?
    C7 C8 H8A . . 109.5 ?
    C7 C8 H8B . . 109.5 ?
    H8A C8 H8B . . 109.5 ?
    C7 C8 H8C . . 109.5 ?
    H8A C8 H8C . . 109.5 ?
    H8B C8 H8C . . 109.5 ?
    C7 C9 H9A . . 109.5 ?
    C7 C9 H9B . . 109.5 ?
    H9A C9 H9B . . 109.5 ?
    C7 C9 H9C . . 109.5 ?
    H9A C9 H9C . . 109.5 ?
    H9B C9 H9C . . 109.5 ?
    C4 C10 H10A . . 109.5 ?
    C4 C10 H10B . . 109.5 ?
    H10A C10 H10B . . 109.5 ?
    C4 C10 H10C . . 109.5 ?
    H10A C10 H10C . . 109.5 ?
    H10B C10 H10C . . 109.5 ?
    N1 C11 C12 . . 122.04(16) ?
    N1 C11 H11 . . 119.0 ?
    C12 C11 H11 . . 119.0 ?
    C13 C12 C11 . . 119.30(16) ?
    C13 C12 H12 . . 120.3 ?
    C11 C12 H12 . . 120.3 ?
    C14 C13 C12 . . 119.00(17) ?
    C14 C13 H13 . . 120.5 ?
    C12 C13 H13 . . 120.5 ?
    C13 C14 C15 . . 118.96(16) ?
    C13 C14 H14 . . 120.5 ?
    C15 C14 H14 . . 120.5 ?
    N1 C15 C14 . . 121.67(14) ?
    N1 C15 C16 . . 114.60(13) ?
    C14 C15 C16 . . 123.70(14) ?
    N2 C16 C17 . . 121.53(14) ?
    N2 C16 C15 . . 114.82(13) ?
    C17 C16 C15 . . 123.62(14) ?
    C18 C17 C16 . . 119.10(15) ?
    C18 C17 H17 . . 120.5 ?
    C16 C17 H17 . . 120.5 ?
    C19 C18 C17 . . 119.35(15) ?
    C19 C18 H18 . . 120.3 ?
    C17 C18 H18 . . 120.3 ?
    C18 C19 C20 . . 118.74(15) ?
    C18 C19 H19 . . 120.6 ?
    C20 C19 H19 . . 120.6 ?
    N2 C20 C19 . . 122.40(16) ?
    N2 C20 H20 . . 118.8 ?
    C19 C20 H20 . . 118.8 ?
    C2A C1A C6A . . 114.66(14) ?
    C2A C1A B1A . . 125.09(14) ?
    C6A C1A B1A . . 120.23(14) ?
    C3A C2A C1A . . 122.83(16) ?
    C3A C2A H2A . . 118.6 ?
    C1A C2A H2A . . 118.6 ?
    C4A C3A C2A . . 120.43(16) ?
    C4A C3A H3A . . 119.8 ?
    C2A C3A H3A . . 119.8 ?
    C5A C4A C3A . . 118.61(16) ?
    C5A C4A H4A . . 120.7 ?
    C3A C4A H4A . . 120.7 ?
    C4A C5A C6A . . 120.18(17) ?
    C4A C5A H5A . . 119.9 ?
    C6A C5A H5A . . 119.9 ?
    C5A C6A C1A . . 123.28(16) ?
    C5A C6A H6A . . 118.4 ?
    C1A C6A H6A . . 118.4 ?
    C8A C7A C12A . . 115.15(14) ?
    C8A C7A B1A . . 124.60(14) ?
    C12A C7A B1A . . 120.25(13) ?
    C9A C8A C7A . . 122.68(16) ?
    C9A C8A H8AA . . 118.7 ?
    C7A C8A H8AA . . 118.7 ?
    C10A C9A C8A . . 120.37(18) ?
    C10A C9A H9AA . . 119.8 ?
    C8A C9A H9AA . . 119.8 ?
    C9A C10A C11A . . 118.70(16) ?
    C9A C10A H10D . . 120.6 ?
    C11A C10A H10D . . 120.6 ?
    C10A C11A C12A . . 120.01(16) ?
    C10A C11A H11A . . 120.0 ?
    C12A C11A H11A . . 120.0 ?
    C11A C12A C7A . . 123.05(16) ?
    C11A C12A H12A . . 118.5 ?
    C7A C12A H12A . . 118.5 ?
    C14A C13A C18A . . 114.82(17) ?
    C14A C13A B1A . . 124.65(13) ?
    C18A C13A B1A . . 120.52(14) ?
    C15A C14A C13A . . 122.89(16) ?
    C15A C14A H14A . . 118.6 ?
    C13A C14A H14A . . 118.6 ?
    C16A C15A C14A . . 120.36(16) ?
    C16A C15A H15A . . 119.8 ?
    C14A C15A H15A . . 119.8 ?
    C15A C16A C17A . . 118.46(16) ?
    C15A C16A H16A . . 120.8 ?
    C17A C16A H16A . . 120.8 ?
    C16A C17A C18A . . 120.57(17) ?
    C16A C17A H17A . . 119.7 ?
    C18A C17A H17A . . 119.7 ?
    C17A C18A C13A . . 122.89(17) ?
    C17A C18A H18A . . 118.6 ?
    C13A C18A H18A . . 118.6 ?
    C20A C19A C24A . . 115.58(13) ?
    C20A C19A B1A . . 124.13(13) ?
    C24A C19A B1A . . 120.29(13) ?
    C21A C20A C19A . . 122.55(14) ?
    C21A C20A H20A . . 118.7 ?
    C19A C20A H20A . . 118.7 ?
    C22A C21A C20A . . 120.11(15) ?
    C22A C21A H21A . . 119.9 ?
    C20A C21A H21A . . 119.9 ?
    C21A C22A C23A . . 119.07(14) ?
    C21A C22A H22A . . 120.5 ?
    C23A C22A H22A . . 120.5 ?
    C24A C23A C22A . . 120.06(14) ?
    C24A C23A H23A . . 120.0 ?
    C22A C23A H23A . . 120.0 ?
    C23A C24A C19A . . 122.58(14) ?
    C23A C24A H24A . . 118.7 ?
    C19A C24A H24A . . 118.7 ?
    C7A B1A C19A . . 107.15(12) ?
    C7A B1A C13A . . 110.50(12) ?
    C19A B1A C13A . . 110.20(12) ?
    C7A B1A C1A . . 109.50(12) ?
    C19A B1A C1A . . 111.19(12) ?
    C13A B1A C1A . . 108.31(12) ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    C6 C1 C2 C3 . . . . 3.2(2) ?
    C7 C1 C2 C3 . . . . -175.93(15) ?
    Ru1 C1 C2 C3 . . . . 55.22(15) ?
    C6 C1 C2 Ru1 . . . . -52.00(13) ?
    C7 C1 C2 Ru1 . . . . 128.85(15) ?
    C1 C2 C3 C4 . . . . -1.1(3) ?
    Ru1 C2 C3 C4 . . . . 54.22(14) ?
    C1 C2 C3 Ru1 . . . . -55.33(14) ?
    C2 C3 C4 C5 . . . . -1.0(2) ?
    Ru1 C3 C4 C5 . . . . 52.27(14) ?
    C2 C3 C4 C10 . . . . -178.31(16) ?
    Ru1 C3 C4 C10 . . . . -125.06(16) ?
    C2 C3 C4 Ru1 . . . . -53.25(14) ?
    C3 C4 C5 C6 . . . . 0.8(2) ?
    C10 C4 C5 C6 . . . . 178.13(16) ?
    Ru1 C4 C5 C6 . . . . 53.30(14) ?
    C3 C4 C5 Ru1 . . . . -52.47(14) ?
    C10 C4 C5 Ru1 . . . . 124.83(16) ?
    C2 C1 C6 C5 . . . . -3.4(2) ?
    C7 C1 C6 C5 . . . . 175.78(15) ?
    Ru1 C1 C6 C5 . . . . -55.84(14) ?
    C2 C1 C6 Ru1 . . . . 52.45(13) ?
    C7 C1 C6 Ru1 . . . . -128.39(14) ?
    C4 C5 C6 C1 . . . . 1.4(2) ?
    Ru1 C5 C6 C1 . . . . 56.31(14) ?
    C4 C5 C6 Ru1 . . . . -54.87(14) ?
    C6 C1 C7 C8 . . . . 146.08(18) ?
    C2 C1 C7 C8 . . . . -34.8(2) ?
    Ru1 C1 C7 C8 . . . . 57.1(2) ?
    C6 C1 C7 C9 . . . . -89.8(2) ?
    C2 C1 C7 C9 . . . . 89.3(2) ?
    Ru1 C1 C7 C9 . . . . -178.77(14) ?
    C15 N1 C11 C12 . . . . -1.1(3) ?
    Ru1 N1 C11 C12 . . . . -177.98(18) ?
    N1 C11 C12 C13 . . . . 0.0(4) ?
    C11 C12 C13 C14 . . . . 0.7(4) ?
    C12 C13 C14 C15 . . . . -0.2(3) ?
    C11 N1 C15 C14 . . . . 1.6(3) ?
    Ru1 N1 C15 C14 . . . . 178.68(14) ?
    C11 N1 C15 C16 . . . . -176.66(17) ?
    Ru1 N1 C15 C16 . . . . 0.40(18) ?
    C13 C14 C15 N1 . . . . -0.9(3) ?
    C13 C14 C15 C16 . . . . 177.17(18) ?
    C20 N2 C16 C17 . . . . -1.6(2) ?
    Ru1 N2 C16 C17 . . . . -178.47(11) ?
    C20 N2 C16 C15 . . . . 176.78(14) ?
    Ru1 N2 C16 C15 . . . . -0.12(17) ?
    N1 C15 C16 N2 . . . . -0.2(2) ?
    C14 C15 C16 N2 . . . . -178.42(16) ?
    N1 C15 C16 C17 . . . . 178.13(14) ?
    C14 C15 C16 C17 . . . . -0.1(3) ?
    N2 C16 C17 C18 . . . . 0.9(2) ?
    C15 C16 C17 C18 . . . . -177.30(15) ?
    C16 C17 C18 C19 . . . . 0.3(2) ?
    C17 C18 C19 C20 . . . . -0.8(2) ?
    C16 N2 C20 C19 . . . . 1.1(2) ?
    Ru1 N2 C20 C19 . . . . 177.71(12) ?
    C18 C19 C20 N2 . . . . 0.1(3) ?
    C6A C1A C2A C3A . . . . -0.4(2) ?
    B1A C1A C2A C3A . . . . -178.56(15) ?
    C1A C2A C3A C4A . . . . 0.9(3) ?
    C2A C3A C4A C5A . . . . -0.5(3) ?
    C3A C4A C5A C6A . . . . -0.3(3) ?
    C4A C5A C6A C1A . . . . 0.9(3) ?
    C2A C1A C6A C5A . . . . -0.5(2) ?
    B1A C1A C6A C5A . . . . 177.80(16) ?
    C12A C7A C8A C9A . . . . -1.0(3) ?
    B1A C7A C8A C9A . . . . 178.62(18) ?
    C7A C8A C9A C10A . . . . -0.8(3) ?
    C8A C9A C10A C11A . . . . 1.3(3) ?
    C9A C10A C11A C12A . . . . -0.1(3) ?
    C10A C11A C12A C7A . . . . -1.8(3) ?
    C8A C7A C12A C11A . . . . 2.3(3) ?
    B1A C7A C12A C11A . . . . -177.37(16) ?
    C18A C13A C14A C15A . . . . -1.0(2) ?
    B1A C13A C14A C15A . . . . 179.59(15) ?
    C13A C14A C15A C16A . . . . 0.6(3) ?
    C14A C15A C16A C17A . . . . 0.0(3) ?
    C15A C16A C17A C18A . . . . -0.1(3) ?
    C16A C17A C18A C13A . . . . -0.4(3) ?
    C14A C13A C18A C17A . . . . 0.9(2) ?
    B1A C13A C18A C17A . . . . -179.66(15) ?
    C24A C19A C20A C21A . . . . -0.8(2) ?
    B1A C19A C20A C21A . . . . 179.82(14) ?
    C19A C20A C21A C22A . . . . -0.9(2) ?
    C20A C21A C22A C23A . . . . 1.3(2) ?
    C21A C22A C23A C24A . . . . 0.1(2) ?
    C22A C23A C24A C19A . . . . -2.0(2) ?
    C20A C19A C24A C23A . . . . 2.3(2) ?
    B1A C19A C24A C23A . . . . -178.31(14) ?
    C8A C7A B1A C19A . . . . 127.43(16) ?
    C12A C7A B1A C19A . . . . -52.97(18) ?
    C8A C7A B1A C13A . . . . -112.49(17) ?
    C12A C7A B1A C13A . . . . 67.11(18) ?
    C8A C7A B1A C1A . . . . 6.7(2) ?
    C12A C7A B1A C1A . . . . -173.66(14) ?
    C20A C19A B1A C7A . . . . 129.97(15) ?
    C24A C19A B1A C7A . . . . -49.35(18) ?
    C20A C19A B1A C13A . . . . 9.70(19) ?
    C24A C19A B1A C13A . . . . -169.62(13) ?
    C20A C19A B1A C1A . . . . -110.41(16) ?
    C24A C19A B1A C1A . . . . 70.27(17) ?
    C14A C13A B1A C7A . . . . -17.8(2) ?
    C18A C13A B1A C7A . . . . 162.90(13) ?
    C14A C13A B1A C19A . . . . 100.45(16) ?
    C18A C13A B1A C19A . . . . -78.87(17) ?
    C14A C13A B1A C1A . . . . -137.72(14) ?
    C18A C13A B1A C1A . . . . 42.96(18) ?
    C2A C1A B1A C7A . . . . 96.69(17) ?
    C6A C1A B1A C7A . . . . -81.38(18) ?
    C2A C1A B1A C19A . . . . -21.5(2) ?
    C6A C1A B1A C19A . . . . 160.42(14) ?
    C2A C1A B1A C13A . . . . -142.74(15) ?
    C6A C1A B1A C13A . . . . 39.19(19) ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    C2 H2 Cl1 2_545 1.00 2.66 3.421(2) 133
    C11 H11 Cl1 2_545 0.95 2.62 3.484(2) 151
    C7 H7 Cg1 2_646 1.00 2.67 3.616(2) 158
    C9 H9B Cg2 1_545 0.98 2.91 3.733(2) 143
    C18 H18 Cg1 1_555 0.95 2.73 3.431(2) 131
    C23A H23A Cg2 2_656 0.95 2.60 3.461(2) 151
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_T_min     0.870
_shelx_estimated_absorpt_T_max     0.947
_shelx_hkl_file
;
   2   0   0 6915.30 319.272   7
  -2   0   0 6806.94 319.588   7
  -3   0   0 2914.40 184.912   7
   3   0   0 3781.88 194.732   7
   4   0   0 75.6612 4.98099   6
  -4   0   0 82.1828 5.26665   1
  -4   0   0 75.1479 5.34919   2
  -4   0   0 79.3578 4.46550   3
  -4   0   0 75.4684 3.90767   5
   4   0   0 83.9010 4.04808   5
   4   0   0 78.7677 5.47335   1
   4   0   0 76.3423 5.34774   2
  -4   0   0 82.4217 5.21712   6
   5   0   0 25.2913 3.15884   2
   5   0   0 30.8429 2.08534   5
   5   0   0 24.1350 2.86905   6
   5   0   0 27.0753 3.95888   1
  -5   0   0 25.7405 3.22209   2
  -5   0   0 26.0608 1.89784   5
  -5   0   0 27.5206 2.44656   3
  -5   0   0 27.1389 3.08900   6
  -5   0   0 25.0491 2.90731   1
   6   0   0 468.991 23.5255   6
  -6   0   0 524.925 21.8173   5
  -6   0   0 551.543 24.8568   2
   6   0   0 567.153 25.0879   1
   6   0   0 486.796 24.4255   2
  -6   0   0 510.847 24.0414   6
  -6   0   0 477.964 22.5910   3
   6   0   0 489.155 21.8681   5
  -6   0   0 516.094 24.0618   1
   7   0   0 1568.42 67.0283   2
   7   0   0 1424.37 61.8562   5
  -7   0   0 1589.06 63.0939   3
  -7   0   0 1519.68 64.7889   6
   7   0   0 1382.71 64.9752   6
   7   0   0 1451.51 65.5087   1
   8   0   0 378.718 16.7164   5
   8   0   0 401.965 20.9133   1
  -8   0   0 350.911 19.8146   2
  -8   0   0 354.639 16.4669   5
  -8   0   0 365.399 17.7773   3
  -8   0   0 395.329 19.7678   6
  -9   0   0 86.4165 4.91265   5
  -9   0   0 87.3060 7.68524   6
  -9   0   0 94.0621 8.29201   2
   9   0   0 85.1057 5.14811   5
   9   0   0 91.1293 8.48378   1
 -10   0   0 23.6355 2.29935   5
 -10   0   0 23.8737 3.85804   3
  10   0   0 33.3884 6.41886   1
 -10   0   0 15.5923 4.00857   6
  10   0   0 23.1756 2.53519   5
  11   0   0 358.553 22.7973   1
 -11   0   0 395.957 21.9490   6
 -11   0   0 385.402 19.3009   3
 -12   0   0 179.421 10.1969   4
 -12   0   0 158.074 10.4260   3
 -12   0   0 151.816 12.5114   6
  12   0   0 160.902 14.1189   1
 -13   0   0 174.225 13.6402   6
  13   0   0 201.412 16.0731   1
 -13   0   0 157.255 10.7875   3
 -13   0   0 159.824 10.1115   4
 -14   0   0 514.746 25.9685   3
 -14   0   0 534.745 29.9774   6
  14   0   0 518.116 31.9235   1
 -15   0   0 4.89402 2.58328   4
 -15   0   0 4.41862 2.96636   3
  15   0   0 6.83993 4.96933   1
 -15   0   0 8.41390 4.41393   6
 -16   0   0 928.777 41.9105   3
 -16   0   0 860.876 40.3183   4
 -16   0   0 915.933 46.9472   6
  16   0   0 839.396 49.1906   1
 -17   0   0 538.475 32.3939   6
  17   0   0 542.568 35.3021   1
 -17   0   0 509.286 26.9113   3
  18   0   0 -0.5678 6.04445   1
 -18   0   0 -5.3365 3.84429   6
 -18   0   0 5.32058 3.12348   3
 -19   0   0 296.866 17.9457   3
  19   0   0 280.266 25.8187   1
 -19   0   0 315.593 23.7697   6
 -20   0   0 146.540 17.0037   6
  20   0   0 143.146 21.2101   1
 -20   0   0 157.027 11.9193   3
  21   0   0 185.880 21.3712   1
 -21   0   0 125.772 18.8843   6
 -21   0   0 181.887 13.0536   3
 -22   0   0 399.688 28.7606   6
 -22   0   0 314.771 20.4439   3
  22   0   0 427.787 33.7185   1
   0  -1   0 5.11896 0.93584   6
   0   1   0 0.60260 0.37840   3
   2  -1   0 2584.61 164.091   7
  -2  -1   0 3182.07 163.021   7
   2   1   0 2563.78 142.807   7
  -2   1   0 2399.76 147.439   7
   3  -1   0 5097.51 269.516   7
  -3  -1   0 4683.88 257.622   7
   3   1   0 4403.95 237.651   7
   4  -1   0 2286.12 93.0130   2
   4  -1   0 2253.78 93.2361   1
   4  -1   0 2207.25 92.6945   6
   4  -1   0 2189.35 91.8418   3
  -4  -1   0 2182.97 92.5841   1
  -4  -1   0 2213.60 92.6296   6
  -4   1   0 2304.42 98.6451   6
   4   1   0 2574.35 99.2304   1
  -4   1   0 2604.06 99.1279   1
   4   1   0 2224.27 99.2513   2
   4   1   0 2133.02 98.2746   6
  -4   1   0 2370.29 97.1783   4
  -5  -1   0 2422.28 94.4601   6
   5  -1   0 2067.46 94.3651   2
   5  -1   0 2427.51 95.1987   1
  -5  -1   0 2089.03 94.7810   2
   5  -1   0 2156.86 94.0613   6
   5  -1   0 2320.94 93.2380   3
  -5   1   0 2420.11 94.0547   5
  -5   1   0 2254.61 96.0285   6
   5   1   0 2173.23 96.2685   1
   5   1   0 2121.64 95.6155   6
  -5   1   0 2434.02 96.2630   1
  -5   1   0 2172.09 94.1007   4
   5   1   0 2455.28 94.4534   5
  -5   1   0 2262.60 94.8562   3
   6  -1   0 650.555 30.8877   2
   6  -1   0 668.358 29.3212   3
  -6  -1   0 686.253 30.6182   1
   6  -1   0 703.772 31.5780   1
   6  -1   0 638.112 30.3490   6
  -6  -1   0 660.375 31.3666   2
  -6  -1   0 677.144 30.5680   6
  -6   1   0 663.332 29.1587   1
   6   1   0 631.181 27.0000   5
  -6   1   0 652.455 26.5859   5
   6   1   0 587.186 28.4488   6
  -6   1   0 637.175 27.6751   3
   6   1   0 646.615 29.6834   1
  -6   1   0 610.803 26.8292   4
  -6   1   0 628.170 28.9727   6
   6   1   0 574.414 29.4963   2
   7  -1   0 661.406 30.3742   1
  -7  -1   0 651.096 30.1632   2
  -7  -1   0 622.799 30.8448   6
   7  -1   0 638.097 31.5900   6
   7  -1   0 551.409 29.1882   2
   7  -1   0 599.734 27.5251   3
  -7   1   0 607.476 30.6285   6
  -7   1   0 645.777 29.1493   3
  -7   1   0 654.021 27.8731   5
  -7   1   0 651.475 28.3106   4
   7   1   0 666.565 28.3999   5
   7   1   0 710.568 31.7855   1
   8  -1   0 52.8651 6.23195   1
  -8  -1   0 56.8782 4.43603   3
  -8  -1   0 44.4370 5.60389   2
  -8  -1   0 48.2507 5.32165   6
  -8   1   0 34.2712 3.65512   5
  -8   1   0 39.2704 4.83384   6
   8   1   0 49.8188 5.75551   1
  -8   1   0 33.8943 3.70827   3
   8   1   0 44.5891 3.37720   5
  -8   1   0 42.3247 3.27459   4
  -9  -1   0 905.733 42.5857   6
  -9  -1   0 939.837 43.9064   2
   9  -1   0 918.779 44.1475   1
   9   1   0 971.239 44.3963   1
   9   1   0 924.261 39.7052   5
  -9   1   0 936.082 43.1102   6
  -9   1   0 885.997 39.7361   4
  -9   1   0 929.653 40.8608   3
  -9   1   0 915.912 38.9804   5
 -10  -1   0 1273.72 58.2909   3
 -10  -1   0 1359.46 61.0875   6
 -10  -1   0 1365.90 62.1167   2
  10  -1   0 1420.82 63.2972   1
 -10   1   0 1357.21 59.2813   3
  10   1   0 1419.73 63.5670   1
 -10   1   0 1338.80 57.1142   5
  10   1   0 1370.15 57.9680   5
 -10   1   0 1354.10 58.1155   4
 -10   1   0 1383.64 61.9934   6
 -11  -1   0 38.9796 4.89025   3
 -11  -1   0 34.7394 6.92930   2
  11  -1   0 35.9063 7.15785   1
 -11  -1   0 32.5919 5.79388   6
 -11   1   0 27.6559 2.47608   5
  11   1   0 33.7343 3.30824   5
 -11   1   0 27.0852 5.33061   6
 -11   1   0 33.2568 4.89279   3
 -11   1   0 29.1561 3.30366   4
  11   1   0 35.8798 7.08096   1
 -12  -1   0 1251.00 54.8066   3
  12  -1   0 1190.75 59.9155   1
 -12  -1   0 1233.61 59.0508   2
 -12  -1   0 1288.87 58.2598   6
  12   1   0 1245.85 60.1236   1
  12   1   0 1244.63 53.0392   5
 -12   1   0 1243.93 53.5064   4
 -12   1   0 1309.39 55.0424   3
 -12   1   0 1216.44 57.9621   6
 -12   1   0 1202.11 51.9890   5
 -13  -1   0 857.227 40.7723   3
 -13  -1   0 930.391 44.6983   6
  13  -1   0 893.628 46.7527   1
 -13  -1   0 896.668 45.3661   2
 -13   1   0 901.549 42.9539   6
  13   1   0 884.799 44.9381   1
 -13   1   0 760.002 37.0020   4
 -13   1   0 860.180 38.9906   3
  13   1   0 836.608 36.7490   5
 -14  -1   0 54.0919 5.83106   3
 -14  -1   0 51.2463 8.85462   6
  14  -1   0 54.1685 10.5284   1
 -14   1   0 54.4109 6.01698   3
  14   1   0 59.4636 10.5901   1
 -14   1   0 46.8717 4.51171   4
  14   1   0 54.0273 4.26244   5
 -14   1   0 67.9132 10.2797   6
 -15  -1   0 439.318 27.2195   6
 -15  -1   0 436.297 23.2049   3
 -15  -1   0 445.186 22.9917   4
  15  -1   0 480.534 30.2578   1
 -15   1   0 451.403 26.6158   6
  15   1   0 377.833 27.8566   1
 -15   1   0 462.424 22.7239   3
 -15   1   0 411.271 20.1915   4
  16  -1   0 131.805 15.8446   1
 -16  -1   0 141.264 10.2540   4
 -16  -1   0 168.945 11.3906   3
 -16  -1   0 152.763 14.2688   6
  16   1   0 157.959 17.1094   1
 -16   1   0 160.438 14.8041   6
 -16   1   0 170.815 11.6909   3
 -16   1   0 147.510 8.84623   4
 -17  -1   0 205.128 17.8647   6
 -17  -1   0 205.899 12.9725   4
 -17  -1   0 216.125 13.9362   3
  17  -1   0 198.316 19.6592   1
 -17   1   0 231.215 14.2488   3
 -17   1   0 240.573 18.7499   6
  17   1   0 215.383 20.6881   1
 -17   1   0 195.547 10.4198   4
 -18  -1   0 248.408 20.1805   6
 -18  -1   0 239.891 14.4604   4
 -18  -1   0 243.243 15.1845   3
  18  -1   0 222.711 21.9236   1
 -18   1   0 240.972 19.6398   6
  18   1   0 214.851 21.7550   1
 -19  -1   0 20.8238 4.85218   3
 -19  -1   0 19.7462 6.59094   6
 -19  -1   0 19.7211 4.31657   4
  19  -1   0 23.2243 8.84889   1
  19   1   0 15.7687 8.10064   1
 -19   1   0 19.9075 5.17391   3
 -19   1   0 6.83892 5.98573   6
 -20  -1   0 234.110 21.0319   6
  20  -1   0 267.658 24.8232   1
 -20  -1   0 233.839 15.7203   3
  20   1   0 256.958 27.4867   1
 -20   1   0 272.622 22.1474   6
 -20   1   0 250.250 16.3541   3
 -21  -1   0 303.300 18.5171   3
  21  -1   0 326.358 29.2007   1
 -21   1   0 335.217 28.7589   6
 -21   1   0 321.616 19.2867   3
  21   1   0 304.485 28.4736   1
 -22  -1   0 43.9379 10.1675   6
  22  -1   0 52.6518 12.4113   1
 -22   1   0 40.6625 11.0929   6
 -22   1   0 35.3174 6.76457   3
  22   1   0 44.5532 13.2801   1
   0  -2   0 299.598 14.4523   6
   0  -2   0 315.278 15.1398   2
   0  -2   0 338.058 14.3587   6
   0   2   0 365.915 16.9958   2
   0   2   0 364.717 15.8995   3
  -1  -2   0 5617.91 290.634   7
   1  -2   0 5986.71 302.181   7
  -1   2   0 5366.87 298.301   7
   1   2   0 6185.77 296.358   7
  -2  -2   0 1133.67 48.1613   6
   2  -2   0 1100.04 47.6735   3
  -2  -2   0 1114.58 47.9285   1
  -2  -2   0 1095.05 49.1141   2
   2  -2   0 1258.26 49.1448   6
   2   2   0 1062.32 45.3036   1
  -2   2   0 1140.17 45.3584   3
   2   2   0 1055.86 46.7082   2
   2   2   0 1074.82 45.7720   6
  -2   2   0 1013.13 45.5032   1
  -2   2   0 1134.16 45.8412   6
  -3  -2   0 1045.12 41.8761   6
   3  -2   0 960.690 41.7669   6
   3  -2   0 961.943 41.1611   3
   3  -2   0 1019.16 41.9587   1
  -3  -2   0 962.409 42.8103   2
  -3  -2   0 925.791 41.1363   1
   3  -2   0 930.303 40.8462   4
   3   2   0 1068.01 44.7493   6
  -3   2   0 1066.16 44.9006   6
   3   2   0 1049.91 46.0512   2
   3   2   0 1158.61 44.7643   1
  -3   2   0 1023.46 44.0577   3
  -3   2   0 909.458 44.4669   1
   4  -2   0 89.0986 4.81341   4
   4  -2   0 90.1657 6.26731   1
  -4  -2   0 88.4121 5.59895   1
   4  -2   0 95.6703 5.57207   3
  -4  -2   0 89.4836 5.96358   6
  -4  -2   0 96.3496 6.89668   2
   4  -2   0 98.6864 6.20466   6
   4   2   0 94.7894 6.09139   1
   4   2   0 94.8793 5.99970   6
   4   2   0 91.3020 5.29496   5
  -4   2   0 100.481 5.54242   3
   4   2   0 77.3103 6.53950   2
  -4   2   0 95.8919 6.16730   6
  -4   2   0 88.1688 5.97255   1
   5  -2   0 1362.15 54.9614   1
   5  -2   0 1261.03 51.9674   4
  -5  -2   0 1190.70 53.8200   6
  -5  -2   0 1334.97 55.3874   2
   5  -2   0 1213.66 53.0133   3
  -5  -2   0 1147.92 53.3791   1
  -5   2   0 1270.11 53.1646   3
  -5   2   0 1308.88 52.5015   4
   5   2   0 1196.67 55.3791   2
   5   2   0 1211.85 52.7746   5
   5   2   0 1183.79 54.2221   1
  -5   2   0 1392.53 54.5832   1
  -5   2   0 1254.42 54.2811   6
   5   2   0 1204.37 53.8299   6
   6  -2   0 3295.13 139.334   6
  -6  -2   0 3344.63 139.276   6
   6  -2   0 3463.28 139.874   2
   6  -2   0 3447.39 140.364   1
  -6  -2   0 3268.06 138.832   1
   6  -2   0 3199.12 138.074   3
  -6   2   0 3469.92 138.635   5
   6   2   0 3425.71 142.933   1
   6   2   0 3209.90 140.435   6
  -6   2   0 3430.09 140.973   1
  -6   2   0 3499.01 138.617   4
  -6   2   0 3325.65 139.441   3
  -6   2   0 3438.04 140.993   6
   6   2   0 3022.36 143.358   2
   6   2   0 3490.23 139.097   5
   7  -2   0 140.833 10.2355   1
  -7  -2   0 150.647 10.4891   2
  -7  -2   0 155.833 9.71338   6
   7  -2   0 135.506 8.27835   3
  -7   2   0 141.161 7.22088   4
   7   2   0 141.733 7.72474   5
   7   2   0 137.282 9.69593   1
  -7   2   0 133.868 8.12296   3
  -7   2   0 135.775 7.04333   5
  -8  -2   0 2408.22 105.401   6
  -8  -2   0 2655.74 106.435   2
   8  -2   0 2294.07 105.597   1
  -8   2   0 2661.89 107.293   6
  -8   2   0 2300.69 103.260   5
   8   2   0 2571.23 108.019   1
   8   2   0 2675.45 104.382   5
  -8   2   0 2319.66 104.814   3
  -8   2   0 2509.03 103.620   4
  -9  -2   0 1540.80 67.0521   6
   9  -2   0 1458.78 68.2711   1
  -9  -2   0 1531.44 68.4385   2
  -9   2   0 1441.23 61.7976   5
  -9   2   0 1579.77 63.9173   3
  -9   2   0 1369.45 62.0812   4
  -9   2   0 1514.84 66.1183   6
   9   2   0 1527.73 62.9084   5
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   3   2   2 274.917 14.4767   2
   3   2   2 250.878 12.8948   6
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   4   2   2 1585.03 68.7784   6
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   5  -2   2 2815.28 118.588   3
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   5  -2   2 2704.94 120.590   1
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   5   2   2 2773.15 124.902   2
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   5   2   2 2659.46 123.977   1
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   6  -2   2 779.850 34.5955   2
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   6   2   2 782.805 36.1597   1
   6   2   2 736.300 33.6289   5
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   7  -2   2 1956.43 84.9798   1
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   7   2   2 1985.30 85.3837   1
   7   2   2 1913.67 82.1427   5
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   8  -2   2 2419.96 98.2795   1
   8   2   2 2404.37 102.028   1
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   9  -2   2 263.122 17.5103   1
   9   2   2 242.293 17.1108   1
   9   2   2 284.460 14.1916   5
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   2   1   3 1366.38 57.5286   6
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   2   1   3 1351.32 57.8932   5
   3  -1   3 1876.25 80.2364   3
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   3  -1   3 1876.56 79.5317   5
   3  -1   3 1755.96 79.0547   2
   3  -1   3 1909.01 80.6185   6
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   3   1   3 1840.96 76.2702   1
  -3   1  -3 1707.42 73.1780   4
   3   1   3 1814.22 74.7601   5
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   3   1   3 1838.77 75.9306   2
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   3   1   3 1821.41 74.6470   6
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   4  -1   3 1213.46 51.5510   1
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   4   1   3 1125.01 51.3101   6
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   4   1   3 1171.92 52.6453   2
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   4   1   3 1195.22 53.2384   1
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   5  -1   3 1696.16 70.9443   1
   5  -1   3 1601.34 68.3227   2
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   5   1   3 1470.63 67.0091   2
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   5   1   3 1536.40 65.4301   5
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   6  -1   3 1756.98 78.4377   1
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   6  -1   3 1895.34 75.2681   5
   6   1   3 1652.09 79.0609   2
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   6   1   3 2061.77 81.1850   1
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   7   1   3 80.8841 8.39941   1
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   7   1   3 90.0470 6.43324   5
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   9   1   3 458.056 28.5743   1
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   9   1   3 511.272 24.8599   5
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   9  -2  -3 1315.10 52.9044   3
   9  -2  -3 1198.43 54.8042   1
   9   2  -3 1187.69 54.2213   1
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   9   2  -3 1229.07 50.5920   5
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   8  -2  -3 386.794 19.9203   6
   8  -2  -3 398.712 18.3666   3
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   8   2  -3 373.249 18.1074   5
   8   2  -3 445.473 21.3475   1
   7  -2  -3 788.250 36.2360   6
   7  -2  -3 744.364 34.6211   3
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   7  -2  -3 865.857 36.7880   1
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   7  -2  -3 839.313 35.9730   4
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  -7   2   3 713.203 32.3249   3
   7   2  -3 785.010 34.5164   6
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   7   2  -3 701.120 34.3981   1
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   6  -2  -3 2620.36 105.166   1
   6  -2  -3 2515.24 105.020   6
   6  -2  -3 2397.66 104.727   4
   6  -2  -3 2370.17 103.555   3
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   6   2  -3 2387.98 111.024   2
   6   2  -3 2677.74 111.183   6
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   6   2  -3 2545.58 110.896   1
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   5  -2  -3 581.533 25.1363   1
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   5  -2  -3 582.007 24.3132   3
   5  -2  -3 592.634 25.7274   4
   5  -2  -3 550.269 25.2503   6
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   5   2  -3 564.462 26.0813   6
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  -5   2   3 560.385 26.4963   4
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   5   2  -3 579.367 27.3183   2
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   5   2  -3 579.594 26.0329   1
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   4  -2  -3 1222.26 54.5971   1
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   4  -2  -3 1332.68 54.4148   3
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   4   2  -3 1255.27 54.6944   1
   4   2  -3 1347.98 55.9141   2
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   3  -2  -3 339.669 15.5814   6
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   3  -2  -3 331.696 15.1594   3
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   3  -2  -3 367.247 15.0212   1
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   3   2  -3 313.533 15.1877   6
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   2  -2  -3 1263.64 50.8125   1
   2  -2  -3 1196.22 51.8104   5
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   2   2  -3 1117.10 54.4523   2
   2   2  -3 1349.02 52.9510   3
   2   2  -3 1271.74 53.8045   6
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   1  -2  -3 572.231 24.6118   1
   1  -2  -3 600.659 25.1749   6
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   1  -2  -3 592.323 26.8413   4
   1  -2  -3 577.507 25.4605   5
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  -1  -2   3 563.670 25.3759   2
   1   2  -3 667.915 28.2261   2
  -1   2   3 662.108 29.8628   4
  -1   2   3 643.382 28.2114   5
   1   2  -3 683.301 28.6128   6
   1   2  -3 599.782 28.1615   6
   1   2  -3 658.613 27.9271   3
   0  -2   3 4475.74 245.775   7
   0  -2  -3 4001.65 214.542   7
  -1  -2  -3 4913.08 251.938   7
  -1   2  -3 5281.94 299.598   7
  -2  -2  -3 4060.38 167.448   1
   2   2   3 4096.59 170.468   2
   3  -2   3 982.568 44.5590   3
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   3  -2   3 966.828 44.9031   6
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   3  -2   3 1011.89 42.8030   4
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  -3   2  -3 977.868 47.0485   1
  -3   2  -3 1055.65 45.6643   5
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   3   2   3 1171.89 46.0466   5
   3   2   3 1065.35 47.5822   2
   3   2   3 1070.85 45.7394   6
   3   2   3 1023.41 46.6582   1
  -4  -2  -3 5505.03 222.440   5
   4  -2   3 5251.71 222.665   3
  -4  -2  -3 5230.46 223.170   1
   4  -2   3 5637.33 223.411   6
   4   2   3 5505.87 221.862   2
   4   2   3 5184.83 219.615   6
  -4   2  -3 5311.17 221.648   1
   5  -2   3 777.463 36.0566   2
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  -5  -2  -3 828.316 38.1441   1
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   4  -3 -23 13.4113 6.12722   3
   4  -3 -23 7.01020 4.40807   1
  -4  -3  23 16.0162 8.41912   4
   4   3 -23 8.21582 6.86340   3
   3  -3 -23 85.4268 12.0107   3
  -3  -3  23 64.6784 12.8303   4
   3   3 -23 70.0097 10.1026   3
   2  -3 -23 198.203 17.1927   3
  -2  -3  23 181.598 20.1675   4
   2   3 -23 165.842 14.7679   3
 -11  -4  23 4.60939 6.81360   4
  11  -4 -23 8.41594 7.51250   2
  11   4 -23 8.65840 6.19025   1
 -11   4  23 11.2027 9.27206   4
  10  -4 -23 83.9910 15.9985   2
 -10   4  23 122.739 21.8991   4
  10   4 -23 139.291 14.6221   1
  -9  -4  23 91.6080 17.3570   4
   9   4 -23 65.2972 11.4421   1
  -9   4  23 69.2242 15.5281   4
   8  -4 -23 3.31427 4.49142   3
  -8  -4  23 13.2229 8.93384   4
   8   4 -23 5.73912 5.55446   1
   7  -4 -23 230.015 16.4454   3
  -7  -4  23 194.961 21.6495   4
   7   4 -23 231.805 19.3878   1
   6  -4 -23 152.250 14.4255   3
  -6  -4  23 157.234 19.0291   4
   6   4 -23 153.424 15.5623   1
   6   4 -23 138.523 11.6827   3
   5  -4 -23 8.84632 5.24344   3
  -5  -4  23 13.1502 8.71150   4
   5   4 -23 13.7291 7.20133   1
   5   4 -23 11.2384 5.32005   3
   4  -4 -23 125.417 13.3145   3
  -4  -4  23 121.769 18.3139   4
   4  -4 -23 118.025 15.8725   1
   4   4 -23 81.5266 10.9399   3
   3  -4 -23 62.9218 11.3165   3
   3   4 -23 72.5596 10.2959   3
   8  -5 -23 150.890 13.4085   3
  -8  -5  23 204.998 21.1992   4
   8   5 -23 189.211 18.2589   1
  -7  -5  23 48.5327 13.0255   4
   7   5 -23 32.3738 8.85962   1
  10   0 -24 280.672 20.2836   1
 -10   0  24 254.865 26.5504   4
  -9   0  24 24.2365 11.3722   4
   9   0 -24 54.7360 9.35316   1
  -8   0  24 85.1913 15.9198   4
   8   0 -24 90.1719 11.6101   1
  -7   0  24 217.240 24.7398   4
   7   0 -24 258.991 18.9047   1
  -6   0  24 12.5194 8.43408   4
   6   0 -24 -3.2152 4.25211   1
   6   0 -24 12.3628 4.30708   3
  -5   0  24 94.0481 18.3761   4
   5   0 -24 99.8673 12.0274   1
  10  -1 -24 16.9826 5.63448   1
 -10  -1  24 13.6365 8.25866   4
  10   1 -24 12.3889 6.01634   1
 -10   1  24 22.5521 10.7528   4
   9  -1 -24 121.080 12.3825   1
  -9  -1  24 151.357 22.2036   4
   9   1 -24 128.937 13.4229   1
  -9   1  24 135.552 22.2406   4
   8  -1 -24 56.0025 9.47455   1
  -8  -1  24 55.9240 13.9504   4
  -8   1  24 58.9400 14.7133   4
   8   1 -24 63.6937 11.0215   1
   7  -1 -24 -6.1893 6.61303   3
   7  -1 -24 -4.7938 3.92966   1
  -7  -1  24 4.36437 8.28055   4
   7   1 -24 7.81637 5.32419   1
  -7   1  24 -9.5171 6.86092   4
   6  -1 -24 34.3919 7.21839   3
   6  -1 -24 58.9270 9.16037   1
  -6  -1  24 54.3717 12.9955   4
   6   1 -24 47.9157 9.22021   1
  -6   1  24 39.9874 12.2126   4
   6   1 -24 43.5706 6.88354   3
   5  -1 -24 42.8048 9.18390   3
  -5  -1  24 26.9756 10.7692   4
   5  -1 -24 30.5088 7.71453   1
  -5   1  24 24.2848 10.2118   4
   5   1 -24 27.7200 7.24173   1
  -9  -2  24 75.4202 16.6634   4
   9  -2 -24 71.1747 11.1512   1
  -9   2  24 61.6678 15.4440   4
   9   2 -24 74.0923 11.4195   1
   8  -2 -24 68.5554 10.3050   1
  -8  -2  24 64.5989 14.6506   4
  -8   2  24 78.8056 18.1585   4
   8   2 -24 98.7146 11.8558   1
  -7  -2  24 46.9779 12.1198   4
   7  -2 -24 39.7799 7.77311   3
   7  -2 -24 78.9764 9.42498   1
  -7   2  24 60.1727 14.9377   4
   7   2 -24 93.9180 11.6063   1
   0   0   0    0.00    0.00   0
_shelx_hkl_checksum   33658
#=====================================================
_publcif_funding_html
;
_shelx_res_file
;
TITL 19038.res in P2(1)
    19038.res
    created by SHELXL-2018/3 at 14:02:25 on 20-Feb-2019
REM Old TITL Integration of RY-1341
REM SHELXT solution in P2(1)
REM R1 0.058,  Rweak 0.030,  Alpha 0.009,  Orientation as input
REM Flack x =  0.045 ( 0.031 ) from Parsons' quotients
REM Formula found by SHELXT:  C40 B Cl N6 Ru
CELL  0.71073  14.1396   9.4811  14.3009   90.000  109.013   90.000
ZERR    2.000   0.0015   0.0011   0.0015    0.000    0.004    0.000
LATT -1
SYMM -X, 1/2+Y, -Z
SFAC C  H  B CL N RU
UNIT 88 84 2 2  4 2
omit   2  14   3  ! (Fo^2^ - Fc^2^)/esd > 10.0
omit -17  -7  13
omit -14   3  15
omit   0   1   2
omit -20   5   8
omit -19  -8  12
omit   1   0   5
omit -15  -8  14
omit   1  13   1
omit -14   8  15
omit   9  12   5
TEMP -173.16
SIZE 0.102 0.151 0.266
acta
conf
wpdb -2
EQIV $1 -x, y-1/2, -z
HTAB C11 Cl1_$1
htab
L.S. 10 4
BOND $H
FMAP 2
PLAN 20
WGHT    0.028000    0.240000
EXTI    0.005372
FVAR       0.76283
RU1   6    0.180683    0.512860    0.074484    11.00000    0.01025    0.01104 =
         0.01128    0.00047    0.00393    0.00032
CL1   4    0.127589    0.745273    0.017257    11.00000    0.01740    0.01448 =
         0.02383    0.00439    0.00261    0.00399
N1    5    0.096007    0.544592    0.168181    11.00000    0.01395    0.01454 =
         0.01636   -0.00354    0.00681   -0.00337
N2    5    0.279447    0.619632    0.194043    11.00000    0.01097    0.01180 =
         0.01477    0.00127    0.00377    0.00037
C1    1    0.225378    0.287241    0.096154    11.00000    0.01701    0.01152 =
         0.01422   -0.00094    0.00385    0.00177
C2    1    0.123552    0.299222    0.034652    11.00000    0.01732    0.01322 =
         0.01301   -0.00140    0.00276   -0.00026
AFIX  13
H2    2    0.070093    0.263351    0.060173    11.00000   -1.20000
AFIX   0
C3    1    0.095257    0.380966   -0.052576    11.00000    0.01812    0.01782 =
         0.01239   -0.00139    0.00303    0.00086
AFIX  13
H3    2    0.022771    0.401613   -0.086461    11.00000   -1.20000
AFIX   0
C4    1    0.168183    0.456754   -0.081181    11.00000    0.02166    0.02164 =
         0.01251    0.00105    0.00742    0.00424
C5    1    0.269460    0.450437   -0.019709    11.00000    0.01908    0.02169 =
         0.01657    0.00138    0.00992    0.00281
AFIX  13
H5    2    0.319034    0.518072   -0.030787    11.00000   -1.20000
AFIX   0
C6    1    0.296358    0.367694    0.068012    11.00000    0.01543    0.01685 =
         0.01625   -0.00086    0.00573    0.00352
AFIX  13
H6    2    0.364984    0.379252    0.116869    11.00000   -1.20000
AFIX   0
C7    1    0.257645    0.193344    0.185617    11.00000    0.02064    0.01500 =
         0.01470    0.00184    0.00097   -0.00030
AFIX  13
H7    2    0.321125    0.232642    0.232325    11.00000   -1.20000
AFIX   0
C8    1    0.181970    0.183624    0.240750    11.00000    0.03014    0.04342 =
         0.02713    0.01666    0.01034    0.00227
AFIX 137
H8A   2    0.169370    0.278072    0.261917    11.00000   -1.50000
H8B   2    0.208624    0.122886    0.298870    11.00000   -1.50000
H8C   2    0.119277    0.143665    0.196898    11.00000   -1.50000
AFIX   0
C9    1    0.280933    0.047404    0.152840    11.00000    0.04785    0.01396 =
         0.02927    0.00131    0.00304    0.00521
AFIX 137
H9A   2    0.219180    0.004466    0.109425    11.00000   -1.50000
H9B   2    0.309489   -0.012467    0.211108    11.00000   -1.50000
H9C   2    0.329040    0.056781    0.117002    11.00000   -1.50000
AFIX   0
C10   1    0.137142    0.546302   -0.172276    11.00000    0.02826    0.03464 =
         0.01674    0.00868    0.01016    0.00575
AFIX 137
H10A  2    0.137720    0.489475   -0.229329    11.00000   -1.50000
H10B  2    0.183840    0.625332   -0.163962    11.00000   -1.50000
H10C  2    0.069533    0.582760   -0.183212    11.00000   -1.50000
AFIX   0
C11   1   -0.000491    0.507785    0.145942    11.00000    0.01657    0.02602 =
         0.02405   -0.00942    0.00969   -0.00949
AFIX  43
H11   2   -0.032789    0.461693    0.084867    11.00000   -1.20000
AFIX   0
C12   1   -0.054558    0.534987    0.209426    11.00000    0.01963    0.03915 =
         0.03214   -0.01178    0.01667   -0.01118
AFIX  43
H12   2   -0.122792    0.507808    0.191893    11.00000   -1.20000
AFIX   0
C13   1   -0.007862    0.602319    0.298794    11.00000    0.02374    0.03878 =
         0.02772   -0.00914    0.01779   -0.00771
AFIX  43
H13   2   -0.043449    0.620928    0.343492    11.00000   -1.20000
AFIX   0
C14   1    0.091451    0.641979    0.321821    11.00000    0.02105    0.02550 =
         0.01858   -0.00579    0.01088   -0.00304
AFIX  43
H14   2    0.124927    0.688474    0.382439    11.00000   -1.20000
AFIX   0
C15   1    0.141606    0.612496    0.254449    11.00000    0.01414    0.01520 =
         0.01486   -0.00279    0.00580   -0.00198
C16   1    0.244994    0.654975    0.268899    11.00000    0.01270    0.01104 =
         0.01400   -0.00005    0.00361   -0.00011
C17   1    0.303846    0.729223    0.351074    11.00000    0.01741    0.01346 =
         0.01558   -0.00159    0.00188   -0.00013
AFIX  43
H17   2    0.278860    0.751998    0.403353    11.00000   -1.20000
AFIX   0
C18   1    0.399566    0.769617    0.355711    11.00000    0.01582    0.01353 =
         0.01993   -0.00079   -0.00145   -0.00125
AFIX  43
H18   2    0.441031    0.820014    0.411425    11.00000   -1.20000
AFIX   0
C19   1    0.434070    0.735773    0.278367    11.00000    0.01294    0.01654 =
         0.02328    0.00236    0.00181   -0.00272
AFIX  43
H19   2    0.499069    0.763543    0.279754    11.00000   -1.20000
AFIX   0
C20   1    0.371970    0.660582    0.198837    11.00000    0.01152    0.01627 =
         0.02065    0.00181    0.00527   -0.00105
AFIX  43
H20   2    0.395644    0.637128    0.145788    11.00000   -1.20000
AFIX   0
C1A   1    0.235304    0.772673    0.604709    11.00000    0.01427    0.01267 =
         0.01254   -0.00124    0.00431    0.00046
C2A   1    0.235650    0.887114    0.542435    11.00000    0.01800    0.01222 =
         0.01476   -0.00077    0.00467   -0.00013
AFIX  43
H2A   2    0.298056    0.920629    0.539820    11.00000   -1.20000
AFIX   0
C3A   1    0.148088    0.953838    0.484120    11.00000    0.02402    0.01401 =
         0.01794    0.00092    0.00315    0.00325
AFIX  43
H3A   2    0.152034    1.030055    0.442426    11.00000   -1.20000
AFIX   0
C4A   1    0.055353    0.909379    0.486766    11.00000    0.01940    0.02084 =
         0.02075   -0.00014    0.00089    0.00628
AFIX  43
H4A   2   -0.004269    0.954885    0.447650    11.00000   -1.20000
AFIX   0
C5A   1    0.051648    0.797025    0.547789    11.00000    0.01404    0.02764 =
         0.02210    0.00140    0.00401    0.00285
AFIX  43
H5A   2   -0.010993    0.765367    0.550926    11.00000   -1.20000
AFIX   0
C6A   1    0.139430    0.730705    0.604343    11.00000    0.01387    0.02236 =
         0.01773    0.00435    0.00463    0.00101
AFIX  43
H6A   2    0.134581    0.653307    0.644725    11.00000   -1.20000
AFIX   0
C7A   1    0.365905    0.756140    0.789845    11.00000    0.01265    0.01316 =
         0.01325   -0.00138    0.00488   -0.00133
C8A   1    0.307619    0.852666    0.821112    11.00000    0.01886    0.02251 =
         0.01605   -0.00568    0.00336    0.00404
AFIX  43
H8AA  2    0.247185    0.885698    0.774408    11.00000   -1.20000
AFIX   0
C9A   1    0.334654    0.902474    0.918225    11.00000    0.02664    0.03245 =
         0.02051   -0.01057    0.00674    0.00559
AFIX  43
H9AA  2    0.293176    0.968914    0.935999    11.00000   -1.20000
AFIX   0
C10A  1    0.421756    0.855435    0.988858    11.00000    0.02385    0.02904 =
         0.01462   -0.00604    0.00523   -0.00430
AFIX  43
H10D  2    0.439700    0.887490    1.055300    11.00000   -1.20000
AFIX   0
C11A  1    0.482271    0.760447    0.960483    11.00000    0.01661    0.02709 =
         0.01461   -0.00163    0.00206   -0.00332
AFIX  43
H11A  2    0.542283    0.727121    1.007701    11.00000   -1.20000
AFIX   0
C12A  1    0.454935    0.714232    0.862968    11.00000    0.01392    0.02116 =
         0.01562   -0.00169    0.00317    0.00033
AFIX  43
H12A  2    0.498421    0.651443    0.844919    11.00000   -1.20000
AFIX   0
C13A  1    0.311680    0.521283    0.677142    11.00000    0.01227    0.01290 =
         0.01387   -0.00060    0.00590   -0.00049
C14A  1    0.340146    0.434892    0.761381    11.00000    0.01931    0.01470 =
         0.01475    0.00003    0.00636    0.00032
AFIX  43
H14A  2    0.376568    0.475869    0.823269    11.00000   -1.20000
AFIX   0
C15A  1    0.317224    0.290856    0.758245    11.00000    0.02510    0.01536 =
         0.02181    0.00227    0.01005   -0.00014
AFIX  43
H15A  2    0.337552    0.236845    0.817420    11.00000   -1.20000
AFIX   0
C16A  1    0.265036    0.226698    0.669260    11.00000    0.02365    0.01475 =
         0.02845   -0.00226    0.01296   -0.00439
AFIX  43
H16A  2    0.249287    0.129060    0.666635    11.00000   -1.20000
AFIX   0
C17A  1    0.236355    0.308375    0.584163    11.00000    0.01996    0.01838 =
         0.02353   -0.00605    0.00714   -0.00574
AFIX  43
H17A  2    0.200600    0.266322    0.522461    11.00000   -1.20000
AFIX   0
C18A  1    0.259534    0.451605    0.588385    11.00000    0.01856    0.01695 =
         0.01646   -0.00149    0.00408   -0.00383
AFIX  43
H18A  2    0.239247    0.504547    0.528734    11.00000   -1.20000
AFIX   0
C19A  1    0.432902    0.718066    0.639041    11.00000    0.01198    0.01166 =
         0.01245   -0.00039    0.00349   -0.00030
C20A  1    0.476540    0.613169    0.597334    11.00000    0.01513    0.01168 =
         0.01559   -0.00053    0.00565   -0.00017
AFIX  43
H20A  2    0.449422    0.520595    0.590472    11.00000   -1.20000
AFIX   0
C21A  1    0.558579    0.639560    0.565386    11.00000    0.01435    0.01674 =
         0.01695   -0.00187    0.00689    0.00034
AFIX  43
H21A  2    0.586610    0.565195    0.538421    11.00000   -1.20000
AFIX   0
C22A  1    0.598973    0.774141    0.573059    11.00000    0.01299    0.02034 =
         0.01564    0.00157    0.00540   -0.00150
AFIX  43
H22A  2    0.653725    0.793064    0.550248    11.00000   -1.20000
AFIX   0
C23A  1    0.558089    0.881184    0.614707    11.00000    0.01470    0.01426 =
         0.01734    0.00122    0.00354   -0.00350
AFIX  43
H23A  2    0.584916    0.973856    0.620306    11.00000   -1.20000
AFIX   0
C24A  1    0.477904    0.852368    0.648132    11.00000    0.01423    0.01253 =
         0.01710   -0.00154    0.00499   -0.00124
AFIX  43
H24A  2    0.452554    0.926073    0.678224    11.00000   -1.20000
AFIX   0
B1A   3    0.336326    0.691726    0.677237    11.00000    0.01248    0.01276 =
         0.01165   -0.00096    0.00362   -0.00091
HKLF 4
REM  19038.res in P2(1)
REM wR2 = 0.0619, GooF = S = 1.006, Restrained GooF = 1.006 for all data
REM R1 = 0.0253 for 17627 Fo > 4sig(Fo) and 0.0273 for all 18389 data
REM 446 parameters refined using 1 restraints
END
WGHT      0.0267      0.2268
REM Instructions for potential hydrogen bonds
HTAB C11 Cl1_$1
REM Highest difference peak  0.430,  deepest hole -0.598,  1-sigma level  0.062
Q1    1   0.2448  0.5152  0.0923  11.00000  0.05    0.43
Q2    1   0.2388  0.4663  0.0756  11.00000  0.05    0.40
Q3    1   0.2352  0.0251  0.1529  11.00000  0.05    0.39
Q4    1   0.2591  0.3157  0.0788  11.00000  0.05    0.37
Q5    1   0.4557  0.6658  0.6188  11.00000  0.05    0.36
Q6    1   0.1164  0.6181  0.2872  11.00000  0.05    0.35
Q7    1  -0.0262  0.5163  0.1805  11.00000  0.05    0.35
Q8    1   0.2898  0.2613  0.7148  11.00000  0.05    0.35
Q9    1   0.2801  0.5115  0.6280  11.00000  0.05    0.35
Q10   1   0.2808  0.7495  0.6304  11.00000  0.05    0.34
Q11   1   0.2887  0.4121  0.0298  11.00000  0.05    0.34
Q12   1   0.4064  0.7017  0.2376  11.00000  0.05    0.32
Q13   1   0.2706  0.6976  0.3070  11.00000  0.05    0.31
Q14   1   0.2352  0.2350  0.1420  11.00000  0.05    0.31
Q15   1   0.1206  0.5208  0.1386  11.00000  0.05    0.31
Q16   1   0.3885  0.6944  0.6460  11.00000  0.05    0.31
Q17   1   0.1836  0.5580  0.0247  11.00000  0.05    0.31
Q18   1   0.3784  0.8674  0.9478  11.00000  0.05    0.31
Q19   1   0.1814  0.7668  0.6017  11.00000  0.05    0.31
Q20   1   0.0476  0.5352  0.1563  11.00000  0.05    0.31
;
_shelx_res_checksum     52301
data_Global
_journal_date_recd_electronic     2019-07-01
_journal_date_accepted     2019-07-13
_journal_name_full     'IUCrData'
_journal_year     2019
_journal_volume     4
_journal_issue      7
_journal_page_first     0
_journal_page_last     0
_journal_paper_category     HM
_journal_paper_doi     10.1107/S241431461901006X
_journal_coeditor_code     SU4172
_publ_contact_author_name     'Stefan M. Kilyanek'
_publ_contact_author_address
;
1 University of Arkansas
Fayetteville, AR 72701
;
_publ_contact_author_email     'kilyanek@uark.edu'
_publ_contact_author_fax     'none'
_publ_contact_author_phone     '479-575-2712'
_publ_section_title
;\
(2,2-Bipyridine-κ²N,N')chlorido[η⁶-1-methyl-4-(propan-2-yl)\
benzene]ruthenium(II) tetraphenylborate
;
loop_
    _publ_author_name
    _publ_author_footnote
    _publ_author_address
    'Thapa, Rajesh' .
;
University of Arkansas
Fayetteville,
AR 72701
USA
;
    'Kilyanek, Stefan M.' .
;
University of Arkansas
Fayetteville,
AR 72701
USA
;
_publ_section_synopsis
;\
The complex
(2,2-bipyridine-κ²N,N')chlorido[η⁶-1-methyl-4-(propan-2-\
yl)benzene]ruthenium tetraphenylborate was prepared by the reaction of the
dichlorido[1-methyl-4-(propan-2-yl)benzene]ruthenium(II) dimer with
2,2'-bipyridine, followed by the addition of ammonium tetraphenylborate.
;
