##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in          #
# Acta Crystallographica Section E. It conforms to the requirements of       #
# Notes for Authors for Acta Crystallographica Section E, and has been       #
# peer reviewed under the auspices of the IUCr Commission on Journals.       #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic.                                       #
#                                                                            #
# Software is freely available for graphical display of the structure(s)     #
# in this CIF. For information consult the CIF software page                 #
# http://www.iucr.org/resources/cif/software.                                #
#                                                                            #
# This file may be used for bona fide research purposes within the           #
# scientific community so long as proper attribution is given to the journal # 
# article from which it was obtained.                                        #
#                                                                            #
##############################################################################
data_I
_audit_creation_method     'SHELXL-2018/1'
_chemical_name_systematic
;
4-[(Prop-2-en-1-yloxy)methyl]-3,6-bis(pyridin-2-yl)pyridazine
;
_chemical_name_common     ?
_chemical_formula_moiety     'C18 H16 N4 O'
_chemical_formula_sum     'C18 H16 N4 O'
_chemical_formula_iupac     'C18 H16 N4 O'
_chemical_formula_weight     304.35
_chemical_melting_point     ?
_space_group_crystal_system     monoclinic
_space_group_name_H-M_alt     'P 21/c'
_space_group_name_Hall     '-P 2ybc'
loop_
    _space_group_symop_operation_xyz
    'x, y, z'
    '-x, y+1/2, -z+1/2'
    '-x, -y, -z'
    'x, -y-1/2, z-1/2'
_cell_length_a     8.9420(2)
_cell_length_b     15.1130(3)
_cell_length_c     11.5829(3)
_cell_angle_alpha     90
_cell_angle_beta     100.1320(10)
_cell_angle_gamma     90
_cell_volume     1540.91(6)
_cell_formula_units_Z     4
_cell_measurement_reflns_used     9267
_cell_measurement_theta_min     4.8585
_cell_measurement_theta_max     74.4815
_cell_measurement_temperature     150.(2)
_exptl_crystal_description     plate
_exptl_crystal_colour     colourless
_exptl_crystal_size_max     0.263
_exptl_crystal_size_mid     0.241
_exptl_crystal_size_min     0.078
_exptl_crystal_density_diffrn     1.312
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     640
_exptl_absorpt_coefficient_mu     0.681
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015)
;
_exptl_absorpt_correction_T_min     0.86
_exptl_absorpt_correction_T_max     0.95
_diffrn_ambient_temperature     150(2)
_diffrn_source     'INCOATEC I\mS micro-focus source'
_diffrn_radiation_type     CuK\a
_diffrn_radiation_wavelength     1.54178
_diffrn_radiation_monochromator     mirror
_diffrn_measurement_device_type     'Bruker D8 VENTURE PHOTON 100 CMOS'
_diffrn_measurement_method     'ω scans'
_diffrn_detector_area_resol_mean     10.4167
_diffrn_reflns_number     11678
_diffrn_reflns_av_R_equivalents     0.0287
_diffrn_reflns_av_unetI/netI     0.0236
_diffrn_reflns_theta_min     4.858
_diffrn_reflns_theta_max     74.473
_diffrn_reflns_theta_full     68.000
_diffrn_measured_fraction_theta_max     0.967
_diffrn_measured_fraction_theta_full     0.987
_diffrn_reflns_limit_h_min     -10
_diffrn_reflns_limit_h_max     10
_diffrn_reflns_limit_k_min     -18
_diffrn_reflns_limit_k_max     18
_diffrn_reflns_limit_l_min     -14
_diffrn_reflns_limit_l_max     13
_refine_special_details
;
Refinement of F² against ALL reflections.  The weighted R-factor wR and
goodness of fit S are based on F², conventional R-factors R are based
on F, with F set to zero for negative F². The threshold expression of
F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement.  R-factors based
on F² are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;
_reflns_number_total     3051
_reflns_number_gt     2688
_reflns_threshold_expression     'I > 2σ(I)'
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0416
_refine_ls_R_factor_gt     0.0367
_refine_ls_wR_factor_gt     0.0970
_refine_ls_wR_factor_ref     0.1012
_refine_ls_goodness_of_fit_ref     1.041
_refine_ls_restrained_S_all     1.041
_refine_ls_number_reflns     3051
_refine_ls_number_parameters     273
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     refall
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
              'w=1/[σ²(Fo²)+(0.0534P)²+0.3637P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     difmap
_atom_sites_solution_primary     'dual space'
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.000
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.184
_refine_diff_density_min     -0.150
_refine_ls_extinction_method
;
SHELXL2018 (Sheldrick, 2015b)
;
_refine_ls_extinction_coef     0.0046(5)
_refine_ls_extinction_expression
                                  'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0181 0.0091
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0311 0.0180
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0492 0.0322
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection
;
APEX3 (Bruker, 2016)
;
_computing_cell_refinement
;
SAINT (Bruker, 2016)
;
_computing_data_reduction
;
SAINT  (Bruker, 2016)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_computing_structure_refinement
;
SHELXL2018 (Sheldrick, 2015b)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg & Putz, 2012)
;
_computing_publication_material
;
SHELXTL (Sheldrick, 2008)
;
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    O O1 0.27225(10) 0.47749(5) 0.30640(7) 0.0319(2) Uani d 1 . .
    N N1 0.19512(11) 0.50876(6) 0.70191(8) 0.0283(2) Uani d 1 . .
    N N2 0.27872(11) 0.58215(6) 0.70850(8) 0.0283(2) Uani d 1 . .
    N N3 0.49183(11) 0.71463(6) 0.53716(8) 0.0299(2) Uani d 1 . .
    N N4 0.07708(13) 0.31558(7) 0.53457(10) 0.0370(3) Uani d 1 . .
    C C1 0.17076(12) 0.45900(7) 0.60429(10) 0.0249(2) Uani d 1 . .
    C C2 0.23110(12) 0.48225(7) 0.50338(10) 0.0244(2) Uani d 1 . .
    C C3 0.31696(12) 0.55846(7) 0.51158(10) 0.0257(2) Uani d 1 . .
    H H3 0.3616(15) 0.5785(9) 0.4416(12) 0.030(3) Uiso d 1 . .
    C C4 0.33924(12) 0.60672(7) 0.61566(9) 0.0244(2) Uani d 1 . .
    C C5 0.43278(12) 0.68871(7) 0.63070(10) 0.0250(2) Uani d 1 . .
    C C6 0.45861(13) 0.73441(8) 0.73683(10) 0.0292(3) Uani d 1 . .
    H H6 0.4125(17) 0.7131(10) 0.8002(13) 0.040(4) Uiso d 1 . .
    C C7 0.54897(14) 0.80913(8) 0.74716(11) 0.0329(3) Uani d 1 . .
    H H7 0.5668(18) 0.8438(11) 0.8229(15) 0.049(4) Uiso d 1 . .
    C C8 0.61156(14) 0.83614(8) 0.65191(11) 0.0326(3) Uani d 1 . .
    H H8 0.6740(17) 0.8887(10) 0.6564(14) 0.042(4) Uiso d 1 . .
    C C9 0.57918(14) 0.78700(8) 0.54977(11) 0.0323(3) Uani d 1 . .
    H H9 0.6207(17) 0.8041(10) 0.4814(14) 0.043(4) Uiso d 1 . .
    C C10 0.07702(12) 0.37891(7) 0.61505(10) 0.0269(3) Uani d 1 . .
    C C11 -0.00417(14) 0.37100(9) 0.70670(11) 0.0346(3) Uani d 1 . .
    H H11 -0.0048(18) 0.4190(11) 0.7619(14) 0.044(4) Uiso d 1 . .
    C C12 -0.08744(15) 0.29497(9) 0.71477(12) 0.0404(3) Uani d 1 . .
    H H12 -0.147(2) 0.2897(11) 0.7774(16) 0.058(5) Uiso d 1 . .
    C C13 -0.08794(16) 0.22904(9) 0.63254(12) 0.0405(3) Uani d 1 . .
    H H13 -0.1415(19) 0.1766(12) 0.6368(14) 0.050(4) Uiso d 1 . .
    C C14 -0.00414(18) 0.24243(9) 0.54512(13) 0.0440(3) Uani d 1 . .
    H H14 -0.0035(19) 0.1969(11) 0.4852(15) 0.052(5) Uiso d 1 . .
    C C15 0.20351(13) 0.43087(8) 0.39007(10) 0.0279(3) Uani d 1 . .
    H H15A 0.0898(16) 0.4252(9) 0.3600(12) 0.032(3) Uiso d 1 . .
    H H15B 0.2466(16) 0.3702(10) 0.4016(12) 0.036(4) Uiso d 1 . .
    C C16 0.23624(15) 0.43750(8) 0.19364(10) 0.0321(3) Uani d 1 . .
    H H16A 0.1233(17) 0.4420(9) 0.1637(13) 0.037(4) Uiso d 1 . .
    H H16B 0.2670(16) 0.3739(10) 0.1992(13) 0.038(4) Uiso d 1 . .
    C C17 0.32018(17) 0.48569(9) 0.11329(11) 0.0377(3) Uani d 1 . .
    H H17 0.436(2) 0.4884(12) 0.1409(17) 0.065(5) Uiso d 1 . .
    C C18 0.2574(2) 0.51972(11) 0.01194(13) 0.0497(4) Uani d 1 . .
    H H18A 0.150(2) 0.5087(12) -0.0128(17) 0.065(6) Uiso d 1 . .
    H H18B 0.314(2) 0.5515(13) -0.0442(18) 0.068(5) Uiso d 1 . .
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    O1 C15 . 1.4224(13) ?
    O1 C16 . 1.4237(14) ?
    N1 N2 . 1.3322(13) ?
    N1 C1 . 1.3434(15) ?
    N2 C4 . 1.3386(14) ?
    N3 C9 . 1.3370(15) ?
    N3 C5 . 1.3445(14) ?
    N4 C10 . 1.3362(15) ?
    N4 C14 . 1.3400(17) ?
    C1 C2 . 1.4151(15) ?
    C1 C10 . 1.4901(15) ?
    C2 C3 . 1.3782(15) ?
    C2 C15 . 1.5075(15) ?
    C3 C4 . 1.3930(15) ?
    C3 H3 . 1.012(14) ?
    C4 C5 . 1.4880(15) ?
    C5 C6 . 1.3934(16) ?
    C6 C7 . 1.3813(17) ?
    C6 H6 . 0.959(15) ?
    C7 C8 . 1.3836(17) ?
    C7 H7 . 1.010(17) ?
    C8 C9 . 1.3836(17) ?
    C8 H8 . 0.966(16) ?
    C9 H9 . 0.968(15) ?
    C10 C11 . 1.3926(17) ?
    C11 C12 . 1.3813(18) ?
    C11 H11 . 0.968(17) ?
    C12 C13 . 1.378(2) ?
    C12 H12 . 0.974(17) ?
    C13 C14 . 1.377(2) ?
    C13 H13 . 0.931(18) ?
    C14 H14 . 0.978(17) ?
    C15 H15A . 1.019(14) ?
    C15 H15B . 0.994(15) ?
    C16 C17 . 1.4851(18) ?
    C16 H16A . 1.011(15) ?
    C16 H16B . 0.999(15) ?
    C17 C18 . 1.314(2) ?
    C17 H17 . 1.03(2) ?
    C18 H18A . 0.96(2) ?
    C18 H18B . 1.01(2) ?
loop_
    _geom_contact_atom_site_label_1
    _geom_contact_atom_site_label_2
    _geom_contact_distance
    _geom_contact_site_symmetry_1
    _geom_contact_site_symmetry_2
    _geom_contact_publ_flag
    O1 C11 3.2992(16) . 3_566 yes
    O1 H3 2.232(14) . . yes
    O1 H11 2.850(16) . 3_566 yes
    N1 C8 3.4105(15) . 2_646 yes
    N4 C15 2.7895(16) . . yes
    N1 H8 2.586(15) . 2_646 yes
    N1 H11 2.441(16) . . yes
    N1 H15A 2.713(14) . 3_566 yes
    N2 H18B 2.86(2) . 1_556 yes
    N2 H13 2.744(17) . 2_556 yes
    N2 H6 2.455(15) . . yes
    N3 H3 2.522(14) . . yes
    N3 H15B 2.652(15) . 3_666 yes
    N4 H15A 2.632(14) . . yes
    N4 H15B 2.485(14) . . yes
    C1 C7 3.5853(17) . 2_646 yes
    C2 C10 3.5420(15) . 3_566 yes
    C3 C11 3.5866(17) . 3_566 yes
    C6 C12 3.5808(18) . 2_556 yes
    C8 C10 3.5797(17) . 2_656 yes
    C11 C15 3.5633(18) . 3_566 yes
    C1 H7 2.925(17) . 2_646 yes
    C6 H16B 2.933(15) . 3_666 yes
    C9 H15B 2.842(15) . 3_666 yes
    C18 H8 2.920(16) . 2_645 yes
    H6 H9 2.56(2) . 4_576 yes
    H8 N1 2.586(16) . 2_656 yes
    H11 H16A 2.57(2) . 3_566 yes
    H12 C6 2.886(18) . 2_546 yes
    H12 H14 2.53(3) . 4_566 yes
    H13 H18B 2.55(3) . 2_545 yes
    H15A H16A 2.36(2) . . yes
    H15B H16B 2.38(2) . . yes
    H16A H18A 2.33(2) . . yes
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    C15 O1 C16 . . 111.09(9) ?
    N2 N1 C1 . . 121.37(9) ?
    N1 N2 C4 . . 119.14(9) ?
    C9 N3 C5 . . 117.07(10) ?
    C10 N4 C14 . . 117.42(11) ?
    N1 C1 C2 . . 121.82(10) ?
    N1 C1 C10 . . 113.24(10) ?
    C2 C1 C10 . . 124.93(10) ?
    C3 C2 C1 . . 116.06(10) ?
    C3 C2 C15 . . 119.63(10) ?
    C1 C2 C15 . . 124.29(10) ?
    C2 C3 C4 . . 119.36(10) ?
    C2 C3 H3 . . 119.3(8) ?
    C4 C3 H3 . . 121.3(8) ?
    N2 C4 C3 . . 122.25(10) ?
    N2 C4 C5 . . 115.80(10) ?
    C3 C4 C5 . . 121.95(10) ?
    N3 C5 C6 . . 122.61(10) ?
    N3 C5 C4 . . 116.15(10) ?
    C6 C5 C4 . . 121.24(10) ?
    C7 C6 C5 . . 119.03(11) ?
    C7 C6 H6 . . 122.1(9) ?
    C5 C6 H6 . . 118.8(9) ?
    C6 C7 C8 . . 118.99(11) ?
    C6 C7 H7 . . 120.0(9) ?
    C8 C7 H7 . . 121.0(9) ?
    C9 C8 C7 . . 118.05(11) ?
    C9 C8 H8 . . 121.2(9) ?
    C7 C8 H8 . . 120.7(9) ?
    N3 C9 C8 . . 124.25(11) ?
    N3 C9 H9 . . 115.5(9) ?
    C8 C9 H9 . . 120.3(9) ?
    N4 C10 C11 . . 122.32(11) ?
    N4 C10 C1 . . 117.02(10) ?
    C11 C10 C1 . . 120.65(10) ?
    C12 C11 C10 . . 118.85(12) ?
    C12 C11 H11 . . 120.9(9) ?
    C10 C11 H11 . . 120.3(10) ?
    C13 C12 C11 . . 119.41(12) ?
    C13 C12 H12 . . 121.3(10) ?
    C11 C12 H12 . . 119.3(10) ?
    C14 C13 C12 . . 117.79(12) ?
    C14 C13 H13 . . 121.0(10) ?
    C12 C13 H13 . . 121.2(10) ?
    N4 C14 C13 . . 124.22(13) ?
    N4 C14 H14 . . 116.4(10) ?
    C13 C14 H14 . . 119.4(10) ?
    O1 C15 C2 . . 108.29(9) ?
    O1 C15 H15A . . 109.5(8) ?
    C2 C15 H15A . . 110.0(8) ?
    O1 C15 H15B . . 110.2(8) ?
    C2 C15 H15B . . 111.0(8) ?
    H15A C15 H15B . . 107.9(11) ?
    O1 C16 C17 . . 108.01(10) ?
    O1 C16 H16A . . 109.7(8) ?
    C17 C16 H16A . . 109.7(8) ?
    O1 C16 H16B . . 109.5(9) ?
    C17 C16 H16B . . 110.4(8) ?
    H16A C16 H16B . . 109.5(12) ?
    C18 C17 C16 . . 124.63(15) ?
    C18 C17 H17 . . 120.8(11) ?
    C16 C17 H17 . . 114.5(11) ?
    C17 C18 H18A . . 116.3(12) ?
    C17 C18 H18B . . 125.0(12) ?
    H18A C18 H18B . . 118.4(16) ?
loop_
    _geom_torsion_atom_site_label_1
    _geom_torsion_atom_site_label_2
    _geom_torsion_atom_site_label_3
    _geom_torsion_atom_site_label_4
    _geom_torsion_site_symmetry_1
    _geom_torsion_site_symmetry_2
    _geom_torsion_site_symmetry_3
    _geom_torsion_site_symmetry_4
    _geom_torsion
    _geom_torsion_publ_flag
    C1 N1 N2 C4 . . . . 0.15(16) ?
    N2 N1 C1 C2 . . . . -0.61(16) ?
    N2 N1 C1 C10 . . . . 178.92(9) ?
    N1 C1 C2 C3 . . . . 0.42(15) ?
    C10 C1 C2 C3 . . . . -179.06(10) ?
    N1 C1 C2 C15 . . . . -177.88(10) ?
    C10 C1 C2 C15 . . . . 2.64(17) ?
    C1 C2 C3 C4 . . . . 0.20(15) ?
    C15 C2 C3 C4 . . . . 178.58(10) ?
    N1 N2 C4 C3 . . . . 0.49(16) ?
    N1 N2 C4 C5 . . . . -179.18(9) ?
    C2 C3 C4 N2 . . . . -0.66(16) ?
    C2 C3 C4 C5 . . . . 179.00(10) ?
    C9 N3 C5 C6 . . . . 0.51(17) ?
    C9 N3 C5 C4 . . . . -178.47(10) ?
    N2 C4 C5 N3 . . . . -178.91(10) ?
    C3 C4 C5 N3 . . . . 1.41(15) ?
    N2 C4 C5 C6 . . . . 2.09(15) ?
    C3 C4 C5 C6 . . . . -177.59(10) ?
    N3 C5 C6 C7 . . . . -0.32(18) ?
    C4 C5 C6 C7 . . . . 178.61(10) ?
    C5 C6 C7 C8 . . . . -0.24(18) ?
    C6 C7 C8 C9 . . . . 0.57(18) ?
    C5 N3 C9 C8 . . . . -0.14(18) ?
    C7 C8 C9 N3 . . . . -0.4(2) ?
    C14 N4 C10 C11 . . . . -0.41(18) ?
    C14 N4 C10 C1 . . . . 178.51(11) ?
    N1 C1 C10 N4 . . . . -164.56(10) ?
    C2 C1 C10 N4 . . . . 14.96(16) ?
    N1 C1 C10 C11 . . . . 14.38(15) ?
    C2 C1 C10 C11 . . . . -166.10(11) ?
    N4 C10 C11 C12 . . . . 0.07(19) ?
    C1 C10 C11 C12 . . . . -178.81(11) ?
    C10 C11 C12 C13 . . . . 0.1(2) ?
    C11 C12 C13 C14 . . . . 0.0(2) ?
    C10 N4 C14 C13 . . . . 0.6(2) ?
    C12 C13 C14 N4 . . . . -0.4(2) ?
    C16 O1 C15 C2 . . . . -173.64(9) ?
    C3 C2 C15 O1 . . . . -2.59(14) ?
    C1 C2 C15 O1 . . . . 175.66(9) ?
    C15 O1 C16 C17 . . . . -176.11(10) ?
    O1 C16 C17 C18 . . . . -126.92(14) ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    _geom_hbond_publ_flag
    C8 H8 N1 2_656 0.966(16) 2.585(16) 3.4104(15) 143.4(12) yes
    C15 H15B Cg 3_666 0.994(15) 2.990(15) 3.8760(13) 149.0(11) yes
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_T_min     0.841
_shelx_estimated_absorpt_T_max     0.949
data_global
_journal_date_recd_electronic     2019-07-29
_journal_date_accepted     2019-08-10
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2019
_journal_volume     75
_journal_issue      9
_journal_page_first     1321
_journal_page_last     1326
_journal_paper_category     GO
_journal_paper_doi     10.1107/S2056989019011186
_journal_coeditor_code     LH5915
_publ_contact_author
;
Nada Kheira Sebbar
Laboratoire de Chimie bioorganique appliquée
Faculté des sciences
Université Ibn Zohr
Agadir
Morocco
Laboratoire de Chimie Organique Hétérocyclique URAC 21,
Pôle de Compétence Pharmacochimie,
Av. Ibn Battouta, BP 1014,
Faculté des Sciences,
Université Mohammed V,
Rabat,
Morocco
;
_publ_contact_author_email     'nadouchsebbarkheira@gmail.com'
_publ_contact_author_fax     ?
_publ_contact_author_phone     ?
_publ_section_title
;
Crystal structure, Hirshfeld surface analysis and interaction energy and DFT
studies of 4-[(prop-2-en-1-yloxy)methyl]-3,6-bis(pyridin-2-yl)pyridazine
;
loop_
    _publ_author_name
    _publ_author_footnote
    _publ_author_address
    'Filali, Mouad' .
;
Laboratoire de Chimie Organique Appliquée,
Université Sidi Mohamed Ben Abdallah,
Faculté des Sciences et Techniques,
Route d'Immouzzer,
BP 2202,
Fez,
Morocco
;
    'Sebbar, Nada Kheira' .
;
Laboratoire de Chimie Bioorganique Appliquée,
Faculté des Sciences,
Université Ibn Zohr,
Agadir
Morocco
Laboratoire de Chimie Organique Hétérocyclique URAC 21,
Pôle de Compétence Pharmacochimie,
Av. Ibn Battouta, BP 1014,
Faculté des Sciences,
Université Mohammed V,
Rabat,
Morocco
;
    'Hökelek, Tuncer' .
;
Department of Physics
Hacettepe University
06800 Beytepe
Ankara
Turkey
;
    'Mague, Joel T.' .
;
Department of Chemistry
Tulane University
New Orleans, LA 70118
USA
;
    'Chakroune, Said' .
;
Laboratoire de Chimie Organique Appliquée,
Université Sidi Mohamed Ben Abdallah,
Faculté des Sciences et Techniques,
Route d'Immouzzer,
BP 2202,
Fez,
Morocco
;
    'Ben-Tama, Abdessalam' .
;
Laboratoire de Chimie Organique Appliquée,
Université Sidi Mohamed Ben Abdallah,
Faculté des Sciences et Techniques,
Route d'Immouzzer,
BP 2202,
Fez,
Morocco
;
    'El Hadrami, El Mestafa' .
;
Laboratoire de Chimie Organique Appliquée,
Université Sidi Mohamed Ben Abdallah,
Faculté des Sciences et Techniques,
Route d'Immouzzer,
BP 2202,
Fez,
Morocco
;
_publ_section_synopsis
;
The title compound consists of a 3,6-bis(pyridin-2-yl)pyridazine unit linked to
a 4-[(prop-2-en-1-yloxy)methyl] moiety. The pyridine-2-yl rings are rotated
slightly out of the plane of the pyridazine ring. In the crystal, C---H...N
hydrogen bonds and C---H...π  interactions link the molecules, forming deeply
corrugated layers approximately parallel to the bc plane and stacked
along the a-axis direction.
;
