##############################################################################
###                                                                        ###
###        Electronic paper (Acta Crystallographica Section E)             ###
###                                                                        ###
##############################################################################
#                                                                            #
# This CIF contains the data in a paper accepted for publication in Acta     #
# Crystallographica Section E. It conforms to the requirements of Notes      #
# for Authors for Section E, and has been peer reviewed under the auspices   #
# of the IUCr Commission on Journals.                                        #
#                                                                            #
# Full details of the Crystallographic Information File format               #
# are given in the paper "The Crystallographic Information File (CIF):       #
# a New Standard Archive File for Crystallography" by S. R. Hall, F. H.      #
# Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685].                  #
#                                                                            #
# The current version of the core CIF dictionary is obtainable from          #
# ftp://ftp.iucr.org/pub/cif_core.dic. The current version number is 2.1.    #
#                                                                            #
# Software is freely available for graphical display of the structure(s) in  #
# this CIF.  For information consult the CIF home page http://www.iucr.org/  #
# cif/home.html                                                              #
#                                                                            #
#            Copyright International Union of Crystallography                #
#                                                                            #
##############################################################################
                                             
data_I
_audit_creation_method     SHELXL-97
_chemical_name_systematic
;
Pyridinium aquapyridinebis(salicylato-κ²O,O')manganese(III)
;
_chemical_name_common     'C24 H21 Mn N2 O7'
_chemical_formula_moiety     'C19 H15 Mn N O7, C5 H6 N'
_chemical_formula_sum     'C24 H21 Mn N2 O7'
_chemical_formula_iupac     '(C5 H6 N) [Mn (C7 H4 O2)2 (C5 H5 N) (H2 O)]'
_chemical_formula_weight     504.37
_chemical_melting_point     ?
_symmetry_cell_setting     Monoclinic
_symmetry_space_group_name_H-M     'P 21/n'
_symmetry_space_group_name_Hall     -P2yn
loop_
    _symmetry_equiv_pos_as_xyz
    'x, y, z'
    '-x+1/2, y+1/2, -z+1/2'
    '-x, -y, -z'
    'x-1/2, -y-1/2, z-1/2'
_cell_length_a     12.0499(9)
_cell_length_b     11.3964(7)
_cell_length_c     16.4446(11)
_cell_angle_alpha     90.00
_cell_angle_beta     104.579(2)
_cell_angle_gamma     90.00
_cell_volume     2185.5(3)
_cell_formula_units_Z     4
_cell_measurement_reflns_used     4113
_cell_measurement_theta_min     2.20
_cell_measurement_theta_max     27.48
_cell_measurement_temperature     295(2)
_exptl_crystal_description     'Prism'
_exptl_crystal_colour     'dark brown'
_exptl_crystal_size_max     0.3
_exptl_crystal_size_mid     0.2
_exptl_crystal_size_min     0.1
_exptl_crystal_density_diffrn     1.533
_exptl_crystal_density_meas     ?
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000     1040
_exptl_absorpt_coefficient_mu     0.654
_exptl_absorpt_correction_type     multi-scan
_exptl_absorpt_process_details     '(SADABS; Sheldrick, 1996)'
_exptl_absorpt_correction_T_min     0.8077
_exptl_absorpt_correction_T_max     1.0000
_exptl_special_details
;
;
_diffrn_ambient_temperature     295(2)
_diffrn_radiation_type     MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_source     'fine-focus sealed tube'
_diffrn_radiation_monochromator     graphite
_diffrn_measurement_device_type     'Rigaku MERCURY CCD'
_diffrn_measurement_method     ω
_diffrn_detector_area_resol_mean     ?
_diffrn_reflns_number     16400
_diffrn_reflns_av_R_equivalents     0.0397
_diffrn_reflns_av_sigmaI/netI     0.0339
_diffrn_reflns_theta_min     2.41
_diffrn_reflns_theta_max     27.48
_diffrn_reflns_theta_full     27.48
_diffrn_measured_fraction_theta_max     0.999
_diffrn_measured_fraction_theta_full     0.999
_diffrn_reflns_limit_h_min     -12
_diffrn_reflns_limit_h_max     15
_diffrn_reflns_limit_k_min     -14
_diffrn_reflns_limit_k_max     12
_diffrn_reflns_limit_l_min     -21
_diffrn_reflns_limit_l_max     19
_diffrn_standards_number     0
_diffrn_standards_interval_count     0
_diffrn_standards_interval_time     0
_diffrn_standards_decay_%     0
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
_reflns_number_total     5015
_reflns_number_gt     3770
_reflns_threshold_expression     I>2σ(I)
_refine_ls_structure_factor_coef     Fsqd
_refine_ls_matrix_type     full
_refine_ls_R_factor_all     0.0711
_refine_ls_R_factor_gt     0.0479
_refine_ls_wR_factor_gt     0.1107
_refine_ls_wR_factor_ref     0.1221
_refine_ls_goodness_of_fit_ref     1.080
_refine_ls_restrained_S_all     1.080
_refine_ls_number_reflns     5015
_refine_ls_number_parameters     319
_refine_ls_number_restraints     0
_refine_ls_hydrogen_treatment     mixed
_refine_ls_weighting_scheme     calc
_refine_ls_weighting_details
         'calc w=1/[σ²(Fo²)+(0.0591P)²+0.2983P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens     geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary     difmap
_refine_ls_shift/su_max     0.001
_refine_ls_shift/su_mean     0.000
_refine_diff_density_max     0.351
_refine_diff_density_min     -0.354
_refine_ls_extinction_method     none
_refine_ls_extinction_coef     ?
loop_
    _atom_type_symbol
    _atom_type_description
    _atom_type_scat_dispersion_real
    _atom_type_scat_dispersion_imag
    _atom_type_scat_source
    'C' 'C' 0.0033 0.0016
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'H' 'H' 0.0000 0.0000
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'N' 'N' 0.0061 0.0033
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'O' 'O' 0.0106 0.0060
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
    'Mn' 'Mn' 0.3368 0.7283
                         'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_computing_data_collection     'CrystalClear (Rigaku, 2000)'
_computing_cell_refinement     'CrystalClear'
_computing_data_reduction     'CrystalClear'
_computing_structure_solution     'SHELXS97 (Sheldrick, 1997)'
_computing_structure_refinement     'SHELXL97 (Sheldrick, 1997)'
_computing_molecular_graphics     'SHELXTL (Bruker, 1997)'
_computing_publication_material     'SHELXTL'
loop_
    _atom_site_type_symbol
    _atom_site_label
    _atom_site_fract_x
    _atom_site_fract_y
    _atom_site_fract_z
    _atom_site_U_iso_or_equiv
    _atom_site_adp_type
    _atom_site_calc_flag
    _atom_site_refinement_flags
    _atom_site_occupancy
    _atom_site_disorder_assembly
    _atom_site_disorder_group
    Mn Mn 0.73667(3) 0.81871(3) 0.98464(2) 0.03360(13) Uani d . 1 . .
    O O1 0.78748(15) 0.82648(15) 1.10238(10) 0.0451(4) Uani d . 1 . .
    O O2 0.89258(14) 0.81669(13) 0.97417(10) 0.0382(4) Uani d . 1 . .
    O O3 1.07537(14) 0.85439(15) 1.00196(11) 0.0459(4) Uani d . 1 . .
    O O4 0.68969(14) 0.80995(14) 0.86739(10) 0.0386(4) Uani d . 1 . .
    O O5 0.58054(14) 0.81959(14) 0.99278(11) 0.0419(4) Uani d . 1 . .
    O O6 0.39422(16) 0.84936(16) 0.95298(14) 0.0571(5) Uani d . 1 . .
    O O7 0.73164(18) 1.01470(17) 0.97321(13) 0.0538(5) Uani d . 1 . .
    C C1 0.8891(2) 0.8647(2) 1.14617(14) 0.0363(5) Uani d . 1 . .
    C C2 0.9006(2) 0.8895(2) 1.23191(15) 0.0461(6) Uani d . 1 . .
    H H2A 0.8366 0.8795 1.2551 0.055 Uiso calc R 1 . .
    C C3 1.0026(3) 0.9280(2) 1.28206(15) 0.0540(7) Uani d . 1 . .
    H H3A 1.0085 0.9426 1.3399 0.065 Uiso calc R 1 . .
    C C4 1.0973(3) 0.9459(2) 1.25041(16) 0.0547(7) Uani d . 1 . .
    H H4A 1.1673 0.9741 1.2856 0.066 Uiso calc R 1 . .
    C C5 1.0881(2) 0.9221(2) 1.16692(16) 0.0438(6) Uani d . 1 . .
    H H5A 1.1528 0.9338 1.1447 0.053 Uiso calc R 1 . .
    C C6 0.9853(2) 0.88076(18) 1.11365(14) 0.0342(5) Uani d . 1 . .
    C C7 0.98561(19) 0.85043(18) 1.02654(14) 0.0326(5) Uani d . 1 . .
    C C8 0.5944(2) 0.8604(2) 0.82185(14) 0.0362(5) Uani d . 1 . .
    C C9 0.5906(2) 0.8885(2) 0.73793(15) 0.0487(6) Uani d . 1 . .
    H H9A 0.6552 0.8725 0.7164 0.058 Uiso calc R 1 . .
    C C10 0.4947(3) 0.9386(3) 0.68677(18) 0.0612(8) Uani d . 1 . .
    H H10A 0.4933 0.9557 0.6300 0.073 Uiso calc R 1 . .
    C C11 0.4000(3) 0.9648(3) 0.71645(18) 0.0620(8) Uani d . 1 . .
    H H11A 0.3346 1.0012 0.6809 0.074 Uiso calc R 1 . .
    C C12 0.4019(2) 0.9376(2) 0.79782(18) 0.0516(7) Uani d . 1 . .
    H H12A 0.3367 0.9549 0.8183 0.062 Uiso calc R 1 . .
    C C13 0.4978(2) 0.88459(19) 0.85187(15) 0.0375(5) Uani d . 1 . .
    C C14 0.4893(2) 0.85055(19) 0.93675(16) 0.0394(6) Uani d . 1 . .
    C C15 0.6636(2) 0.5543(2) 1.02244(17) 0.0489(6) Uani d . 1 . .
    H H15A 0.6089 0.5981 1.0425 0.059 Uiso calc R 1 . .
    C C16 0.6601(3) 0.4340(2) 1.02669(18) 0.0562(7) Uani d . 1 . .
    H H16A 0.6038 0.3960 1.0488 0.067 Uiso calc R 1 . .
    C C17 0.7390(3) 0.3696(3) 0.99850(17) 0.0556(7) Uani d . 1 . .
    H H17A 0.7387 0.2863 1.0006 0.067 Uiso calc R 1 . .
    C C18 0.8181(3) 0.4285(2) 0.96733(18) 0.0571(7) Uani d . 1 . .
    H H18A 0.8743 0.3867 0.9477 0.069 Uiso calc R 1 . .
    C C19 0.8152(2) 0.5494(2) 0.96471(16) 0.0497(7) Uani d . 1 . .
    H H19A 0.8703 0.5893 0.9424 0.060 Uiso calc R 1 . .
    C C20 1.1134(3) 0.7948(3) 0.8006(2) 0.0605(8) Uani d . 1 . .
    H H20A 1.1857 0.8196 0.8342 0.073 Uiso calc R 1 . .
    C C21 1.1028(3) 0.7619(3) 0.7205(2) 0.0658(9) Uani d . 1 . .
    H H21A 1.1670 0.7656 0.6969 0.079 Uiso calc R 1 . .
    C C22 0.9997(3) 0.7233(3) 0.67344(18) 0.0636(9) Uani d . 1 . .
    H H22A 0.9922 0.6979 0.6173 0.076 Uiso calc R 1 . .
    C C23 0.9066(3) 0.7210(3) 0.70732(19) 0.0667(9) Uani d . 1 . .
    H H23A 0.8342 0.6941 0.6751 0.080 Uiso calc R 1 . .
    C C24 0.9201(3) 0.7585(3) 0.78877(19) 0.0597(8) Uani d . 1 . .
    H H24A 0.8565 0.7597 0.8131 0.072 Uiso calc R 1 . .
    N N1 0.73941(17) 0.61282(18) 0.99179(12) 0.0402(5) Uani d . 1 . .
    N N2 1.0221(2) 0.7927(2) 0.83277(16) 0.0541(6) Uani d . 1 . .
    H H7B 0.799(3) 1.054(3) 0.9837(19) 0.074(10) Uiso d . 1 . .
    H H7A 0.686(3) 1.053(3) 1.0003(19) 0.075(10) Uiso d . 1 . .
    H H2B 1.033(4) 0.817(3) 0.890(3) 0.127(16) Uiso d . 1 . .
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
    _geom_bond_atom_site_label_1
    _geom_bond_atom_site_label_2
    _geom_bond_site_symmetry_2
    _geom_bond_distance
    _geom_bond_publ_flag
    Mn O4 . 1.8705(16) yes
    Mn O1 . 1.8800(16) yes
    Mn O5 . 1.9194(16) yes
    Mn O2 1 1.9294(16) ?
    Mn O2 . 1.9294(16) yes
    Mn O7 . 2.241(2) yes
    Mn N1 . 2.349(2) yes
    O1 C1 . 1.328(3) ?
    O2 C7 . 1.288(3) ?
    O3 C7 . 1.247(3) ?
    O4 C8 . 1.334(3) ?
    O5 C14 . 1.293(3) ?
    O6 C14 . 1.240(3) ?
    O7 H7B . 0.90(3) ?
    O7 H7A . 0.90(3) ?
    C1 C6 . 1.405(3) ?
    C1 C2 . 1.410(3) ?
    C2 C3 . 1.368(4) ?
    C2 H2A . 0.9500 ?
    C3 C4 . 1.384(4) ?
    C3 H3A . 0.9500 ?
    C4 C5 . 1.376(3) ?
    C4 H4A . 0.9500 ?
    C5 C6 . 1.407(3) ?
    C5 H5A . 0.9500 ?
    C6 C7 . 1.475(3) ?
    C7 O3 1 1.247(3) ?
    C7 O2 1 1.288(3) ?
    C8 C13 . 1.401(3) ?
    C8 C9 . 1.406(3) ?
    C9 C10 . 1.372(4) ?
    C9 H9A . 0.9500 ?
    C10 C11 . 1.382(4) ?
    C10 H10A . 0.9500 ?
    C11 C12 . 1.368(4) ?
    C11 H11A . 0.9500 ?
    C12 C13 . 1.405(4) ?
    C12 H12A . 0.9500 ?
    C13 C14 . 1.477(3) ?
    C15 N1 . 1.328(3) ?
    C15 C16 . 1.375(4) ?
    C15 H15A . 0.9500 ?
    C16 C17 . 1.370(4) ?
    C16 H16A . 0.9500 ?
    C17 C18 . 1.367(4) ?
    C17 H17A . 0.9500 ?
    C18 C19 . 1.378(4) ?
    C18 H18A . 0.9500 ?
    C19 N1 . 1.327(3) ?
    C19 H19A . 0.9500 ?
    C20 N2 . 1.336(4) ?
    C20 C21 . 1.344(4) ?
    C20 H20A . 0.9500 ?
    C21 C22 . 1.361(5) ?
    C21 H21A . 0.9500 ?
    C22 C23 . 1.373(4) ?
    C22 H22A . 0.9500 ?
    C23 C24 . 1.376(4) ?
    C23 H23A . 0.9500 ?
    C24 N2 . 1.318(4) ?
    C24 H24A . 0.9500 ?
    N2 H2B . 0.95(4) ?
loop_
    _geom_angle_atom_site_label_1
    _geom_angle_atom_site_label_2
    _geom_angle_atom_site_label_3
    _geom_angle_site_symmetry_1
    _geom_angle_site_symmetry_3
    _geom_angle
    _geom_angle_publ_flag
    O4 Mn O1 . . 178.62(7) yes
    O4 Mn O5 . . 91.41(7) ?
    O1 Mn O5 . . 89.93(7) yes
    O4 Mn O2 . . 87.49(7) yes
    O1 Mn O2 . . 91.17(7) ?
    O5 Mn O2 . . 178.85(7) yes
    O4 Mn O7 . . 88.39(7) ?
    O1 Mn O7 . . 91.97(8) yes
    O5 Mn O7 . . 89.68(7) yes
    O2 Mn O7 . . 90.62(7) ?
    O4 Mn N1 . . 89.72(7) ?
    O1 Mn N1 . . 89.93(7) ?
    O5 Mn N1 . . 90.20(7) ?
    O2 Mn N1 . . 89.47(7) ?
    O7 Mn N1 . . 178.10(7) yes
    C1 O1 Mn . . 126.20(14) ?
    C7 O2 Mn . . 129.76(14) ?
    C8 O4 Mn . . 123.39(14) ?
    C8 O4 H24A . . 124.3 ?
    Mn O4 H24A . . 108.9 ?
    C14 O5 Mn . . 128.63(15) ?
    Mn O7 H7B . . 118(2) ?
    Mn O7 H7A . . 117(2) ?
    H7B O7 H7A . . 107(3) ?
    O1 C1 C6 . . 124.9(2) ?
    O1 C1 C2 . . 116.9(2) ?
    C6 C1 C2 . . 118.2(2) ?
    C3 C2 C1 . . 120.9(3) ?
    C3 C2 H2A . . 119.5 ?
    C1 C2 H2A . . 119.5 ?
    C2 C3 C4 . . 121.4(2) ?
    C2 C3 H3A . . 119.3 ?
    C4 C3 H3A . . 119.3 ?
    C5 C4 C3 . . 118.6(3) ?
    C5 C4 H4A . . 120.7 ?
    C3 C4 H4A . . 120.7 ?
    C4 C5 C6 . . 121.6(3) ?
    C4 C5 H5A . . 119.2 ?
    C6 C5 H5A . . 119.2 ?
    C1 C6 C5 . . 119.2(2) ?
    C1 C6 C7 . . 122.9(2) ?
    C5 C6 C7 . . 117.8(2) ?
    O3 C7 O2 . . 118.3(2) ?
    O3 C7 C6 . . 121.4(2) ?
    O2 C7 C6 . . 120.3(2) ?
    O4 C8 C13 . . 124.1(2) ?
    O4 C8 C9 . . 117.4(2) ?
    C13 C8 C9 . . 118.5(2) ?
    C10 C9 C8 . . 120.7(3) ?
    C10 C9 H9A . . 119.6 ?
    C8 C9 H9A . . 119.6 ?
    C9 C10 C11 . . 121.1(3) ?
    C9 C10 H10A . . 119.4 ?
    C11 C10 H10A . . 119.4 ?
    C12 C11 C10 . . 119.0(3) ?
    C12 C11 H11A . . 120.5 ?
    C10 C11 H11A . . 120.5 ?
    C11 C12 C13 . . 121.7(3) ?
    C11 C12 H12A . . 119.2 ?
    C13 C12 H12A . . 119.2 ?
    C8 C13 C12 . . 119.1(2) ?
    C8 C13 C14 . . 122.9(2) ?
    C12 C13 C14 . . 117.9(2) ?
    O6 C14 O5 . . 120.6(2) ?
    O6 C14 C13 . . 119.6(2) ?
    O5 C14 C13 . . 119.7(2) ?
    N1 C15 C16 . . 123.6(3) ?
    N1 C15 H15A . . 118.2 ?
    C16 C15 H15A . . 118.2 ?
    C17 C16 C15 . . 118.9(3) ?
    C17 C16 H16A . . 120.5 ?
    C15 C16 H16A . . 120.5 ?
    C18 C17 C16 . . 118.2(3) ?
    C18 C17 H17A . . 120.9 ?
    C16 C17 H17A . . 120.9 ?
    C17 C18 C19 . . 119.3(3) ?
    C17 C18 H18A . . 120.4 ?
    C19 C18 H18A . . 120.4 ?
    N1 C19 C18 . . 123.2(3) ?
    N1 C19 H19A . . 118.4 ?
    C18 C19 H19A . . 118.4 ?
    N2 C20 C21 . . 119.9(3) ?
    N2 C20 H20A . . 120.0 ?
    C21 C20 H20A . . 120.0 ?
    C20 C21 C22 . . 119.7(3) ?
    C20 C21 H21A . . 120.1 ?
    C22 C21 H21A . . 120.1 ?
    C21 C22 C23 . . 119.8(3) ?
    C21 C22 H22A . . 120.1 ?
    C23 C22 H22A . . 120.1 ?
    C22 C23 C24 . . 118.7(3) ?
    C22 C23 H23A . . 120.6 ?
    C24 C23 H23A . . 120.6 ?
    N2 C24 C23 . . 119.5(3) ?
    N2 C24 H24A . . 120.3 ?
    C23 C24 H24A . . 120.3 ?
    C15 N1 C19 . . 116.8(2) ?
    C15 N1 Mn . . 121.18(18) ?
    C19 N1 Mn . . 121.97(17) ?
    C24 N2 C20 . . 122.3(3) ?
    C24 N2 H2B . . 121(3) ?
    C20 N2 H2B . . 117(3) ?
loop_
    _geom_hbond_atom_site_label_D
    _geom_hbond_atom_site_label_H
    _geom_hbond_atom_site_label_A
    _geom_hbond_site_symmetry_A
    _geom_hbond_distance_DH
    _geom_hbond_distance_HA
    _geom_hbond_distance_DA
    _geom_hbond_angle_DHA
    O7 H7B O3 3_777 0.90(3) 1.81(3) 2.706(3) 173(3)
    O7 H7A O6 3_677 0.90(3) 1.77(3) 2.665(3) 170(3)
    N2 H2B O3 1 0.95(4) 1.84(4) 2.783(3) 172(4)
    C24 H24A O4 . 0.95 2.46 3.396(3) 167
    C21 H21A O1 4_675 0.95 2.60 3.452(3) 150
data_global
_journal_date_recd_electronic     2006-11-22
_journal_date_accepted     2007-03-28
_journal_name_full     'Acta Crystallographica, Section E'
_journal_year     2007
_journal_volume     63
_journal_issue      6
_journal_page_first     m1616
_journal_page_last     m1618
_journal_paper_category     EM
_journal_coeditor_code     CS2025
_publ_contact_author     'Chen, Changneng'
_publ_contact_author_email     ccn@ms.fjirsm.ac.cn
_publ_contact_author_fax     '+86-591-83792395'
_publ_contact_author_phone     '+86-591-83792395'
_publ_section_title
;
Pyridinium aquapyridinebis(salicylato-κ²O,O')manganese(III)
;
loop_
    _publ_author_name
    _publ_author_address
    'Wang, Hui-Sheng'
;
State Key Laboratory of Structural Chemistry
Fujian Institute of Research on the Structure of Matter
Fuzhou
Fujian 350002
People's Republic of China
;
    'Ma, Cheng-Bing'
;
State Key Laboratory of Structural Chemistry
Fujian Institute of Research on the Structure of Matter
Fuzhou
Fujian 350002
People's Republic of China
;
    'Wang, Mei'
;
State Key Laboratory of Structural Chemistry
Fujian Institute of Research on the Structure of Matter
Fuzhou
Fujian 350002
People's Republic of China
;
    'Chen, Chang-Neng'
;
State Key Laboratory of Structural Chemistry
Fujian Institute of Research on the Structure of Matter
Fuzhou
Fujian 350002
People's Republic of China
;
    'Liu, Qiu-Tian'
;
State Key Laboratory of Structural Chemistry
Fujian Institute of Research on the Structure of Matter
Fuzhou
Fujian 350002
People's Republic of China
;
